JP2005110525A - Method for producing dry powder of chaaga extract and dry powder of chaaga extract - Google Patents
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本発明は、天然キノコであるカバノアナタケに含まれるグルカン多糖類及び抗酸化酵素抽出物の乾燥粉末の製造法ならびにその乾燥粉末に関する。 The present invention relates to a method for producing a dry powder of a glucan polysaccharide and an antioxidant enzyme extract contained in a bamboo shoot, which is a natural mushroom, and the dry powder.
カバノアナタケは、多年生の猿の腰掛型の白色腐朽菌であり、カバノキ類の立ち木の幹に塊状で大型の菌核を形成し、心材を白く腐らせるタバコウロコタケ科、サビアナタケ属の、キノコである。 The birch is a perennial monkey perched white rot fungus, which is a mushroom belonging to the genus Saccharomyces genus, Sabinatake, which forms a large and large nuclei on the trunk of birch standing trees and rots the heartwood white.
このキノコは、白樺など、カバノキ類の生育する北海道からロシアなどの北部地方では、古くから薬効が知られて煎じて飲まれており、ロシアやフィンランドでは、β―Dグルカンなどのグルカン多糖類及び抗酸化酵素が多く含まれることが注目されて、免疫力を高める効果があることが知られていた。 This mushroom has been known for its medicinal properties for a long time in Hokkaido and other northern regions where birch grows, such as birch, and has been drunk in Russia and Finland. In Russia and Finland, glucan polysaccharides such as β-D glucan and It has been noticed that many antioxidant enzymes are contained, and it has been known that it has an effect of enhancing immunity.
しかし、カバノアナタケの菌核は、10〜20cmで、表面は黒く、縦横に亀裂が走り、石炭のように硬く、木の皮の下に背着して平たくひろがっている。このため、木の皮の除去、乾燥後の粉砕、使用量の小分け、とろ火での湯煎、ろ過と、摂取のためには、非常に手間がかかるという問題があった。 However, the mycorrhiza of the birch is 10-20 cm, the surface is black, cracks run vertically and horizontally, it is hard like coal, and it spreads flat under the bark of the tree. For this reason, there is a problem that it takes much time to remove the bark of the tree, pulverize after drying, divide the amount of use, hot water roasting and filtering, and intake.
このため、粉砕小分けしたティーパックや、湯煎液をビン詰めして供給することがなされているが、ティーパックでは湯煎の手間がかかり、ビン詰めでは、エキス成分が不安定であるため、賞味期限が短く、さらに液体であるため重量、輸送手間の問題があった。 For this reason, tea packs that have been pulverized and bottled with hot water are supplied. However, tea packs require time for hot water bathing, and the extract components are unstable when bottled. However, since it is short and liquid, there are problems in weight and labor.
カバノアナタケからの成分抽出物は、そのエキス単独では固形成分が非常に少なく、十分無いため、粉末形成が困難で、安定した物質が得られず長期間の保存性に問題があった。 The extract of birch bamboo has a very small amount of solid components and the extract itself is not sufficient, so that powder formation is difficult, a stable substance cannot be obtained, and there is a problem in long-term storage stability.
このため、カバノアナタケからの成分抽出物の粉末化に当たっては、食品添加物としての賦形物質の中から、エキス内の抗酸化酵素、グルカン多糖類、リグニン様ポリフェノールを安定した乾燥粉末とするための物質が望まれていた。特許文献1にはきのこ類の水性抽出物の粉末化方法及び粉末生成物が開示されている。 For this reason, in pulverizing the component extract from birch bamboo, it is necessary to make the antioxidant enzyme, glucan polysaccharide, and lignin-like polyphenol in the extract into a stable dry powder from the excipients as food additives. The material was desired. Patent Document 1 discloses a method for powdering an aqueous extract of mushrooms and a powder product.
本発明は、前記の問題に鑑みてなされたものでカバノアナタケ湯煎エキス成分を安定させた乾燥粉末の製造方法及びカバノアナタケ乾燥粉末の提供を課題とする。 This invention is made in view of the said problem, and makes it a subject to provide the manufacturing method of the dry powder which stabilized the birch anatake hot-spring extract component, and the birch anatake dry powder.
前記課題を解決するため、本発明のカバノアナタケ抽出物の乾燥粉末製法は、カバノアナタケ菌核の表面の付着物を清掃・洗浄する原体清掃段階と、自然乾燥する原体乾燥段階と、エキス抽出をするために原体を細片にする原体粉砕段階と、粉砕された細片を所定時間抽出用水に浸けておく抽出準備段階と、エキス抽出のために沸騰させる煮沸段階と、沸騰後に所定時間煎じてエキス成分を抽出させる湯煎段階と、所定時間自然に冷却させる冷却段階と、抽出液のろ過段階と、抽出液に賦形物質を所定量配合してエキス成分を賦形物質に包接または吸着させる賦形物質配合段階と、抽出液を濃縮させる濃縮段階と、濃縮された抽出液を乾燥させ抽出物を粉末化する乾燥段階と、乾燥粉末を包装体に所定量ずつ収納する包装段階とからなることを特徴とする。 In order to solve the above-mentioned problems, the dry powder manufacturing method of the birch moth bamboo extract of the present invention comprises an active ingredient cleaning stage for cleaning and washing deposits on the surface of the birch oyster mushroom core, an active ingredient drying stage for natural drying, and an extract extraction. In order to do this, the active ingredient pulverization step for making the active ingredient into pieces, the extraction preparation step for immersing the crushed pieces in extraction water for a predetermined time, the boiling step for boiling for extraction, and the predetermined time after boiling A decoction stage in which the extract component is extracted by decoction, a cooling step in which the extract component is naturally cooled for a predetermined time, a filtration step of the extract, and a predetermined amount of the excipient is included in the extract and the extract component is included in the excipient. A composition step for adsorbing an excipient, a concentration step for concentrating the extract, a drying step for drying the concentrated extract to powder the extract, and a packaging step for storing the dry powder in a predetermined amount in a package. Consist of And it features.
また、前記賦形物質は、多糖類、オリゴ糖類、これらの加水分解物から選択された1種以上の物質であることを特徴とする。 In addition, the excipient is one or more substances selected from polysaccharides, oligosaccharides, and hydrolysates thereof.
また、前記賦形物質には、少なくともデキストリン類が含まれていることを特徴とする。 Further, the excipient is characterized by containing at least dextrins.
また、前記濃縮段階は、減圧濃縮、凍結濃縮、逆浸透圧濃縮のいずれか、又はその組み合わせより行うことを特徴とする。 In addition, the concentration step is performed by any one of vacuum concentration, freeze concentration, reverse osmotic pressure concentration, or a combination thereof.
また、前記乾燥段階は、熱風乾燥、真空乾燥、噴霧乾燥、凍結真空乾燥のいずれか、又はその組み合わせにより行うことを特徴とする。 The drying step may be performed by hot air drying, vacuum drying, spray drying, freeze vacuum drying, or a combination thereof.
また、前記包装段階は、乾燥粉末を微粉末、顆粒状、タブレット状、カプセル状、ブロック状のいずれかに加工してからガス封入包装体に収納することを特徴とする。 In the packaging step, the dry powder is processed into any of fine powder, granule, tablet, capsule, and block, and then stored in the gas-sealed package.
本発明のカバノアナタケ抽出物乾燥粉末は、カバノアナタケ抽出物に、賦形物質として多糖類、オリゴ糖類、これらの加水分解物から選択された1種以上の物質を所定量配合してエキス成分を賦形物質に包接または吸着させて安定させたことを特徴とする。 The dried birch extract of the present invention is formed by adding a predetermined amount of one or more substances selected from polysaccharides, oligosaccharides, and hydrolysates thereof as an excipient to the extract of birch bamboo shoot. It is characterized by being stabilized by inclusion or adsorption to a substance.
また、前記賦形物質として、少なくともデキストリン類を配合し、カバノアナタケ抽出物をデキストリン環状構造に包接させたことを特徴とする。 Moreover, at least dextrins are blended as the excipient, and the birch extract is included in a dextrin ring structure.
本発明によれば、従来カバノアナタケのエキスを摂取したい希望者は、湯煎のような調理手間を掛けていたが、乾燥粉末を常温水、冷水、ぬるま湯などに溶かす作業のみで、いつでも、希望する濃度のカバノアナタケエキスを飲用することができる。すなわち、乾燥粉末化されたことで、飲料又は食用としての利便性が向上する。 According to the present invention, a person who wants to take the extract of birch salmon conventionally has taken cooking effort like hot water roasting, but only by the work of dissolving the dry powder in room temperature water, cold water, lukewarm water, etc. The birch extract can be drunk. That is, the convenience as a drink or an edible thing improves by having been made into dry powder.
また、賦形物質を所定量配合してエキス成分を賦形物質に包接または吸着させることにより、エキスに含有する抗酸化酵素を安定させ、長期間の賞味期限とすることができる。 Moreover, the antioxidant enzyme contained in an extract can be stabilized and it can be set as a long-term expiration date by mix | blending a predetermined amount of excipient | fillers and making an extract component include or adsorb | suck to an excipient | filler.
さらに、賦形物質にデキストリン類を配合し、グルカン多糖類及び抗酸化酵素(例えばスーパーオキシドディスムターゼ)を安定化せしめ、環状トリテルペンやグリニン様ポリフェノールをデキストリン環状構造に包接させることで苦味、刺激官能を緩和させ摂取しやすい状態の粉末とすることが出来る。 In addition, dextrins are added to the excipients, glucan polysaccharides and antioxidant enzymes (eg superoxide dismutase) are stabilized, and cyclic triterpenes and glycin-like polyphenols are included in the dextrin cyclic structure, resulting in bitterness and stimulating function. Can be made into a powder that is easy to ingest.
また、エキス成分の乾燥粉末とすることにより、微粉末状、顆粒状、タブレット状、カプセル状、ブロック状のいずれかに加工して、携帯性と取り扱いの容易性を高めることが出来る。さらに、ガス封入包装体に収納することにより、保存期間を長期とすることが出来る。 Moreover, by making it into the dry powder of an extract component, it can process in any of a fine powder form, a granule form, a tablet form, a capsule form, and a block form, and can improve portability and the ease of handling. Furthermore, the storage period can be extended by storing in a gas-filled package.
以下、図面を参照して本発明の実施の形態を詳細に説明する。 Hereinafter, embodiments of the present invention will be described in detail with reference to the drawings.
図1は、本発明のカバノアナタケ抽出物の乾燥粉末製法を示す流れ図である。 FIG. 1 is a flow chart showing a method for producing a dry powder of the birch extract of the present invention.
S1は、原体清掃段階で、採取されたカバノアナタケには、白樺やダケカンバなど、寄生していた樹木の木の皮(表皮)などが付着しているので、これらの付着物を取り除き、表面(黒色)の汚れを洗浄する。 S1 is the active ingredient cleaning stage, and the collected birch shells are covered with bark (skin) of parasitic trees such as birch and bamboo birch, so remove these deposits and remove the surface ( Clean the black stain.
尚、カバノアナタケは、表面は黒く、縦横に亀裂が走り、石炭のように硬い径10〜20センチの塊状である。内部は黄褐色で、子実体は背着生で樹皮の下に平たく広がり厚さ2〜8mmの全面に茶褐色の管孔が並ぶカバノキ類の寄生菌である。 The birch is black, has cracks running vertically and horizontally, and is a lump with a hard diameter of 10 to 20 cm like coal. The inside is yellowish brown, and the fruiting body is a parasite of birch species that spreads under the bark and spreads flat under the bark and has brown-brown tubes on its entire surface.
次にS2原体乾燥段階で、原体を乾燥させて保存する。この乾燥は、自然乾燥が望ましい。この乾燥段階は、カバノアナタケそのものを採取された際の固体の形のまま行う。 Next, in the S2 bulk drying stage, the bulk is dried and stored. This drying is preferably natural drying. This drying step is performed in the form of a solid when the birch itself is collected.
次にS3原体粉砕段階で、抽出物の乾燥粉末製造に使用する分量に相当する乾燥された原体を取り出して、エキスを抽出し易いように細片に粉砕する。この粉砕には、裁断機、プレス機、回転ミキサーなどの装置を用いる。 Next, in the S3 bulk grinding stage, the dried bulk corresponding to the amount used for the dry powder production of the extract is taken out and ground into small pieces so that the extract can be easily extracted. For this pulverization, an apparatus such as a cutter, a press, or a rotary mixer is used.
次に、S4抽出準備段階で、粉砕されたカバノアナタケの原体の細片を、エキス抽出用の水に浸けて、数時間〜数日おく。この間に、常温で溶出するエキスが抽出される。 Next, in the S4 extraction preparation stage, the ground strip of birch salmon stock is soaked in water for extraction and left for several hours to several days. During this time, the extract eluting at room temperature is extracted.
次に、S5煮沸段階で、S4で、抽出液に浸され、湿潤された細片が入った抽出用水を加熱して沸騰させ、煮沸により溶出するエキスの抽出を行う。 Next, in the S5 boiling stage, in S4, the extraction water immersed in the extract and wetted with the fine pieces is heated and boiled, and the extract eluted by boiling is extracted.
次に、S6湯煎段階で、数時間から1日かけて弱火で煎じて溶出するエキスの抽出を行う。 Next, in the S6 hot water roasting stage, the extract extracted by roasting over low heat over several hours to 1 day is extracted.
次に、S7冷却段階で、火をとめ、抽出液を自然冷却で常温まで冷却する。 Next, in the S7 cooling stage, the fire is turned off and the extract is cooled to room temperature by natural cooling.
次に、S8ろ過段階で、エキスを抽出した菌核の細片と、抽出液とをろ過により分離する。ろ過は、網状の濾過装置で、細片を取り除き、布(繊維)状のろ過装置で、粉状の菌核を取り除くことが望ましい。 Next, in the S8 filtration stage, the sclerotium fragments from which the extract has been extracted and the extract are separated by filtration. For filtration, it is desirable to remove fine particles with a net-like filtration device and to remove powdery fungal nuclei with a cloth (fiber) filtration device.
次に、S9賦形物質配合段階で、抽出液に賦形物質を所定量配合してエキス成分を賦形物質に包接または吸着させる。 Next, in the S9 shaping substance blending stage, a predetermined amount of the shaping substance is blended in the extract, and the extract component is included or adsorbed on the shaping substance.
この賦形物質は、多糖類、オリゴ糖類、これらの加水分解物から選択された1種以上の物質で、例えば、マルトース、サッカロース、乳糖、キシリトール、トレハロース、麦芽糖、果糖、マンニットール、ソルビット、ブドウ糖、1.4グルカン結合、1.6グルカン結合の誘導体、可溶化澱粉、アルファー澱粉、タピオカ澱粉、の一つ或いは複数の組み合わせを用いる。 The excipient is one or more substances selected from polysaccharides, oligosaccharides, and hydrolysates thereof, such as maltose, saccharose, lactose, xylitol, trehalose, maltose, fructose, mannitol, sorbitol, glucose, One or a combination of 1.4 glucan bond, 1.6 glucan bond derivative, solubilized starch, alpha starch, tapioca starch is used.
また、前記賦形物質に、デキストリン類を用いる事によればカバノアナタケ抽出物のグルカン多糖類及び抗酸化酵素(例えばスーパーオキシドディスムターゼ)を安定化せしめ、環状トリテルペンやグリニン様ポリフェノールをデキストリン環状構造に包接させることで苦味、刺激官能を緩和させ摂取しやすい状態の粉末とすることが出来る。 In addition, by using dextrins as the excipient, the glucan polysaccharide and antioxidant enzyme (eg superoxide dismutase) of the birch extract are stabilized, and cyclic triterpenes and glycin-like polyphenols are encapsulated in the dextrin cyclic structure. By touching it, the bitterness and stimulating sensation can be eased and the powder can be easily ingested.
次に、S10濃縮段階で、賦形物質が配合された抽出液を濃縮する。濃縮方法としては、減圧濃縮、凍結濃縮、逆浸透濃縮などの方法の一つ或いはその組み合わせにより行う。 Next, in the S10 concentration step, the extract containing the excipient is concentrated. As the concentration method, one of a method such as vacuum concentration, freeze concentration, reverse osmosis concentration or a combination thereof is used.
次に、S11乾燥段階で、濃縮された抽出液を乾燥させて、抽出液中のエキス及び配合物質を乾燥粉末とする。乾燥方法は、真空凍結乾燥が最も効率的であるが、スプレードライヤー・熱風式乾燥或いは熱風乾燥、真空乾燥、噴霧乾燥、その他の乾燥手段であってもよい。 Next, in the S11 drying stage, the concentrated extract is dried, and the extract and the compounding substance in the extract are made into a dry powder. As the drying method, vacuum freeze-drying is the most efficient, but a spray dryer, hot air drying or hot air drying, vacuum drying, spray drying, or other drying means may be used.
次に、S12包装段階で、乾燥粉末を計量して、包装体に所定量ずつ収納密封する。 Next, in the S12 packaging stage, the dry powder is weighed and stored in a package by a predetermined amount.
包装体の形態は、微粉末のまま、ガス封入包装体に収納密閉してもよいが、顆粒状、タブレット状、カプセル状、ブロック状のいずれかに加工して、携帯性と取り扱いの容易性を高めて、所定量の包装体としてもよい。 The form of the package may be stored and sealed in a gas-filled package as it is in a fine powder form, but it can be processed into any of granular, tablet, capsule, or block shapes for portability and ease of handling. It is good also as a package of a predetermined amount.
図2は、カバノアナタケ抽出物の乾燥粉末の包装の形態を示し、(a)は、顆粒状の乾燥抽出物のシート状包装体、(b)は、ステック状包装体を示す。 FIG. 2 shows a dry powder packaging form of the birch extract, (a) is a granular dry extract sheet-shaped package, and (b) is a stick-shaped package.
このような包装形態とすることにより、携帯することが容易で、免疫強化などの日常習慣として、どこにでも携帯して、飲用することができる。また、微粉末又は顆粒状としておくことで、どこでも入手可能な水で溶かすことができる。 By adopting such a packaging form, it is easy to carry and can be taken anywhere and taken as daily habits such as immune enhancement. Moreover, it can melt | dissolve with water which can be obtained anywhere by setting it as a fine powder or a granular form.
1 カバノアナタケ抽出物顆粒
10 シート状包装体
20 ステック状包装体
1 Bamboo shoot
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Cited By (2)
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KR101240631B1 (en) | 2011-01-31 | 2013-03-11 | 주식회사 해송케이엔에스 | freeze drying method for Sarcodon aspratus |
CN105685754A (en) * | 2016-01-20 | 2016-06-22 | 哈尔滨瑞烨环保科技有限公司 | Inonotuso bliquus pilat compound solid beverage as well as preparation method and application thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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KR101240631B1 (en) | 2011-01-31 | 2013-03-11 | 주식회사 해송케이엔에스 | freeze drying method for Sarcodon aspratus |
CN105685754A (en) * | 2016-01-20 | 2016-06-22 | 哈尔滨瑞烨环保科技有限公司 | Inonotuso bliquus pilat compound solid beverage as well as preparation method and application thereof |
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