JP2007532976A - 有機銀塩を含有する熱現像可能な材料 - Google Patents
有機銀塩を含有する熱現像可能な材料 Download PDFInfo
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- JP2007532976A JP2007532976A JP2007508394A JP2007508394A JP2007532976A JP 2007532976 A JP2007532976 A JP 2007532976A JP 2007508394 A JP2007508394 A JP 2007508394A JP 2007508394 A JP2007508394 A JP 2007508394A JP 2007532976 A JP2007532976 A JP 2007532976A
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- Prior art keywords
- silver
- particles
- silver salt
- rod
- reaction vessel
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- 239000000463 material Substances 0.000 title claims abstract description 266
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 title claims description 78
- -1 silver ions Chemical class 0.000 claims abstract description 176
- 229910052709 silver Inorganic materials 0.000 claims abstract description 160
- 239000004332 silver Substances 0.000 claims abstract description 159
- 239000002245 particle Substances 0.000 claims abstract description 117
- 238000003384 imaging method Methods 0.000 claims abstract description 71
- 150000003378 silver Chemical class 0.000 claims abstract description 34
- 125000001841 imino group Chemical group [H]N=* 0.000 claims abstract description 26
- 239000010410 layer Substances 0.000 claims description 123
- 150000001875 compounds Chemical class 0.000 claims description 66
- 238000000034 method Methods 0.000 claims description 53
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 52
- 239000000203 mixture Substances 0.000 claims description 49
- 238000006243 chemical reaction Methods 0.000 claims description 48
- 239000011230 binding agent Substances 0.000 claims description 45
- 239000006185 dispersion Substances 0.000 claims description 45
- 239000000243 solution Substances 0.000 claims description 44
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 41
- IBWXIFXUDGADCV-UHFFFAOYSA-N 2h-benzotriazole;silver Chemical compound [Ag].C1=CC=C2NN=NC2=C1 IBWXIFXUDGADCV-UHFFFAOYSA-N 0.000 claims description 40
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 40
- 239000003638 chemical reducing agent Substances 0.000 claims description 40
- 108010010803 Gelatin Proteins 0.000 claims description 37
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- 235000011852 gelatine desserts Nutrition 0.000 claims description 37
- 229920000642 polymer Polymers 0.000 claims description 30
- 229910001961 silver nitrate Inorganic materials 0.000 claims description 26
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- 239000011668 ascorbic acid Substances 0.000 claims description 18
- 230000001965 increasing effect Effects 0.000 claims description 18
- 239000012964 benzotriazole Substances 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 16
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims description 15
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 13
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 238000007792 addition Methods 0.000 claims description 9
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 claims description 7
- 239000011241 protective layer Substances 0.000 claims description 7
- ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 claims description 7
- ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 claims description 6
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- 238000001556 precipitation Methods 0.000 abstract description 3
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- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 37
- 239000000975 dye Substances 0.000 description 37
- JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 description 34
- 238000011161 development Methods 0.000 description 24
- 239000000126 substance Substances 0.000 description 22
- 230000003595 spectral effect Effects 0.000 description 20
- JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 17
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- 125000004432 carbon atom Chemical group C* 0.000 description 13
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- 125000003118 aryl group Chemical group 0.000 description 11
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- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 9
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- 238000011160 research Methods 0.000 description 9
- 239000011593 sulfur Substances 0.000 description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 8
- 239000000654 additive Substances 0.000 description 8
- 230000015572 biosynthetic process Effects 0.000 description 8
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 125000002252 acyl group Chemical group 0.000 description 6
- 125000000217 alkyl group Chemical group 0.000 description 6
- 125000004429 atom Chemical group 0.000 description 6
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 6
- 125000000623 heterocyclic group Chemical group 0.000 description 6
- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 6
- 229910052741 iridium Inorganic materials 0.000 description 6
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- 230000003287 optical effect Effects 0.000 description 6
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
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- 125000001424 substituent group Chemical group 0.000 description 6
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- QGKMIGUHVLGJBR-UHFFFAOYSA-M (4z)-1-(3-methylbutyl)-4-[[1-(3-methylbutyl)quinolin-1-ium-4-yl]methylidene]quinoline;iodide Chemical compound [I-].C12=CC=CC=C2N(CCC(C)C)C=CC1=CC1=CC=[N+](CCC(C)C)C2=CC=CC=C12 QGKMIGUHVLGJBR-UHFFFAOYSA-M 0.000 description 4
- NVXLIZQNSVLKPO-UHFFFAOYSA-N Glucosereductone Chemical compound O=CC(O)C=O NVXLIZQNSVLKPO-UHFFFAOYSA-N 0.000 description 4
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- 229910052757 nitrogen Inorganic materials 0.000 description 4
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- WREDNSAXDZCLCP-UHFFFAOYSA-N methanedithioic acid Chemical class SC=S WREDNSAXDZCLCP-UHFFFAOYSA-N 0.000 description 1
- HNQIVZYLYMDVSB-UHFFFAOYSA-N methanesulfonimidic acid Chemical compound CS(N)(=O)=O HNQIVZYLYMDVSB-UHFFFAOYSA-N 0.000 description 1
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- XKJCHHZQLQNZHY-UHFFFAOYSA-N phthalimide Chemical compound C1=CC=C2C(=O)NC(=O)C2=C1 XKJCHHZQLQNZHY-UHFFFAOYSA-N 0.000 description 1
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- 229940017794 potassium ascorbate Drugs 0.000 description 1
- FYRHIOVKTDQVFC-UHFFFAOYSA-M potassium phthalimide Chemical compound [K+].C1=CC=C2C(=O)[N-]C(=O)C2=C1 FYRHIOVKTDQVFC-UHFFFAOYSA-M 0.000 description 1
- CONVKSGEGAVTMB-RXSVEWSESA-M potassium-L-ascorbate Chemical compound [K+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] CONVKSGEGAVTMB-RXSVEWSESA-M 0.000 description 1
- 239000010970 precious metal Substances 0.000 description 1
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- PBMFSQRYOILNGV-UHFFFAOYSA-N pyridazine Chemical compound C1=CC=NN=C1 PBMFSQRYOILNGV-UHFFFAOYSA-N 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- UNLTXKMPCPWQGQ-UHFFFAOYSA-N pyridine;silver Chemical compound [Ag].C1=CC=NC=C1 UNLTXKMPCPWQGQ-UHFFFAOYSA-N 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
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- 229910052703 rhodium Inorganic materials 0.000 description 1
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- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 125000006413 ring segment Chemical group 0.000 description 1
- 238000009666 routine test Methods 0.000 description 1
- WKEDVNSFRWHDNR-UHFFFAOYSA-N salicylanilide Chemical compound OC1=CC=CC=C1C(=O)NC1=CC=CC=C1 WKEDVNSFRWHDNR-UHFFFAOYSA-N 0.000 description 1
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- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
- YPNVIBVEFVRZPJ-UHFFFAOYSA-L silver sulfate Chemical class [Ag+].[Ag+].[O-]S([O-])(=O)=O YPNVIBVEFVRZPJ-UHFFFAOYSA-L 0.000 description 1
- 229910000367 silver sulfate Inorganic materials 0.000 description 1
- KGQZXOXYPGZOCB-UHFFFAOYSA-N silver;2h-triazole Chemical compound [Ag].C=1C=NNN=1 KGQZXOXYPGZOCB-UHFFFAOYSA-N 0.000 description 1
- BYKSCRRKDZGSQR-UHFFFAOYSA-N silver;triazine Chemical compound [Ag].C1=CN=NN=C1 BYKSCRRKDZGSQR-UHFFFAOYSA-N 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 235000010378 sodium ascorbate Nutrition 0.000 description 1
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium ascorbate Substances [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 description 1
- 229960005055 sodium ascorbate Drugs 0.000 description 1
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
- PPASLZSBLFJQEF-RXSVEWSESA-M sodium-L-ascorbate Chemical compound [Na+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RXSVEWSESA-M 0.000 description 1
- 239000002195 soluble material Substances 0.000 description 1
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- 238000001228 spectrum Methods 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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- LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 1
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- 230000001225 therapeutic effect Effects 0.000 description 1
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- VLLMWSRANPNYQX-UHFFFAOYSA-N thiadiazole Chemical compound C1=CSN=N1.C1=CSN=N1 VLLMWSRANPNYQX-UHFFFAOYSA-N 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 125000000101 thioether group Chemical group 0.000 description 1
- 150000003585 thioureas Chemical class 0.000 description 1
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- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/494—Silver salt compositions other than silver halide emulsions; Photothermographic systems ; Thermographic systems using noble metal compounds
- G03C1/498—Photothermographic systems, e.g. dry silver
- G03C1/49809—Organic silver compounds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/0051—Tabular grain emulsions
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/06—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with non-macromolecular additives
- G03C1/34—Fog-inhibitors; Stabilisers; Agents inhibiting latent image regression
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Non-Silver Salt Photosensitive Materials And Non-Silver Salt Photography (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/826,417 US6977139B2 (en) | 2004-04-16 | 2004-04-16 | Thermally developable materials containing organic silver salts with rod-like morphology and method of making and using |
| PCT/US2005/011720 WO2005106581A1 (en) | 2004-04-16 | 2005-04-05 | Thermally developable materials containing organic silver salts |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2007532976A true JP2007532976A (ja) | 2007-11-15 |
| JP2007532976A5 JP2007532976A5 (enExample) | 2008-03-21 |
Family
ID=34965069
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2007508394A Withdrawn JP2007532976A (ja) | 2004-04-16 | 2005-04-05 | 有機銀塩を含有する熱現像可能な材料 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US6977139B2 (enExample) |
| EP (1) | EP1735661B1 (enExample) |
| JP (1) | JP2007532976A (enExample) |
| DE (1) | DE602005002358T2 (enExample) |
| WO (1) | WO2005106581A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4437980B2 (ja) * | 2005-08-05 | 2010-03-24 | 富士フイルム株式会社 | 熱現像感光材料 |
| JP4459149B2 (ja) * | 2005-10-06 | 2010-04-28 | 富士フイルム株式会社 | 含窒素へテロ環化合物の銀塩粒子を含有する熱現像感光材料 |
| US7468241B1 (en) | 2007-09-21 | 2008-12-23 | Carestream Health, Inc. | Processing latitude stabilizers for photothermographic materials |
| US7622247B2 (en) | 2008-01-14 | 2009-11-24 | Carestream Health, Inc. | Protective overcoats for thermally developable materials |
| US20250171639A1 (en) * | 2023-11-27 | 2025-05-29 | Phosio Corporation | Uv-curable aqueous precursor for deposition of low refractive index porous films |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE696925A (enExample) * | 1966-04-12 | 1967-09-18 | ||
| JPS59218443A (ja) | 1983-05-26 | 1984-12-08 | Fuji Photo Film Co Ltd | 画像形成方法 |
| JP2517343B2 (ja) * | 1988-01-26 | 1996-07-24 | 富士写真フイルム株式会社 | 熱現像感光材料 |
| JPH0234370A (ja) | 1988-07-26 | 1990-02-05 | Brother Ind Ltd | プリンタ |
| US6268118B1 (en) | 1998-11-25 | 2001-07-31 | Konica Corporation | Photosensitive emulsion, thermally developable photosensitive material containing the same, image recording method and image forming method employing the same |
| JP2001188313A (ja) * | 1999-10-20 | 2001-07-10 | Fuji Photo Film Co Ltd | 有機酸銀塩の製造方法およびそれを用いた熱現像感光材料 |
| JP2001249428A (ja) | 2000-03-02 | 2001-09-14 | Konica Corp | 熱現像感光材料、画像記録方法及び画像形成法 |
| US6426181B2 (en) | 2000-06-13 | 2002-07-30 | Eastman Kodak Company | Mixtures of organic silver salts in color photothermographic systems |
| US6548236B1 (en) | 2001-11-21 | 2003-04-15 | Eastman Kodak Company | Core/shell silver donors for photothermographic systems comprising an oxidatively less reactive shell |
| US6576414B1 (en) | 2001-11-21 | 2003-06-10 | Eastman Kodak Company | Core/shell silver donors for photothermographic systems comprising an oxidatively more reactive shell |
| US6576410B1 (en) * | 2002-07-11 | 2003-06-10 | Eastman Kodak Company | High-speed thermally developable imaging materials and methods of using same |
-
2004
- 2004-04-16 US US10/826,417 patent/US6977139B2/en not_active Expired - Fee Related
-
2005
- 2005-04-05 JP JP2007508394A patent/JP2007532976A/ja not_active Withdrawn
- 2005-04-05 EP EP05732005A patent/EP1735661B1/en not_active Ceased
- 2005-04-05 WO PCT/US2005/011720 patent/WO2005106581A1/en not_active Ceased
- 2005-04-05 DE DE602005002358T patent/DE602005002358T2/de not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP1735661B1 (en) | 2007-09-05 |
| DE602005002358D1 (de) | 2007-10-18 |
| DE602005002358T2 (de) | 2008-05-29 |
| US6977139B2 (en) | 2005-12-20 |
| US20050233268A1 (en) | 2005-10-20 |
| EP1735661A1 (en) | 2006-12-27 |
| WO2005106581A1 (en) | 2005-11-10 |
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