JP2008238224A - Friction stir welding method - Google Patents

Friction stir welding method Download PDF

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JP2008238224A
JP2008238224A JP2007082721A JP2007082721A JP2008238224A JP 2008238224 A JP2008238224 A JP 2008238224A JP 2007082721 A JP2007082721 A JP 2007082721A JP 2007082721 A JP2007082721 A JP 2007082721A JP 2008238224 A JP2008238224 A JP 2008238224A
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joined
friction stir
stir welding
probe
solid lubricant
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JP4543204B2 (en
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Masato Tsujikawa
正人 辻川
Yukio Oki
幸男 沖
Kenji Azuma
健司 東
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Osaka Industrial Promotion Organization
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Abstract

<P>PROBLEM TO BE SOLVED: To perform superior butt welding on workpieces to be joined, without causing a misjoined part so-called kissing bond in the weld zone of the workpieces, without causing root crack, with less tendency of fatigue fracture generation, and at a low cost and with excellent productivity. <P>SOLUTION: In friction stir welding, a metallic foil 21 is clamped between the abutting part 33 including its periphery of workpieces 31, 32 and a backing 10, with a solid lubricating layer 22 interposed between the metallic foil 21 and the backing 10. Furthermore, a supporting body 23 is for facilitating support of the solid lubricant layer 22, but is not necessarily required. <P>COPYRIGHT: (C)2009,JPO&INPIT

Description

本発明は、アルミニウム合金板等の被接合材同士を良好に突合わせ接合することができる摩擦攪拌接合方法に関する。   The present invention relates to a friction stir welding method capable of satisfactorily butting and joining materials to be joined such as an aluminum alloy plate.

アルミニウム合金板等の被接合材同士を鉄鋼板等の裏当て治具の上に突合わせて載置固定し、この被接合材の突合わせ部に表面側から、被接合材の表面に接するショルダ部とその先端に突設されたプローブを有する回転ツールのプローブ(ピンとも称する)を挿入し、ツールを高速回転させながら突合わせ部に沿って相対的に移動させ、その時に発生する摩擦熱により突合わせ部を可塑化させることにより、被接合材の突合わせ部を接合する接合方法は、摩擦攪拌接合と呼ばれ、広く知られている(例えば特許文献1および2)。   The material to be joined such as an aluminum alloy plate is placed on and fixed to a backing jig such as a steel plate, and the shoulder contacting the surface of the material to be joined from the surface side to the butt part of the material to be joined. Insert a probe (also called a pin) of a rotating tool having a probe protruding at the tip and the tip of the tool, and move the tool relatively along the abutting part while rotating the tool at a high speed. A joining method for joining the butted portions of the materials to be joined by plasticizing the butted portions is called friction stir welding and is widely known (for example, Patent Documents 1 and 2).

この種の摩擦攪拌接合によれば、ツールにより被接合材に生じる摩擦熱を利用して被接合材が軟化し軟化部分が固相状態で攪拌され混合されてなる攪拌領域を形成して接合される。攪拌領域は微結晶化するため、アーク溶接などの溶融溶接に比べて、接合部における強度低下が小さく、気孔や割れなどの接合欠陥が少なく、接合部の表面面も平坦である等の利点があり、すでに鉄道車両、船舶、土木構造物、自動車などの分野で実用化されている。   According to this type of friction stir welding, the material to be welded is softened using the frictional heat generated in the material to be welded by a tool, and the softened portion is stirred and mixed in a solid phase to form a stirring region and joined. The Since the agitation region is microcrystallized, there are advantages such as less strength reduction at the joint, less joint defects such as pores and cracks, and a flat surface at the joint, compared to fusion welding such as arc welding. Yes, it has already been put to practical use in the fields of railway vehicles, ships, civil engineering structures, automobiles, etc.

このような従来の摩擦攪拌接合にあっては、被接合材へのプローブの挿入深さが接合部の品質に大きな影響を与える。プローブは被接合材の突合わせ部に表面側から内部に向けて挿入されるが、確実に接合するには、上記攪拌領域が被接合材の裏側面に達しかつ接合部の両側に一定の幅を有していることが望ましい。   In such a conventional friction stir welding, the insertion depth of the probe into the material to be joined greatly affects the quality of the joint. The probe is inserted into the butted part of the material to be joined from the front side to the inside. To ensure joining, the stirring region reaches the back side of the material to be joined and has a certain width on both sides of the joint. It is desirable to have

プローブの側面のみならず底面でも被接合材が撹拌されるので、被接合材の裏までプローブの先端が達する必要はないが、プローブの先端はできるだけ被接合材の底面ぎりぎりまで到達することが好ましい。したがって、ツール位置決め精度の高い装置を用い、攪拌領域が被接合材の突合わせ部の裏面に十分形成されるように被接合材を攪拌することが望ましい。   Since the material to be bonded is stirred not only on the side surface but also on the bottom surface of the probe, it is not necessary for the tip of the probe to reach the back of the material to be bonded, but it is preferable that the tip of the probe reaches as close as possible to the bottom surface of the material to be bonded. . Therefore, it is desirable to stir the materials to be joined using an apparatus with high tool positioning accuracy so that the stirring region is sufficiently formed on the back surface of the butted portion of the materials to be joined.

被接合材の接合部の裏側に、プローブにより攪拌されない領域あるいは攪拌不足の領域が生じると、キッシングボンドと呼ばれる突合わせ線を含む未接合部が生ずる。このような未接合部が存在すると、そこからルート割れと呼ばれる割れが発生して接合強度が低下したり、疲労破壊の起点になったりする。特に直線状のキッシングボンドがあると、キッシングボンドと直交する方向の応力を受けた場合に強度が低下しやすくなる。
なお、摩擦攪拌接合の操作を被接合材の表面側のみならず反転させて裏面側からも同様に行えば、キッシングボンドは発生しないが、この方法では生産性が著しく低下する。
If a region that is not stirred by the probe or a region that is insufficiently stirred is formed on the back side of the bonded portion of the material to be bonded, an unbonded portion including a butt line called a kissing bond is generated. If such an unjoined portion exists, a crack called a root crack is generated from the unbonded portion, resulting in a decrease in joining strength or a starting point of fatigue failure. In particular, when there is a linear kissing bond, the strength tends to decrease when a stress in a direction orthogonal to the kissing bond is applied.
If the friction stir welding operation is performed not only on the surface side of the material to be joined but also reversed and similarly performed from the back side, no kissing bond occurs, but this method significantly reduces productivity.

通常、摩擦攪拌接合においては、プローブの前進角を1〜5°程度に設定しておき、プローブの長さを被接合材の厚みよりも0.1〜0.2mm程度短くして、被接合材へのプローブの挿入深さは、できるだけ裏当て治具と接触しないように設定して接合操作が行われる。   Usually, in friction stir welding, the advance angle of the probe is set to about 1 to 5 °, and the length of the probe is made shorter by about 0.1 to 0.2 mm than the thickness of the material to be joined. The depth of insertion of the probe into the material is set so as not to contact the backing jig as much as possible, and the joining operation is performed.

しかしながら、ツールは前進角を設けて被接合材に挿入されるため斜めに差し込まれることになり、ツールの後ろ半分は深くなり、この状態で被接合材に対し相対的にツールを前進させて摩擦攪拌接合されるが、ツールに対する種々の力が生じ、微妙に上下に振動することがある。   However, since the tool is inserted into the material to be joined with an advancing angle, it is inserted diagonally, and the rear half of the tool becomes deep, and in this state, the tool is advanced relative to the material to be frictioned. Although they are agitated and joined, various forces are generated on the tool, and they may vibrate up and down slightly.

ツールが高速回転で高荷重の場合には、ショルダ部と接する被接合材は摩擦熱により軟化する。高い押圧力がツールにかかっているためツールのショルダ部と接する被接合材の軟化部分の表面部にツールのショルダ部が沈み込み、その結果プローブ先端が設定深さよりも深くなることがある。
被接合材と被接合材とを突き合わせた接合線は必ずしも直線ではなく、屈折部または曲率半径の短い曲線部では一般にツールの前進速度が落ちるため摩擦による被接合材のショルダ部に接する部分近傍の軟化が進みツールが沈み込むことがある。
以上の他にも加工中にはさまざまな変動要素があり、摩擦攪拌接合加工中のツールの深さ制御は必ずしも高精度には行えない。
When the tool rotates at a high speed and has a high load, the material to be joined that contacts the shoulder portion is softened by frictional heat. Since a high pressing force is applied to the tool, the shoulder portion of the tool may sink into the surface portion of the softened portion of the material to be joined that contacts the shoulder portion of the tool, and as a result, the probe tip may become deeper than the set depth.
The joining line where the material to be joined and the material to be joined is not necessarily a straight line. In general, in the refracted part or the curved part with a short radius of curvature, the forward speed of the tool generally decreases. It may soften and the tool may sink.
In addition to the above, there are various variable factors during machining, and the depth control of the tool during friction stir welding cannot always be performed with high accuracy.

この結果、プローブ挿入深さやプローブ姿勢(プローブ前進角)を精密に設定していても、摩擦攪拌接合加工中にプローブの先端が被接合材を突き抜けて裏当て治具の表面に接することが生じる。裏当て材は鋼製が多いため、プローブ先端が裏当て治具に接したまま前進させようとすると、プローブが折損したり先端が損傷したり、あるいは裏当て治具の表面が損傷するという問題が生じる。   As a result, even if the probe insertion depth and the probe posture (probe advance angle) are precisely set, the tip of the probe may penetrate the workpiece and contact the surface of the backing jig during the friction stir welding process. . Since the backing material is often made of steel, if you try to advance the probe while the tip of the probe is in contact with the backing jig, the probe may break or the tip may be damaged, or the surface of the backing jig may be damaged. Occurs.

上記問題に直接対処するものではないが、裏当て材に被接合材の固着とルート割れの両方を防ぐ試みがなされており、下記特許文献3には、可塑化した被接合材に対する親和性の低い裏当て材(裏当て治具)を使用する摩擦攪拌接合方法が提案されている。ここで、特に好ましい裏当て材として、炭素系材料、金属酸化物、建築用耐火断熱材料、粗面化した金属が挙げられており、高温安定性に優れ且つプローブとの潤滑性の良好な黒鉛ボード等が例示されている。   Although it does not directly address the above problem, attempts have been made to prevent both the adherence of the material to be bonded and the root cracking to the backing material. Patent Document 3 listed below has an affinity for the plasticized material to be bonded. A friction stir welding method using a low backing material (backing jig) has been proposed. Here, as a particularly preferable backing material, carbon-based materials, metal oxides, fireproof heat insulating materials for construction, and roughened metals are mentioned, and graphite having excellent high-temperature stability and good lubricity with a probe. A board or the like is illustrated.

ところが、黒鉛ボードは、通常、黒鉛の粉体から焼結固形化により成形され、黒鉛の粉末から黒鉛ボードを成形するには相当の手間がかかり、コスト高になる。   However, a graphite board is usually formed from graphite powder by sintering and solidification, and it takes much labor to form a graphite board from graphite powder, resulting in high costs.

更に、プローブの先端をできるだけ被接合材の底面ぎりぎりまで到達させたとしても、突合わせの線が残りキッシングボンドとなることがある。
摩擦攪拌接合にあっては、プローブを有するツールのショルダ部を被接合材の突合わせ部に沿って強い力で押さえるため、この押圧力により被接合材および裏当て材には、通常2,500〜5,000N程度、ときには約10,000N程度の大きな負荷がかかる。
このため攪拌時においても被接合材の底面ぎりぎりの部分が裏当て材との摩擦により攪拌されずに残り、両側の被接合材の突合せ部で形成される線が残りキッシングボンドとなるものと推察される。
特開平11−267858号公報 特開2005−205496号公報 特開平10−202374号公報
Furthermore, even if the tip of the probe is made to reach the bottom of the material to be joined as much as possible, the butt line may remain and become a kissing bond.
In the friction stir welding, the shoulder portion of the tool having the probe is pressed with a strong force along the butted portion of the material to be joined. A large load of about ˜5,000 N, sometimes about 10,000 N is applied.
For this reason, it is speculated that even at the time of agitation, the marginal part of the bottom surface of the material to be joined remains without being agitated due to friction with the backing material, and the line formed at the butt portion of the material to be joined on both sides remains as a kissing bond. Is done.
JP-A-11-267858 JP 2005-20596 A JP-A-10-202374

本発明は、上記の問題に鑑みてなされたものであり、その目的とするところは、表面側からだけの摩擦攪拌接合であっても、被接合材の接合部にキッシングボンドが発生せず、疲労破壊も発生しにくく、且つ低コストで生産性よく被接合材同士を良好に突合わせ接合することのできる摩擦攪拌接合方法を提供することにある。   The present invention has been made in view of the above problems, and the purpose of the present invention is that, even in friction stir welding only from the surface side, no kissing bond occurs in the joint portion of the material to be joined, An object of the present invention is to provide a friction stir welding method that is less likely to cause fatigue failure, and that can satisfactorily butt-join materials to be joined together at low cost and high productivity.

上記の目的は、下記の特徴を有する本発明の摩擦攪拌接合方法によって達成することができる。
すなわち、請求項1に記載の発明は、被接合材同士を裏当て治具の上に突合わせて載置固定し、この被接合材の突合わせ部に表面側からプローブを挿入し、このプローブを高速回転させながら突合わせ部に沿って相対的に移動させ、その時に発生する摩擦熱により突合わせ部を可塑化させて攪拌することにより、被接合材の突合わせ部を接合する摩擦攪拌接合方法において、
上記突合わせ部を含む被接合材と裏当て治具との間に金属箔を挟着し、かつ該金属箔と裏当て治具との間に固体潤滑剤を介在させることを特徴とする。
The above object can be achieved by the friction stir welding method of the present invention having the following characteristics.
That is, the invention described in claim 1 is to place and fix the materials to be joined together on the backing jig, and insert a probe into the abutting portion of the material to be joined from the surface side. Friction stir welding to join the butt part of the material to be joined by relatively moving along the butt part while rotating at high speed, and plasticizing the butt part by the frictional heat generated at that time and stirring In the method
A metal foil is sandwiched between a material to be joined including the butted portion and a backing jig, and a solid lubricant is interposed between the metal foil and the backing jig.

また、請求項2に記載の発明は、上記請求項1に記載の発明において、裏当て治具と固体潤滑剤との間に支持体を挟着することを特徴とする。   The invention described in claim 2 is characterized in that, in the invention described in claim 1, the support is sandwiched between the backing jig and the solid lubricant.

また、請求項3に記載の発明は、上記請求項1または2に記載の発明において、固体潤滑剤が粉体であることを特徴とする。   The invention according to claim 3 is the invention according to claim 1 or 2, wherein the solid lubricant is a powder.

また、請求項4に記載の発明は、上記請求項1または2に記載の発明において、固体潤滑剤が二硫化モリブデンの粉体または黒鉛の粉体であることを特徴とする。   According to a fourth aspect of the present invention, in the first or second aspect of the present invention, the solid lubricant is a molybdenum disulfide powder or a graphite powder.

また、請求項5に記載の発明は、請求項1乃至4のいずれかに記載の発明において、金属箔が被接合材と同質または類似の材料からなることを特徴とする。   The invention according to claim 5 is the invention according to any one of claims 1 to 4, characterized in that the metal foil is made of the same or similar material as the material to be joined.

請求項6に記載の発明は、請求項2乃至5のいずれかに記載の発明において、支持体が被接合材と同質または類似の材料からなることを特徴とする。   The invention according to claim 6 is the invention according to any one of claims 2 to 5, wherein the support is made of the same or similar material as the material to be joined.

請求項7に記載の発明は、請求項1または2に記載の発明において、被接合材がアルミニウムまたはその合金からなり、金属箔がアルミニウム箔またはその合金箔からなり、固体潤滑剤が二硫化モリブデンまたは黒鉛からなることを特徴とする。   The invention according to claim 7 is the invention according to claim 1 or 2, wherein the material to be joined is made of aluminum or an alloy thereof, the metal foil is made of an aluminum foil or an alloy foil thereof, and the solid lubricant is molybdenum disulfide. Or it consists of graphite.

請求項8に記載の発明は、請求項2に記載の発明において、被接合材がアルミニウムまたはその合金からなり、金属箔がアルミニウム箔またはその合金箔からなり、固体潤滑剤が二硫化モリブデンまたは黒鉛からなり、支持体がアルミニウムまたはその合金からなることを特徴とする。   The invention according to claim 8 is the invention according to claim 2, wherein the material to be joined is made of aluminum or an alloy thereof, the metal foil is made of an aluminum foil or an alloy foil thereof, and the solid lubricant is molybdenum disulfide or graphite. And the support is made of aluminum or an alloy thereof.

以下、図面を参照しながら本発明を詳細に説明する。
図1は本発明の摩擦攪拌接合方法の一例を示す一部切欠斜視図である。図1において、先ず、裏当て治具10の上の所望の部位に支持体23を配置した後、その上に固体潤滑剤22の粉体を層状に散布し、さらにその上に金属箔21を配置する。
Hereinafter, the present invention will be described in detail with reference to the drawings.
FIG. 1 is a partially cutaway perspective view showing an example of the friction stir welding method of the present invention. In FIG. 1, first, a support 23 is arranged at a desired position on the backing jig 10, and then a powder of the solid lubricant 22 is spread on the support 23, and a metal foil 21 is further formed thereon. Deploy.

上記の例では、金属箔21と固体潤滑剤層22と下側の支持体23とのサンドイッチ状の三層構造としたが、支持体23を省き、上側の金属箔21と固体潤滑剤層22との二層構造としてもよい。このような二層構造とする場合は、裏当て治具10の上の所望の部位に、固体潤滑剤22の粉体を直接に層状に散布し、その上に金属箔21を配置する。   In the above example, a sandwich-like three-layer structure of the metal foil 21, the solid lubricant layer 22 and the lower support 23 is used, but the support 23 is omitted and the upper metal foil 21 and the solid lubricant layer 22 are omitted. It is good also as a two-layer structure. In the case of such a two-layer structure, the powder of the solid lubricant 22 is directly dispersed in a desired layer on the backing jig 10 and the metal foil 21 is disposed thereon.

上記のようなサンドイッチ状の三層構造あるいは二層構造の形成は、上述のような方法で形成する以外に、予め金属箔21と支持体23との間に固体潤滑剤層22を形成し一体化した三層構造体あるいは予め一枚の金属箔21を二つ折りした中に固体潤滑剤層22を形成した構造体を作製しておき、このような構造体を裏当て治具10の上の所望の部位に配置するようにしてもよい。   For forming the sandwich-like three-layer structure or the two-layer structure as described above, the solid lubricant layer 22 is previously formed between the metal foil 21 and the support 23 in addition to the above-described method. A three-layer structure or a structure in which a solid lubricant layer 22 is formed in advance by folding a sheet of metal foil 21 in advance is prepared, and such a structure is placed on the backing jig 10. You may make it arrange | position in a desired site | part.

金属箔21は被接合材の裏面に当接した状態で摩擦攪拌接合され箔の厚みがバッファーになるため、プローブ先端が被接合材の裏面を突き抜け、箔の厚みまで到達させることが可能になり攪拌領域の形成が被接合材の裏面まで形成される。
一方、支持体23は主として固体潤滑剤層22を支持する役割がある。しかし、金属箔21は、プローブの攪拌により可塑化された被接合材の中に巻き込まれて分散されるので、接合強度の低下の原因となる恐れがある。
Since the metal foil 21 is friction stir welded in contact with the back surface of the material to be joined and the thickness of the foil becomes a buffer, the tip of the probe can penetrate the back surface of the material to be joined and reach the thickness of the foil. Formation of the stirring region is formed up to the back surface of the material to be joined.
On the other hand, the support 23 mainly serves to support the solid lubricant layer 22. However, since the metal foil 21 is wound and dispersed in the material to be joined that has been plasticized by the stirring of the probe, there is a possibility that the joining strength may be reduced.

このような接合強度の低下を防ぐために、金属箔は被接合材の材質あるいはそれに類似の材質のものが好適に使用される。通常、アルミニウム(合金)の接合にはアルミニウム(合金)箔が、銅(合金)の接合には銅(合金)箔が、チタン(合金)の接合にはチタン(合金)箔が、鉄(スチール)の接合には鉄(スチール)箔が、ステンレスの接合にはステンレス箔が好適に使用される。被接合材と被接合材との突合わせによる接合線は通常直線であることが多いため、金属箔21および支持体23は接合線近傍のみ存在すれば十分なことからリボン状、テープ状が好ましい。   In order to prevent such a decrease in bonding strength, the metal foil is preferably made of a material to be bonded or a similar material. Usually, aluminum (alloy) foil is used for joining aluminum (alloy), copper (alloy) foil is used for joining copper (alloy), titanium (alloy) foil is used for joining titanium (alloy), and iron (steel). ) Is preferably used as an iron (steel) foil, and stainless steel as a stainless steel foil. Since the joining line due to the joining of the material to be joined and the material to be joined is usually a straight line, it is sufficient that the metal foil 21 and the support 23 exist only in the vicinity of the joining line. .

金属箔21の厚みは、被接合材の厚みやプローブの長さなどを勘案して、10〜100μm程度の厚さのものが好ましい。金属箔21は突合わせ部を含む被接合材と裏当て治具との間、即ち被接合材の突合わせ部とその周辺に亘って被接合材と裏当て治具との間、に挟着されるため、幅は、ツールのショルダ径(通常は直径12〜15mm程度)やプローブ径(通常は直径5〜6mm程度)などを勘案すると、15mm程度の幅のものが好ましいが、それ以上の余裕のある幅であってもよい。   The thickness of the metal foil 21 is preferably about 10 to 100 μm in consideration of the thickness of the material to be joined and the length of the probe. The metal foil 21 is sandwiched between the bonded material including the butted portion and the backing jig, that is, between the bonded material and the backing jig across the butted portion of the bonded material and its periphery. Therefore, when considering the shoulder diameter of the tool (usually about 12 to 15 mm) and the probe diameter (usually about 5 to 6 mm), the width is preferably about 15 mm, but more than that The width may be sufficient.

固体潤滑剤22は、プローブ先端と裏当て材との摩擦を軽減しプローブの損傷を防止する役割がある。このような固体潤滑剤22としては、特に限定されないが結晶格子中に辷りやすい層を有する構造を有するものが好ましく、二硫化モリブデン(MoS)、黒鉛(グラファイト)、二硫化タングステン、PTFE(ポリテトラフルオロエチレン)、窒化ホウ素(BN)等 が使用できる。中でも高温安定性に優れ且つプローブとの潤滑性(減摩性)が良好な二硫化モリブデン(MoS)または黒鉛(グラファイト)が好ましい。 The solid lubricant 22 has a role of reducing friction between the probe tip and the backing material and preventing damage to the probe. The solid lubricant 22 is not particularly limited, but preferably has a structure having a layer that easily breaks in the crystal lattice. Molybdenum disulfide (MoS 2 ), graphite (graphite), tungsten disulfide, PTFE (polyethylene oxide) Tetrafluoroethylene), boron nitride (BN), etc. can be used. Among these, molybdenum disulfide (MoS 2 ) or graphite (graphite), which has excellent high-temperature stability and good lubricity (friction properties) with the probe, is preferable.

固体潤滑剤22の形状は限定されず、板状、テープ状、シート状のものであってもよいが、コスト面から粉体が好ましい。
固体潤滑剤22は、軟化した金属箔21とともに被接合材の突合わせ部の攪拌領域内に金属箔21と一緒に巻き込まれることも生じる。この場合、固体潤滑剤22の粒径が大きすぎると被接合材の接合部の強度が低下するので、その粒径は平均粒径で30μm以下が好ましい。また、固体潤滑剤22の層の厚さは、被接合材の厚みやプローブの長さなどを勘案して、0.01〜0.1g/cm程度(20〜500μm程度)のものが好適に使用される。
The shape of the solid lubricant 22 is not limited and may be a plate shape, a tape shape, or a sheet shape, but a powder is preferable from the viewpoint of cost.
The solid lubricant 22 may be engulfed together with the metal foil 21 together with the softened metal foil 21 in the stirring region of the butt portion of the material to be joined. In this case, if the particle size of the solid lubricant 22 is too large, the strength of the bonded portion of the material to be bonded is lowered. Therefore, the average particle size is preferably 30 μm or less. The thickness of the solid lubricant 22 layer is preferably about 0.01 to 0.1 g / cm 2 (about 20 to 500 μm) in consideration of the thickness of the material to be joined and the length of the probe. Used for.

特に、二硫化モリブデン(MoS)または黒鉛(グラファイト)は、いずれも金属光沢を呈し鋼灰色ないし黒色結晶質で、天然物、人造物のいずれも粒子状または粉末状で産出され得るので、粉末からボード状に成形する必要がなく、好都合である。 In particular, molybdenum disulfide (MoS 2 ) or graphite (graphite) has a metallic luster and is a steel gray or black crystalline, and both natural products and artificial products can be produced in the form of particles or powders. This is convenient because it is not necessary to form the board into a board.

支持体23は固体潤滑剤の粉をうまく裏当て治具に載せるために用いられる。形状は特定されないが、厚みは均一であることが望ましく被接合材と被接合材との突合わせによる接合線は通常直線であることが多いため、支持体は接合線近傍のみ存在すれば十分なことからリボン状、テープ状が好ましい。   The support member 23 is used for successfully placing the solid lubricant powder on the backing jig. Although the shape is not specified, it is desirable that the thickness be uniform, and the joining line by the butt between the joining material and the joining material is usually a straight line. Therefore, it is sufficient that the support exists only in the vicinity of the joining line. Therefore, a ribbon shape and a tape shape are preferable.

支持体23は、摩擦攪拌接合による熱が伝達されるので温度が上がるため耐熱性を有することが好ましい。更に固体潤滑剤粉体22がうまく潤滑作用を示すように支持体は柔らかすぎてはならず、又金属箔21を突き抜けたプローブの先端が裏当て治具10に当たらないよう、支持体23を突き抜けないことが好ましい。したがって、破断強度が小さくない方が好ましい。   It is preferable that the support 23 has heat resistance because heat is transferred by friction stir welding so that the temperature rises. Further, the support body 23 should not be too soft so that the solid lubricant powder 22 exhibits a good lubricating action, and the support body 23 should be placed so that the tip of the probe that has penetrated the metal foil 21 does not hit the backing jig 10. It is preferable not to penetrate. Therefore, it is preferable that the breaking strength is not small.

支持体23はプローブの先端により摩擦撹拌され被接合材に支持体材料の一部が巻き込まれる事態が生じた場合においても接合部分の強度を損じないことが望ましい。   Even when the support 23 is frictionally stirred by the tip of the probe and a part of the support material is caught in the material to be joined, it is desirable that the strength of the joined portion is not impaired.

したがって、上記条件を満たす支持体23としては、金属箔21と同様、被接合体となじみのよい、被接合材と同じ材質あるいはそれに類似の材質のものが好ましい。アルミニウム(合金)の接合にはアルミニウム(合金)箔が、銅(合金)の接合には銅(合金)箔が、チタン(合金)の接合にはチタン(合金)箔が、鉄(スチール)の接合には鉄(スチール)箔が、ステンレスの接合にはステンレス箔が好ましい。   Therefore, as the support 23 that satisfies the above-described conditions, the same material as the material to be joined or a material similar to the material to be joined, which is compatible with the material to be joined, is preferable as with the metal foil 21. Aluminum (alloy) foil for joining aluminum (alloy), copper (alloy) foil for joining copper (alloy), titanium (alloy) foil for joining titanium (alloy), iron (steel) An iron (steel) foil is preferable for bonding, and a stainless steel foil is preferable for bonding stainless steel.

裏当て治具10は、通常、SKD61やS50Cなどの硬い公知の鋼製の裏当て治具が好適に使用されるが、これに限定されない。ツールのショルダ部から受けるほぼ法線方向からの強い荷重に耐える剛性強度を有し座屈しないものであれば使用できる。   As the backing jig 10, a hard known steel backing jig such as SKD61 or S50C is preferably used, but it is not limited to this. Any tool can be used as long as it has sufficient rigidity to withstand a strong load in the normal direction received from the shoulder portion of the tool and does not buckle.

次に、上述の金属箔21と固体潤滑剤22と支持体23とのサンドイッチ状の三層構成あるいは金属箔21と固体潤滑剤22との二層構成のほぼ中央部に接合用の板状の被接合材31および32の突合わせ部33が位置するように、被接合材31および32を配置し慣用の固定具を用いて固定する。   Next, a plate-like plate for bonding is provided at the substantially central portion of the above-described sandwiched three-layer configuration of the metal foil 21, the solid lubricant 22 and the support 23 or the two-layer configuration of the metal foil 21 and the solid lubricant 22. The to-be-joined materials 31 and 32 are arrange | positioned so that the abutting part 33 of the to-be-joined materials 31 and 32 may be located, and it fixes using a conventional fixing tool.

被接合材31および32としては、アルミニウム(合金)をはじめ、マグネシウム(合金)、銅(合金)、チタン(合金)、鉄鋼、ステンレス等からなる板状の被接合材が使用される。これ等の被接合材31および32は、裏当て治具10の形状に対応して平たい単純な板状のものが多いが、単純な2次元的な曲面を有する板状のものであってもよく、また3次元的な曲面を有する板状のものであってもよい。特に、3次元的な曲面を有する被接合材の場合は、プローブ挿入深さやプローブ姿勢(プローブ前進角)の制御が難しいため、このような3次元的な曲面を有する被接合材の接合に有効である。   As the materials to be joined 31 and 32, plate-like materials made of aluminum (alloy), magnesium (alloy), copper (alloy), titanium (alloy), steel, stainless steel or the like are used. These materials to be joined 31 and 32 are mostly flat and simple plate-like shapes corresponding to the shape of the backing jig 10, but even if they are plate-like shapes having a simple two-dimensional curved surface. Alternatively, it may be a plate having a three-dimensional curved surface. In particular, in the case of a material to be joined having a three-dimensional curved surface, it is difficult to control the probe insertion depth and the probe posture (probe advance angle), so it is effective for joining such a material to be joined having a three-dimensional curved surface. It is.

その後、板状の被接合材31、32の突合わせ部33の一端に、回転ツール40、すなわち径の大きいショルダ部42とその先端にプローブ41を有する硬い工具鋼からなるツール40のプローブ41を強い力で挿入し、上記ツール40を矢印A方向に高速回転させながら突合わせ部33に沿って他端(矢印B方向)に移動させ、その時に発生する摩擦熱によりを突合せ部33を軟化させ攪拌することにより、被接合材31、32の突合わせ部33を可塑化して、ツール40のショルダ部42による圧力を負荷しながら接合する。   Thereafter, the probe 41 of the tool 40 made of hard tool steel having the rotary tool 40, that is, the shoulder portion 42 having a large diameter and the probe 41 at the tip thereof, is attached to one end of the abutting portion 33 of the plate-shaped materials 31 and 32. The tool 40 is inserted with a strong force and moved to the other end (arrow B direction) along the abutting portion 33 while rotating the tool 40 at a high speed in the arrow A direction, and the abutting portion 33 is softened by the frictional heat generated at that time. By agitating, the abutting portion 33 of the materials to be joined 31 and 32 is plasticized and joined while applying pressure by the shoulder portion 42 of the tool 40.

上記ツール40は、径の大きいショルダ部42とその先端にプローブ41を有し、接合する被接合材31、32の材質よりも硬いSKD61等のSKあるいはSKD工具鋼やPCBN(polycrystalline cubic boron nitride)などからなる。そして、通常、プローブ41にはねじが切ってあってもよく、ねじが切ってないものであってもよい。また、厚みが3〜6mm程度の被接合材31、32を使用する場合は、上記ツール40のショルダ部42の直径は12〜15mm程度で、プローブ41の直径は5〜6mm程度のものが好適に使用される。   The tool 40 has a shoulder portion 42 having a large diameter and a probe 41 at its tip, and is harder than the material of the materials 31 and 32 to be joined, such as SK or SKD tool steel, such as SKD61, or PCBN (polycrystalline cubic boron). Etc. In general, the probe 41 may be threaded or may not be threaded. Moreover, when using the to-be-joined materials 31 and 32 about 3-6 mm in thickness, the diameter of the shoulder part 42 of the said tool 40 is about 12-15 mm, and the diameter of the probe 41 is about 5-6 mm is suitable. Used for.

ショルダ42は、突合わせ部33に沿った被接合材31および32を押圧する必要があり、通常は被接合材31および32と当接する面が平面であるもの或いはプローブ41を中心としてやや円弧状または円錐状に凹んだものが使用されるが、場合によっては、プローブ41を中心としてやや円弧状または円錐状に突出したものも使用できる。上記プローブ41の長さは、裏当て治具10と接触しないように、プローブの先端が深く挿入されるのが好ましい。プローブ前進角は一般に1〜5°程度に設定される。また、ツール40の回転速度は一般に数百〜数千回転/分、接合速度は一般に数十〜数百mm/分である。   The shoulder 42 needs to press the materials 31 and 32 to be joined along the abutting portion 33, and usually has a flat surface in contact with the materials 31 and 32 to be joined or a slightly arc shape with the probe 41 as the center. Alternatively, a conical concavity is used, but depending on the case, it is also possible to use a probe that protrudes in a slightly arc shape or a conical shape with the probe 41 as the center. It is preferable that the tip of the probe 41 is inserted deeply so as not to contact the backing jig 10. The probe advance angle is generally set to about 1 to 5 °. The rotation speed of the tool 40 is generally several hundred to several thousand rotations / minute, and the joining speed is generally several tens to several hundreds mm / minute.

上記ツール40は、定盤軸(X)と横行軸(Y)と昇降軸(Z)の機械3軸からなる公知の摩擦攪拌接合装置に取り付けられて使用される。また、定盤軸(X)と横行軸(Y)と昇降軸(Z)の機械3軸および揺動軸(A)と旋回軸(B)のツール2軸とからなる公知の5軸枠型の摩擦攪拌接合装置等に取り付けられて使用される。また、三つの関節軸と二つの回転軸を具備した公知のロボットアームの先端に搭載されたマシンヘッドに取り付けて使用されることもあるが、これ等に限定されない。   The tool 40 is used by being attached to a known friction stir welding apparatus composed of three machine axes including a surface plate axis (X), a traverse axis (Y), and a lifting / lowering axis (Z). Further, a known 5-axis frame type comprising a machine plate 3 axis of a surface plate axis (X), a transverse axis (Y), an elevating axis (Z), and a tool axis 2 of a swing axis (A) and a swing axis (B). It is used by attaching to a friction stir welding apparatus. Moreover, although it may be attached and used for the machine head mounted in the front-end | tip of the well-known robot arm provided with three joint axes and two rotating shafts, it is not limited to these.

最後に、裏当て治具10の上で接合された被接合材31および32を取り出す。この場合、金属箔21と固体潤滑剤22と支持体23とのサンドイッチ状の三層構造体あるいは金属箔21と固体潤滑剤22との二層構造体の余分な部分が、被接合材の裏面の接合部に一部固着することがあるが、この余分な部分は引っ張って簡単に除去できる。こうして、被接合材31と32との接合体が得られる。なお、34はショルダ部42により形成される接合痕、35はプローブ41による接合部の攪拌領域である。   Finally, the materials to be joined 31 and 32 joined on the backing jig 10 are taken out. In this case, the excess part of the sandwich-like three-layer structure of the metal foil 21, the solid lubricant 22 and the support 23 or the two-layer structure of the metal foil 21 and the solid lubricant 22 is the back surface of the material to be joined. Some of them may stick to the joints, but this extra part can be easily removed by pulling. In this way, a joined body of the materials to be joined 31 and 32 is obtained. Reference numeral 34 denotes a joining mark formed by the shoulder portion 42, and reference numeral 35 denotes a stirring region of the joining portion by the probe 41.

本発明の摩擦攪拌接合方法によれば、突合せ部とその周辺の被接合材と裏当て治具との間に金属箔を挟着するため、被接合材の突合せ部を跨ぐように被接合材と裏当て治具との間に金属箔が挟着されており、金属箔は被接合材の裏面に当接してプローブ先端が裏当て治具に当たらないように、厚さ方向の精度制御に対するバッファーとして働く。
また、固体潤滑剤層は金属箔からプローブの先端が突き抜けても裏当て治具に当たらないように、厚さ方向の精度制御に対するバッファーとして働く。
したがって、高速回転するプローブの先端を裏当て治具により損傷させることなしに、プローブの先端を被接合材の裏面近傍あるいは裏面まで問題なく良好に挿入することができ、その結果、被接合材の接合部が良好に可塑化攪拌される。
According to the friction stir welding method of the present invention, since the metal foil is sandwiched between the butted portion and the surrounding material to be joined and the backing jig, the material to be joined so as to straddle the butted portion of the material to be joined. A metal foil is sandwiched between the back and the backing jig, and the metal foil touches the back surface of the material to be joined so that the probe tip does not hit the backing jig. Acts as a buffer.
In addition, the solid lubricant layer serves as a buffer for accuracy control in the thickness direction so that it does not hit the backing jig even if the tip of the probe penetrates from the metal foil.
Therefore, without damaging the tip of the probe that rotates at high speed with the backing jig, the tip of the probe can be inserted into the vicinity of the back surface or the back surface of the material to be joined without any problem. The joint is well plasticized and stirred.

しかも、上記金属箔と裏当て治具との間に固体潤滑剤が介在することで、高速回転するプローブの先端と裏当て治具とが接触するようなことがあっても、固体潤滑剤によりプローブ先端と裏当て治具との摩擦が著しく軽減され、ツールや裏当て治具の損傷が防止される。したがって、プローブの先端を被接合材の裏面近傍あるいは裏面までぎりぎりの深さまで安心して挿入することが可能となる。   Moreover, even if the tip of the probe that rotates at high speed and the backing jig come into contact with each other due to the presence of the solid lubricant between the metal foil and the backing jig, Friction between the probe tip and the backing jig is significantly reduced, and damage to the tool and backing jig is prevented. Therefore, it is possible to insert the tip of the probe to the vicinity of the back surface of the material to be joined or to the back surface with a minimum depth.

更に、裏当て治具との間に固体潤滑剤が介在することで、摩擦が小さくなり、被接合材の裏面の皮膜状部分も回転され攪拌混合される。   Further, the solid lubricant is interposed between the backing jig and the friction is reduced, and the film-like portion on the back surface of the material to be joined is also rotated and mixed.

このように、本発明の摩擦攪拌接合方法によれば、プローブの先端を被接合材の裏面近傍から固体潤滑剤層に達するまで深く挿入でき、ツールや裏当て材の損傷もなく、強い押当て力の下での加工であっても、被接合材の裏面の皮膜状の部分も回転され攪拌混合される。
したがって、被接合材の突合わせ部は、被接合材の裏面までも十分に攪拌され、その結果、攪拌領域が拡大され、表面側からだけの摩擦攪拌接合であっても、被接合材の接合部にキッシングボンドが発生せず、ルート割れが発生せず、疲労破壊も発生しにくく、且つ低コストで生産性よく被接合材同士を良好に突合わせ接合することができる。
As described above, according to the friction stir welding method of the present invention, the tip of the probe can be inserted deeply from the vicinity of the back surface of the material to be joined until it reaches the solid lubricant layer, and there is no damage to the tool or the backing material and strong pressing. Even in the processing under force, the film-like portion on the back surface of the material to be joined is also rotated and mixed.
Therefore, the butted portion of the material to be joined is sufficiently agitated even to the back surface of the material to be joined, and as a result, the agitation region is expanded, and even when the friction stir welding is performed only from the front side, the joining of the materials to be joined is performed. Kissing bonds do not occur in the parts, root cracks do not occur, fatigue failure does not easily occur, and the materials to be joined can be satisfactorily butt-joined with good productivity at low cost.

以下、本発明の具体的な実施例を挙げる。なお、本発明はこれ等の実施例に限定されるものではない。   Specific examples of the present invention will be given below. The present invention is not limited to these examples.

(スポット摩擦攪拌接合)
図1に示すように、平板状の鋼製(SKD61)の裏当て治具10の表面の中央部の長さ方向に沿って、支持体23として表面平滑なアルミニウム箔(厚さ15μm)を載置した。
(Spot friction stir welding)
As shown in FIG. 1, an aluminum foil (thickness 15 μm) having a smooth surface is mounted as a support 23 along the length direction of the center portion of the surface of a flat steel (SKD61) backing jig 10. I put it.

次いで、上記アルミニウム箔23の上に、二硫化モリブデン(MoS)の粉末22を散布し、さらにその上に上記と同じアルミニウム箔21を載置した。 Next, a powder 22 of molybdenum disulfide (MoS 2 ) was sprayed on the aluminum foil 23, and the same aluminum foil 21 as described above was placed thereon.

次いで、上記アルミニウム箔21の上に、アルミニウム合金(5083−O)からなる二枚の平板状の被接合材31、32(厚さ3mm)の接合面を互いに突き合わせて載置した。この際、被接合材31、32の突合せ部33が、上側のアルミニウム箔21と二硫化モリブデン(MoS)22と下側のアルミニウム箔23で構成された三層構造体の中央に位置するように配置し固定した。 Next, on the aluminum foil 21, two flat joining surfaces 31 and 32 (thickness 3 mm) made of an aluminum alloy (5083-O) were placed in contact with each other. At this time, the butted portion 33 of the materials to be joined 31 and 32 is positioned at the center of the three-layer structure including the upper aluminum foil 21, molybdenum disulfide (MoS 2 ) 22, and the lower aluminum foil 23. Placed and fixed.

その後、定盤軸(X)と横行軸(Y)と昇降軸(Z)の機械3軸からなる摩擦攪拌接合装置に取り付けられている工具鋼からなるツール40のプローブ41を、1000rpmで回転させながら上記突合せ部33の一端に挿入し、200mm/分の送り速度で被接合材31、32の突合せ部33に沿って他端に移動させて摩擦攪拌接合を行い、被接合材31と32との接合体を作製した。   After that, the probe 41 of the tool 40 made of tool steel attached to the friction stir welding apparatus consisting of the three axes of the platen axis (X), the transverse axis (Y), and the elevating axis (Z) is rotated at 1000 rpm. While being inserted into one end of the butt portion 33 and moved to the other end along the butt portion 33 of the materials to be joined 31, 32 at a feed rate of 200 mm / min, friction stir welding is performed. A joined body was prepared.

なお、上記ツール40は、プローブ41の直径が4.0mm、長さが2.9mmであり、ねじが切ってあり、ショルダ部42の直径は12mmで、突合せ部33に沿った被接合材31、32を押圧するためのショルダ面は平面であった。ツール40への負荷は約10,000Nであった。   The tool 40 has a probe 41 with a diameter of 4.0 mm and a length of 2.9 mm, is threaded, a shoulder portion 42 has a diameter of 12 mm, and a material to be joined 31 along the butt portion 33. The shoulder surface for pressing 32 is a flat surface. The load on the tool 40 was about 10,000N.

(突合わせ線に沿った摩擦攪拌接合)
図1に示すように、平板状の鋼製(SKD61)の裏当て治具10の表面の中央部の長さ方向に沿って、支持体23として表面平滑なアルミニウム箔(厚さ15μm)を載置した。
(Friction stir welding along the butt line)
As shown in FIG. 1, an aluminum foil (thickness 15 μm) having a smooth surface is mounted as a support 23 along the length direction of the center portion of the surface of a flat steel (SKD61) backing jig 10. I put it.

次いで、上記アルミニウム箔23の上に、二硫化モリブデン(MoS)の粉末22を散布し、さらにその上に上記と同じアルミニウム箔21を載置した。 Next, a powder 22 of molybdenum disulfide (MoS 2 ) was sprayed on the aluminum foil 23, and the same aluminum foil 21 as described above was placed thereon.

次いで、上記アルミニウム箔21の上に、アルミニウム合金(5083−O)からなる二枚の平板状の被接合材31、32(厚さ3mm)の接合面を互いに突き合わせて載置した。この際、被接合材31、32の突合せ部33が、上側のアルミニウム箔21と二硫化モリブデン(MoS)22と下側のアルミニウム箔23で構成された三層構造体の中央に位置するように配置し固定した。 Next, on the aluminum foil 21, two flat joining surfaces 31 and 32 (thickness 3 mm) made of an aluminum alloy (5083-O) were placed in contact with each other. At this time, the butted portion 33 of the materials to be joined 31 and 32 is positioned at the center of the three-layer structure including the upper aluminum foil 21, molybdenum disulfide (MoS 2 ) 22, and the lower aluminum foil 23. Placed and fixed.

その後、定盤軸(X)と横行軸(Y)と昇降軸(Z)の機械3軸からなる摩擦攪拌接合装置に取り付けられている工具鋼からなるツール40のプローブ41を、1000rpmで回転させながら上記突合せ部33の一端に挿入し、200mm/分の送り速度で被接合材31、32の突合せ部33に沿って他端に移動させて摩擦攪拌接合を行い、被接合材31と32との接合体を作製した。   After that, the probe 41 of the tool 40 made of tool steel attached to the friction stir welding apparatus consisting of the three axes of the platen axis (X), the transverse axis (Y), and the elevating axis (Z) is rotated at 1000 rpm. While being inserted into one end of the butt portion 33 and moved to the other end along the butt portion 33 of the materials to be joined 31, 32 at a feed rate of 200 mm / min, friction stir welding is performed. A joined body was prepared.

なお、上記ツール40は、プローブ41の直径が4.0mm、長さが2.9mmであり、ねじが切ってあり、ショルダ部42の直径は12mmで、突合せ部33に沿った被接合材31、32を押圧するためのショルダ面は平面であった。また、プローブ41の前進角は3°、ツール40への負荷は約10,000Nであった。   The tool 40 has a probe 41 with a diameter of 4.0 mm and a length of 2.9 mm, is threaded, a shoulder portion 42 has a diameter of 12 mm, and a material to be joined 31 along the butt portion 33. The shoulder surface for pressing 32 is a flat surface. The advance angle of the probe 41 was 3 °, and the load on the tool 40 was about 10,000 N.

(比較例1)
(スポット摩擦攪拌接合)
比較のために、アルミニウム箔21と二硫化モリブデン(MoS)の粉末22と支持体のアルミニウム箔23で構成された三層構造体を使用しなかったこと以外は、上記実施例1と同様にして摩擦攪拌接合を行った。
(Comparative Example 1)
(Spot friction stir welding)
For comparison, in the same manner as in Example 1 except that a three-layer structure composed of aluminum foil 21, molybdenum disulfide (MoS 2 ) powder 22 and support aluminum foil 23 was not used. Then, friction stir welding was performed.

(比較例2)
(突合せ線に沿った摩擦攪拌接合)
比較のために、アルミニウム箔21と二硫化モリブデン(MoS)の粉末22と支持体のアルミニウム箔23で構成された三層構造体を使用しなかったこと以外は、上記実施例2と同様にして摩擦攪拌接合を行った。
(Comparative Example 2)
(Friction stir welding along the butt line)
For comparison, in the same manner as in Example 2 except that a three-layer structure composed of aluminum foil 21, molybdenum disulfide (MoS 2 ) powder 22 and support aluminum foil 23 was not used. Then, friction stir welding was performed.

(結果)
実施例1のスポット摩擦攪拌接合部分の裏面を拡大した顕微鏡写真を図2に示す。また、比較例1のスポット摩擦攪拌接合部分の裏面を拡大した顕微鏡写真を図3に示す。
図2(実施例1)の中にわかりやすくするため描き加えた太い破線で示したように、左右の被接合材はスポット摩擦攪拌接合をした部分で渦巻状に攪拌混合されている。
一方、図3(比較例1)では同様にわかりやすくするため描き加えた太い破線のように、左右の被接合材の突合せ線に沿った略直線状のキッシングボンドが観察される。
また、図2(実施例1)、図3(比較例1)の両図とも裏当て材の表面の凹凸が転写されており、強い圧力が付加されていることがわかる。
(result)
The microscope picture which expanded the back surface of the spot friction stir welding part of Example 1 is shown in FIG. Moreover, the microscope picture which expanded the back surface of the spot friction stir welding part of the comparative example 1 is shown in FIG.
As shown by the thick broken lines drawn for easy understanding in FIG. 2 (Example 1), the left and right workpieces are stirred and mixed in a spiral shape at the spot friction stir welded portion.
On the other hand, in FIG. 3 (Comparative Example 1), substantially straight Kissing bonds are observed along the butt lines of the left and right materials to be joined, as shown by the thick broken lines drawn for easy understanding.
Further, in both the drawings of FIG. 2 (Example 1) and FIG. 3 (Comparative Example 1), the surface irregularities of the backing material are transferred, and it can be seen that a strong pressure is applied.

実施例2の突合せ線に沿った摩擦攪拌接合部分の裏面を拡大した顕微鏡写真を図4に示す。また、比較例2の突合せ線に沿った摩擦攪拌接合部分の裏面を拡大した顕微鏡写真を図5に示す。
図4(実施例2)から、裏面まで摩擦攪拌されており、左右の被接合材は渾然一体に摩擦攪拌接合されていることがわかる。
一方、図5(比較例2)では描き加えた太い破線で示すように、左右の被接合材の突合せ線に沿った略直線状のキッシングボンドが観察される。
The microscope picture which expanded the back surface of the friction stir welding part along the butt line of Example 2 is shown in FIG. Moreover, the microscope picture which expanded the back surface of the friction stir welding part along the butt line of the comparative example 2 is shown in FIG.
From FIG. 4 (Example 2), it can be seen that friction stirring is performed up to the back surface, and the left and right materials to be joined are friction stir bonded integrally.
On the other hand, in FIG. 5 (Comparative Example 2), as shown by the thick broken line drawn, a substantially linear kissing bond is observed along the butt line of the left and right bonded materials.

実施例2の突合せ線に沿った摩擦攪拌接合部分の突合せ線と直交方向の断面を拡大した顕微鏡写真を図6に示す。また、比較例2の突合せ線に沿った摩擦攪拌接合部分の突合せ線と直交方向の断面を拡大した顕微鏡写真を図7に示す。
図6(実施例2)では、描き加えた太い破線で示すように裏面まで摩擦攪拌領域が十分形成されていることがわかる。一方、図7(比較例2)では描き加えた太い破線で示すように、摩擦攪拌領域は狭いことがわかる。しかしながら、摩擦攪拌領域は被接合材の裏面まで達しており、摩擦攪拌領域が見かけ上裏面に達していても図5(比較例2)のようなキッシングボンドが形成されることが裏付けられる。
The microscope picture which expanded the cross section orthogonal to the butt line of the friction stir welding part along the butt line of Example 2 is shown in FIG. Moreover, the microscope picture which expanded the cross section orthogonal to the butt line of the friction stir welding part along the butt line of the comparative example 2 is shown in FIG.
In FIG. 6 (Example 2), it can be seen that the friction stir zone is sufficiently formed to the back surface as shown by the thick broken line drawn. On the other hand, as shown by the thick broken line drawn in FIG. However, the friction stir zone reaches the back surface of the material to be joined, and it is confirmed that a kissing bond as shown in FIG. 5 (Comparative Example 2) is formed even if the friction stir zone apparently reaches the back surface.

本発明の摩擦攪拌加工方法の一例を示す一部切欠斜視図である。It is a partially cutaway perspective view showing an example of the friction stir processing method of the present invention. 本発明の実施例1で得られた接合体の裏面の状態を示す顕微鏡写真である。It is a microscope picture which shows the state of the back surface of the conjugate | zygote obtained in Example 1 of this invention. 本発明の比較例1で得られた接合体の裏面の状態を示す顕微鏡写真である。It is a microscope picture which shows the state of the back surface of the conjugate | zygote obtained by the comparative example 1 of this invention. 本発明の実施例2で得られた接合体の裏面の状態を示す顕微鏡写真である。It is a microscope picture which shows the state of the back surface of the conjugate | zygote obtained in Example 2 of this invention. 本発明の比較例2で得られた接合体の裏面の状態を示す顕微鏡写真である。It is a microscope picture which shows the state of the back surface of the conjugate | zygote obtained by the comparative example 2 of this invention. 本発明の実施例2で得られた接合体の断面の状態を示す顕微鏡写真である。It is a microscope picture which shows the state of the cross section of the conjugate | zygote obtained in Example 2 of this invention. 本発明の比較例2で得られた接合体の断面の状態を示す顕微鏡写真である。It is a microscope picture which shows the state of the cross section of the conjugate | zygote obtained by the comparative example 2 of this invention.

符号の説明Explanation of symbols

10 裏当て治具
21 金属箔
22 固体潤滑剤
23 支持体
31 被接合材
32 被接合材
33 被接合材の突合せ部
34 被接合材の接合痕
35 被接合材の接合部
40 ツール
41 ツールのプローブ
42 ツールのショルダ部
DESCRIPTION OF SYMBOLS 10 Backing jig | tool 21 Metal foil 22 Solid lubricant 23 Support body 31 To-be-joined material 32 To-be-joined material 33 Butted part of to-be-joined material 34 Joining mark of to-be-joined material 35 Joined part of to-be-joined material 40 Tool 41 Tool probe 42 Tool shoulder

Claims (8)

被接合材同士を裏当て治具の上に突合わせて載置固定し、この被接合材の突合わせ部に表面側からプローブを挿入し、このプローブを高速回転させながら突合わせ部に沿って相対的に移動させ、その時に発生する摩擦熱により突合わせ部を可塑化させて攪拌することにより、被接合材の突合わせ部を接合する摩擦攪拌接合方法において、
上記突合わせ部を含む被接合材と裏当て治具との間に金属箔を挟着し、かつ該金属箔と裏当て治具との間に固体潤滑剤を介在させることを特徴とする摩擦攪拌接合方法。
The materials to be joined are abutted and fixed on the backing jig, and a probe is inserted into the abutting portion of the materials to be joined from the surface side, and the probe is rotated at a high speed along the abutting portion. In the friction stir welding method for joining the butt portion of the material to be joined, by relatively moving, plasticizing the butt portion by the frictional heat generated at that time and stirring.
Friction characterized in that a metal foil is sandwiched between a material to be joined including the butted portion and a backing jig, and a solid lubricant is interposed between the metal foil and the backing jig. Stir welding method.
裏当て治具と固体潤滑剤との間に支持体を挟着することを特徴とする請求項1に記載の摩擦攪拌接合方法。   2. The friction stir welding method according to claim 1, wherein a support is sandwiched between the backing jig and the solid lubricant. 固体潤滑剤が粉体であることを特徴とする請求項1または2に記載の摩擦攪拌接合方法。   The friction stir welding method according to claim 1 or 2, wherein the solid lubricant is powder. 固体潤滑剤が二硫化モリブデンの粉体または黒鉛の粉体であることを特徴とする請求項1または2に記載の摩擦攪拌接合方法。   The friction stir welding method according to claim 1 or 2, wherein the solid lubricant is a powder of molybdenum disulfide or a powder of graphite. 金属箔が被接合材と同質または類似の材料からなることを特徴とする請求項1乃至4のいずれかに記載の摩擦攪拌接合方法。   The friction stir welding method according to any one of claims 1 to 4, wherein the metal foil is made of the same or similar material as the material to be joined. 支持体が被接合材と同質または類似の材料でからなることを特徴とする請求項2乃至5のいずれかに記載の摩擦攪拌接合方法。   6. The friction stir welding method according to claim 2, wherein the support is made of the same or similar material as the material to be joined. 被接合材がアルミニウムまたはその合金からなり、金属箔がアルミニウム箔またはその合金箔からなり、固体潤滑剤が二硫化モリブデンまたは黒鉛からなることを特徴とする請求項1に記載の摩擦攪拌接合方法。   The friction stir welding method according to claim 1, wherein the material to be joined is made of aluminum or an alloy thereof, the metal foil is made of an aluminum foil or an alloy foil thereof, and the solid lubricant is made of molybdenum disulfide or graphite. 被接合材がアルミニウムまたはその合金からなり、金属箔がアルミニウム箔またはその合金箔からなり、固体潤滑剤が二硫化モリブデンまたは黒鉛からなり、支持体がアルミニウムまたはその合金からなることを特徴とする請求項2に記載の摩擦攪拌接合方法。
The material to be joined is made of aluminum or an alloy thereof, the metal foil is made of an aluminum foil or an alloy foil thereof, the solid lubricant is made of molybdenum disulfide or graphite, and the support is made of aluminum or an alloy thereof. Item 3. The friction stir welding method according to Item 2.
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