JP2007208564A - Method of manufacturing piezoelectric vibrator - Google Patents

Method of manufacturing piezoelectric vibrator Download PDF

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JP2007208564A
JP2007208564A JP2006023947A JP2006023947A JP2007208564A JP 2007208564 A JP2007208564 A JP 2007208564A JP 2006023947 A JP2006023947 A JP 2006023947A JP 2006023947 A JP2006023947 A JP 2006023947A JP 2007208564 A JP2007208564 A JP 2007208564A
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piezoelectric vibrator
atmosphere
value
container
manufacturing
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Kengi Goto
健義 後藤
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Kyocera Crystal Device Corp
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Abstract

<P>PROBLEM TO BE SOLVED: To enable a piezoelectric vibrator to be encapsulated in a state in which its CI value is kept low even when the piezoelectric vibrator is made to be a small piece. <P>SOLUTION: When a piezoelectric vibrator manufacturing method encapsulates a piezoelectric vibrator in a hermetically sealed case, the inner pressure of the case is raised up to the pressure higher than normal pressures by 0.3 MPa once using helium gas in a process of filling the case with a hermetically sealed atmosphere, and then the case is hermetically sealed up when its inner pressure is kept at a pressure slightly higher or 0.02 MPa or so higher than normal pressures in a process of returning the inner pressure of the case to normal pressures. Accordingly, the problem can be solved by the piezoelectric vibrator manufacturing method characterized by the fact that a CI value is set lower than the normal pressures. <P>COPYRIGHT: (C)2007,JPO&INPIT

Description

本発明は、圧電振動子のCI値を低く抑えることができる圧電振動子の製造方法に関
する。
The present invention relates to a method of manufacturing a piezoelectric vibrator that can keep the CI value of the piezoelectric vibrator low.

従来から密閉容器の中に水晶板を収容し、はんだ等の金属ろう材の溶融によって蓋を接合することにより、あるいは、最近では密閉容器と蓋との接合に電子ビームやレーザビームを照射し発生する熱で融着して水晶振動子を収納した容器を封止して水晶振動子が製造されている。   Conventionally, a quartz plate is housed in an airtight container, and the lid is joined by melting a soldering material such as solder, or recently, the electron beam or laser beam is applied to the joint between the airtight container and the lid. The crystal unit is manufactured by sealing the container containing the crystal unit by fusing with heat.

またその一方で、圧電振動子の容器の外形寸法が、搭載する電子機器が小型化することで、非常に極小型化、低背化している現状にある。ここで電子機器の一例を挙げると携帯電話機や携帯端末などがあり、これらの電子機器は日々小型化、軽量化している。   On the other hand, the outer dimensions of the container of the piezoelectric vibrator are currently extremely miniaturized and reduced in height due to the downsizing of the electronic equipment to be mounted. Here, examples of electronic devices include mobile phones and mobile terminals, and these electronic devices are becoming smaller and lighter every day.

ここで、密閉容器でガス封入による封止については特許文献1に示すものがある。また、製造フローを図4に示す。なお、同出願人が出願人が提示する特許文献2の製造方法もあるが、この場合には容器内圧を極端に低くして封止するという事例として挙げたものがある。
特開2002−16165号公報 特開2004−153645号公報
Here, there exists a thing shown in patent document 1 about sealing by gas sealing with an airtight container. The manufacturing flow is shown in FIG. In addition, there is a manufacturing method of Patent Document 2 that the applicant presents, but in this case, there is an example in which sealing is performed with an extremely low internal pressure of the container.
JP 2002-16165 A JP 2004-153645 A

従来の技術に記載するように、圧電部品を搭載する電子機器の小型化に対応するために、圧電振動子についても、特に外形寸法や搭載する基板に占める搭載面積を極端に小さく(少なく)するための要望と要求が強く、当然のことながら、その要求を受け入れるには圧電振動子の内部に収納する圧電板そのものの外形寸法を小さくすることをはじめとする、圧電板を収納する容器の外形寸法も小さくせざるを得ない現状にある。   As described in the prior art, in order to cope with the downsizing of electronic devices on which piezoelectric parts are mounted, especially for piezoelectric vibrators, the external dimensions and the mounting area occupied on the mounting board are extremely small (small). There is a strong demand and demand for this, and of course, to accept the request, the outer dimensions of the container that houses the piezoelectric plate, including reducing the outer dimensions of the piezoelectric plate itself that is housed inside the piezoelectric vibrator. The current situation is that the dimensions must be reduced.

ところが、圧電板で例えば短冊形状の水晶素板に電極を配置した水晶振子を例に考えると、水晶振動子の主面の面積が小さくなり、水晶振動子が小片化すると、水晶振動子の振動する振動エネルギーが、水晶振動子の主面と水晶振動子に配置する電極の面積が大きくなるため、水晶振動子の起動に必要とするエネルギーを必要とすることなどで、水晶振動子のCI値(クリスタルインピーダンス)が増加する傾向にあり、小型化の要望を達成するのに反して、水晶振動子の発振が阻害されるという問題を起こしてしまう。   However, considering a crystal pendulum, for example, a piezoelectric plate with electrodes arranged on a strip-shaped crystal base plate, the area of the main surface of the crystal unit becomes small, and when the crystal unit becomes smaller, the vibration of the crystal unit Since the vibration energy to be increased increases the area of the main surface of the crystal unit and the electrode disposed on the crystal unit, the CI value of the crystal unit is required by requiring energy necessary for starting the crystal unit. (Crystal Impedance) tends to increase, and contrary to achieving the demand for miniaturization, the problem arises that the oscillation of the crystal resonator is hindered.

また、その一方では、容器内圧を極端に減圧した例えば特許文献2の例を挙げると、容器外雰囲気からのガスが、常圧より減圧した容器内雰囲気のために、外気ガスを容器内に取り込んでしまうという問題が生じる場合が考えられるという課題が挙げられる。   On the other hand, for example, in Patent Document 2 in which the internal pressure of the container is extremely reduced, the external atmosphere gas is taken into the container because the gas from the external atmosphere of the container is reduced from the normal pressure. The problem that the case where the problem of being produced arises is considered.

上述の課題を解決するために本発明は、密閉容器内に圧電振動子を収容する圧電振動子の製造方法において、該容器を密閉雰囲気にする過程で、一度ヘリウムガスにて常圧より0.3MPaまで高い内圧まで加圧し、その後常圧に戻して行く過程で、常圧よりも少し圧が加わった状態の0.02MPa程度にして密閉封止することにより、常圧よりもCI値を低減することを特徴とする圧電振動子の製造方法である。   In order to solve the above-described problems, the present invention provides a piezoelectric vibrator manufacturing method in which a piezoelectric vibrator is accommodated in a sealed container, and in the process of making the container a sealed atmosphere, helium gas is once discharged from atmospheric pressure to a pressure of 0. In the process of pressurizing to a high internal pressure up to 3 MPa and then returning to the normal pressure, the CI value is reduced from the normal pressure by hermetically sealing to about 0.02 MPa in a state where a little pressure is applied than the normal pressure. This is a method for manufacturing a piezoelectric vibrator.

具体的には、圧電振動子の製造方法の該容器を密閉雰囲気にする過程で、該圧電振動子のCI値を常圧雰囲気で測定する工程と、該圧電振動子をチャンバ雰囲気に入れ、ヘリウムガスを約0.3MPaまで加圧した雰囲気中でCI値を測定する工程と、再度常圧雰囲気に戻してCI値を測定する工程と、ヘリウムガスにより常圧より約0.02MPa高い内圧の該気密容器雰囲気で封止する工程を特徴とする圧電振動子の製造方法であり、加圧雰囲気時にヘリウムガスを充填するものである。   Specifically, in the process of making the container of the method for manufacturing a piezoelectric vibrator into a sealed atmosphere, the CI value of the piezoelectric vibrator is measured in a normal pressure atmosphere, the piezoelectric vibrator is put in a chamber atmosphere, and helium A step of measuring the CI value in an atmosphere in which the gas is pressurized to about 0.3 MPa, a step of measuring the CI value by returning to the atmospheric pressure again, and an internal pressure of about 0.02 MPa higher than the normal pressure by helium gas. This is a method for manufacturing a piezoelectric vibrator characterized by sealing in an airtight container atmosphere, and is filled with helium gas in a pressurized atmosphere.

従来では、ベーキング(熱)処理を行った後に、窒素ガス雰囲気中で封止を行っていたものを、ベーキング処理を行った後に、本願発明の工程を行い、ヘリウムガスを充填して封止を行うものである。
なお、本発明は実験により圧電振動子のCI値の改善を実現したもので、上述の製造方法により、従来に窒素ガスを封入した密閉容器内雰囲気に対し、ヘリウムガス雰囲気の方が、封入ガスの分子直径が小さく軽いため、例えば水晶振動子が振動する初期発振動作において、振動し易くなるものと考えられるものである。
Conventionally, after performing baking (thermal) treatment, sealing was performed in a nitrogen gas atmosphere. After performing baking treatment, the process of the present invention was performed, and helium gas was filled to perform sealing. Is what you do.
In the present invention, the CI value of the piezoelectric vibrator has been improved by experiment. With the above-described manufacturing method, the helium gas atmosphere is more effective in the sealed gas atmosphere than the conventional sealed container atmosphere in which nitrogen gas is sealed. This is considered to be easy to vibrate in the initial oscillation operation in which the crystal resonator vibrates.

以上のように、本発明により圧電振動子のCI値を改善することで、製品歩留まりを大きく改善できるものであるが、特に、従来用いていた真空雰囲気や窒素ガス雰囲気の封止雰囲気に比べて、本発明の製造方法であるヘリウムガスの充填雰囲気により、圧電振動子のCI値を従来の20〜25%改善することができる。   As described above, by improving the CI value of the piezoelectric vibrator according to the present invention, the product yield can be greatly improved. In particular, compared with the conventionally used vacuum atmosphere or nitrogen gas atmosphere sealing atmosphere. The CI value of the piezoelectric vibrator can be improved by 20 to 25% of the conventional value by the helium gas filling atmosphere which is the manufacturing method of the present invention.

以下、添付図面に従ってこの発明の実施例を説明する。なお、各図において同一の符号は同様の対象を示すものとする。図1は、本発明の圧電振動子の製造方法の一部で、本発明の特徴であるベーキング処理後の製造フローを示した図である。チャンバーなどで密閉雰囲気(真空環境)にして、そこに圧電振動子を収納しベーキングを行うが、ベーキング(熱)処理された圧電振動子を真空の雰囲気から、ヘリウム(He)ガスを充填し加圧する。この時の雰囲気圧は、約0.3MPa(メガパスカル)である。   Embodiments of the present invention will be described below with reference to the accompanying drawings. In each figure, the same numerals indicate the same objects. FIG. 1 is a diagram showing a part of the method for manufacturing a piezoelectric vibrator according to the present invention and a manufacturing flow after baking that is a feature of the present invention. A chamber or the like is used to create a sealed atmosphere (vacuum environment), and the piezoelectric vibrator is housed therein and baked. The baked (thermal) treated piezoelectric vibrator is filled with helium (He) gas from a vacuum atmosphere. Press. At this time, the atmospheric pressure is about 0.3 MPa (megapascal).

その後、チャンバー内のヘリウムガスを少しずつ減圧し、約0.02MPaの雰囲気圧にし、ヘリウムガス(0.02MPa圧)の雰囲気で圧電振動子を封止するものである。   Thereafter, the helium gas in the chamber is gradually reduced to an atmospheric pressure of about 0.02 MPa, and the piezoelectric vibrator is sealed in an atmosphere of helium gas (0.02 MPa pressure).

図2は本発明の圧電振動子の製造方法におけるCI値測定を行ったフロー図である。図2の手順を説明すると、圧電振動子のCI値を測定するために、例えばπ回路キャリブレーションにより構成された測定系で、測定ジグに圧電振動子をセットし、常圧雰囲気中でCI値を測定する。その後、圧電振動子の雰囲気をヘリウムガスにし、約0.3MPaに加圧して、この状態で再度CI値を測定する。再度、圧電振動子の周囲雰囲気圧を常圧に戻してCI値を測定するものである。   FIG. 2 is a flowchart showing the CI value measurement in the method for manufacturing a piezoelectric vibrator of the present invention. The procedure of FIG. 2 will be explained. In order to measure the CI value of the piezoelectric vibrator, for example, in a measurement system configured by π circuit calibration, the piezoelectric vibrator is set in a measurement jig, and the CI value is measured in an atmospheric pressure atmosphere. Measure. Thereafter, the atmosphere of the piezoelectric vibrator is changed to helium gas, pressurized to about 0.3 MPa, and the CI value is measured again in this state. Again, the ambient pressure of the piezoelectric vibrator is returned to normal pressure, and the CI value is measured.

発明者は、図2の測定フローにおいて、約0.3MPaから徐々に昇圧雰囲気にする経過で、0.1MPaずつのCI値を測定してCI値の変化を検証したものである。そして、最終的には圧電振動子を収納する密閉容器を僅かに減圧(約0.02MPa)した状態で封止するものである。この時のCI値の変化は図3に示す。   In the measurement flow of FIG. 2, the inventor has verified the change in the CI value by measuring the CI value by 0.1 MPa in the course of gradually increasing the pressure from about 0.3 MPa. Finally, the sealed container that houses the piezoelectric vibrator is sealed in a state where the pressure is slightly reduced (about 0.02 MPa). The change of the CI value at this time is shown in FIG.

図3は発明者が本発明を検証するために実験した圧力値とCI値のグラフである。図3(a)は圧電振動子の容器内をヘリウムガスを充填したときのCI値の変化で、図3(b)は窒素ガスを充填したときのCI値の変化である。また、グラフの縦軸にはCI値を、横軸には圧電振動子の環境雰囲気圧を示して、圧力によるCI値の推移を測定したものである。グラフからも分かるように一度圧電振動子の周囲雰囲気圧を低くし、昇圧することでCI値が変化することが分かる。そして、窒素ガス雰囲気とヘリウムガス雰囲気とのCI値の違いについてもグラフからその良好さを見ることができる。   FIG. 3 is a graph of the pressure value and the CI value that the inventor experimented to verify the present invention. FIG. 3A shows a change in the CI value when the container of the piezoelectric vibrator is filled with helium gas, and FIG. 3B shows a change in the CI value when the gas is filled with nitrogen gas. In addition, the vertical axis of the graph shows the CI value, and the horizontal axis shows the environmental atmospheric pressure of the piezoelectric vibrator, and the transition of the CI value due to the pressure is measured. As can be seen from the graph, the CI value changes when the ambient pressure around the piezoelectric vibrator is once lowered and increased. The goodness of the CI value difference between the nitrogen gas atmosphere and the helium gas atmosphere can also be seen from the graph.

本発明のフロー図である。It is a flowchart of this invention. CI値を測定する1実施例を示すフロー図である。It is a flowchart which shows one Example which measures CI value. 本発明で実験し検証したCI値の変化を示すグラフである。It is a graph which shows the change of CI value which it experimented and verified by this invention. 従来のフロー図である。It is a conventional flowchart.

Claims (3)

密閉容器内に圧電振動子を収容する圧電振動子の製造方法において、
該容器を密閉雰囲気にする過程で、少なくとも常圧より低い減圧雰囲気で該圧電振動子のCI値を測定し、常圧に対して約0.02MPa高い容器内圧の該気密容器雰囲気で封止することを特徴とする圧電振動子の製造方法。
In a method for manufacturing a piezoelectric vibrator that houses a piezoelectric vibrator in a sealed container,
In the process of making the container hermetically sealed, the CI value of the piezoelectric vibrator is measured at least in a reduced-pressure atmosphere lower than normal pressure, and the container is sealed with the air-tight container atmosphere having a container internal pressure about 0.02 MPa higher than the normal pressure. A method of manufacturing a piezoelectric vibrator.
密閉容器内に圧電振動子を収容する圧電振動子の製造方法において、
該容器を密閉雰囲気にする過程で、該圧電振動子のCI値を常圧雰囲気で測定する工程と、該圧電振動子をチャンバ雰囲気に入れ、常圧に対してヘリウムガスを約0.3MPaまで加圧した雰囲気中でCI値を測定する工程と、再度常圧雰囲気に戻してCI値を測定する工程と、常圧に対してヘリウムガスを約0.02MPa高い容器内圧の該気密容器雰囲気で封止する工程を特徴とする圧電振動子の製造方法。
In a method for manufacturing a piezoelectric vibrator that houses a piezoelectric vibrator in a sealed container,
Measuring the CI value of the piezoelectric vibrator in a normal pressure atmosphere in the process of putting the container in a sealed atmosphere; placing the piezoelectric vibrator in a chamber atmosphere; and increasing the helium gas to about 0.3 MPa with respect to the normal pressure A step of measuring the CI value in a pressurized atmosphere, a step of measuring the CI value by returning to the atmospheric pressure again, and an airtight container atmosphere in which the helium gas is about 0.02 MPa higher than the normal pressure in the airtight container atmosphere. A method of manufacturing a piezoelectric vibrator characterized by a sealing step.
請求項1と請求項2に記載のヘリウムガスの注入は、加圧時に充填することを特徴とする圧電振動子の製造方法。
3. The method of manufacturing a piezoelectric vibrator according to claim 1, wherein the helium gas injection according to claim 1 is filled at the time of pressurization.
JP2006023947A 2006-01-31 2006-01-31 Method of manufacturing piezoelectric vibrator Pending JP2007208564A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009100213A (en) * 2007-10-16 2009-05-07 Murata Mfg Co Ltd Method of manufacturing piezoelectric vibrating apparatus
JP2015213231A (en) * 2014-05-02 2015-11-26 セイコーエプソン株式会社 Electronic component, electronic apparatus and movable body

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009100213A (en) * 2007-10-16 2009-05-07 Murata Mfg Co Ltd Method of manufacturing piezoelectric vibrating apparatus
JP2015213231A (en) * 2014-05-02 2015-11-26 セイコーエプソン株式会社 Electronic component, electronic apparatus and movable body

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