JP2005029513A - Breath cool-refreshing preparation and method for producing the same - Google Patents

Abstract

<P>PROBLEM TO BE SOLVED: To provide a cool-refreshing preparation effectively removing offensive odor emitted from a foul mouth or exhaled breath, giving oral cavity cool refreshingness and imparting exhaled breath with favorable fragrance. <P>SOLUTION: The breath cool-refreshing preparation comprises a soft filmy material wrapping a lipophilic liquid cool-refreshing preparation therein. In this preparation, the lipophilic liquid cool-refreshing preparation contains a cool-refreshing agent consisting of menthol and/or a derivative thereof. <P>COPYRIGHT: (C)2005,JPO&NCIPI

Description

  The present invention relates to a breath freshener that effectively removes an unpleasant odor generated from breath and breath and gives a refreshing sensation to the oral cavity and a method for producing the breath refresher.

  In recent years, with the internationalization of dietary content and diversification of lifestyles, there has been a marked change in consumer demand for cosmetics applied to the oral cavity of humans in addition to increased awareness of bad breath and breath odor. It is coming. In particular, unpleasant odors generated from bad breath or breath when you go out or on the go, as well as after eating or drinking foods (such as dumplings or grilled meat) or alcoholic beverages that tend to leave an unpleasant food odor in the oral cavity For the purpose of removal of candy, confectionery such as gums and candy containing a refreshing agent that can be easily applied to the oral cavity is often used.

  However, these gums, candy, etc., are only those that leave the range of confectionery mainly for the purpose of providing taste such as sweetness, and therefore, the refreshing feeling exhibited by the refreshing agent blended there is also In many cases, it is often masked by the sweetness derived from relatively large amounts of sweetening ingredients contained in these confectionery, and in fact, it is difficult to actively expect the effective removal of unpleasant odors generated from bad breath and breath. There is also.

  Various oral compositions mainly composed of a refreshing agent have been proposed for the purpose of solving the above-mentioned problems in confectionery with a dominant sweet component. For example, an oral composition in the form of an easily disintegrating granule formed by granulating menthol together with a fragrance (see, for example, Patent Document 1), a flavor improver comprising alcohol dehydrogenase and peppermint oil (for example, Patent Document) 2) and a composition for oral cavity containing menthol and baking soda (for example, see Patent Document 3) has been proposed.

  However, any of these prior art compositions (formulations) is merely intended to incorporate a refreshing agent into the composition. For this reason, consideration for chemical changes in the composition from the time of manufacture of the composition to application to humans is not always sufficient. For example, many of the cooling components are volatile. Therefore, when a certain period of time is required until these compositions are used, the cooling components deteriorate over time (natural consumption), resulting in In many cases, the reduction of the refreshing effect is unavoidable.

  Therefore, in this technical field, in order to solve the problems of these compositions containing a refreshing agent, research has also been conducted on a configuration in which a relatively high concentration of the refreshing agent is contained. .

  That is, a mouth-to-mouth refreshing agent (see, for example, Patent Document 4) in which a liquid / oil refreshing agent is finely encapsulated and a flavor oil capsule in which flavor oil droplets are coated (to be strictly contained in the refreshing agent) For example, attempts to encapsulate a cooling agent have been proposed so far, such as Patent Document 5).

  Certainly, by adopting such a capsule utilization form, it is possible to effectively maintain a relatively high concentration of the refreshing agent until the capsule is applied to the human oral cavity, and the high concentration of the refreshing agent is applied to the oral cavity. It becomes possible to guide in. In addition, since the refreshing agent is enclosed in the capsule, deterioration of the refreshing agent with time (natural consumption) is also suppressed, and its preservability is also improved.

However, these conventional techniques are devised to keep the refreshing agent without deteriorating, but the unfavorable bitterness derived from the refreshing agent and the fragrance blended therein still remains. However, although there are some differences in the degree of sweetness, since the taste tends to be monotonous, it is the actual situation that only tasteless and attractive items are obtained.
JP 04-124123 A JP 2001-86952 A JP 2002-212041 A JP 52-148635 A JP 07-508164

  An object of the present invention is to provide a breath freshener that not only solves the various problems in the prior art described above, but also satisfies diversifying consumer preferences.

  That is, the gist of the present invention resides in a breath freshener comprising a lipophilic liquid freshener and a soft film material encapsulating the lipophilic liquid freshener.

  According to another aspect of the present invention, (1) a liquid mixture of a lipophilic liquid emulsifier and a hydrophilic sweetener is prepared, (2) the liquid mixture is stirred under heating, and then brought to room temperature. Cooling, (3) adding cooling agents and fragrances to the cooled liquid mixture, then dissolving with stirring, and (4) adding edible oils to the solubilized liquid mixture, then There is provided a method for producing a lipophilic liquid freshener comprising a step of stirring. And the manufacturing method of the breath freshener including the process of encapsulating the lipophilic liquid refresher manufactured in this way with a soft film material is also provided.

  Further, according to another method for producing the breath freshener of the present invention, (a) a liquid mixture of a lipophilic liquid emulsifier and a hydrophilic sweetener is prepared, and (b) the liquid mixture is heated. Stirring, then cooling to room temperature, and (c) adding a cooling agent, fragrance and edible fat to the cooled liquid mixture and then stirring to dissolve it A manufacturing method is provided. And the manufacturing method of a breath freshener including the process of encapsulating the lipophilic liquid freshener manufactured in this way with a soft film material is also provided.

  According to yet another aspect of the invention, there is provided an edible composition comprising a hydrophilic sweetener comprising sucralose and / or acesulfame potassium.

  Moreover, according to the other aspect of this invention, the edible composition containing the refreshing agent which consists of menthol and / or its derivative (s) is also provided.

  According to the present invention, a breath freshener with good storage stability in which deterioration of the freshener is suppressed is realized.

  Further, since the breath refresher of the present invention uses a hydrophilic sweetener, the bitterness derived from the refresher and the fragrance is skillfully masked and alleviated, and at the same time, various tastes including sweetness are imparted. The company has also succeeded in responding to changes in consumer preferences.

  Further, since the soft film material is beautifully colored with transparency, the aesthetics of the breath freshener of the present invention are also emphasized and have an attractive appearance.

  As described above, the breath freshener of the present invention synergistically exhibits many excellent effects in various aspects.

  The present invention is described in detail below.

  According to one aspect of the present invention, there is provided a breath freshener comprising a lipophilic liquid freshener and a soft film material encapsulating the same.

  The term “lipophilic liquid refreshing agent” used in the present specification is a constituent for imparting a refreshing feeling to the human oral cavity or trachea in the breath refreshing agent of the present invention. , Flavors, hydrophilic sweeteners, lipophilic liquid emulsifiers and edible fats and oils.

  As the refreshing agent used in this lipophilic liquid refreshing agent, natural or natural ingredients that release refreshing components commonly used in oral products such as dentifrices, mouth washes, mouth refreshing agents, gums, and candy are used. An artificial cooling agent can be suitably used. For example, naturally occurring refreshing agents include peppermint oil, spearmint oil, mint oil, mastic oil, parsley oil, anise oil, eucalyptus oil, wintergreen oil, cassia oil, lemon oil, orange oil, cardamom oil, coriander Natural essential oils such as oil, mandarin oil, lime oil, lavender oil, laurel oil, camomile oil, caraway oil, bay oil, lemongrass oil, pine needle oil, neroli oil, rose oil, jasmine oil can be used in the present invention. It is. Alternatively, natural essential oils such as peppermint oil, spearmint oil, and mint oil originally containing menthol can be suitably used in the breath freshener of the present invention. In addition, menthol, limonene, menthone, carvone, anethole, methyl salicylate, cinnamic aldehyde, octyl aldehyde, linalool, linalyl acetate, menthyl acetate, pinene, etc. are artificially purified and isolated substances having a cooling effect. These can also be used in the present invention.

  Among these natural or artificial refreshing agents, menthol or a derivative thereof can be suitably used in the breath refreshing agent of the present invention based on the viewpoint that the cooling effect can be efficiently obtained. Such menthol derivatives include 3- (1-menthoxy) propane-1,2-diol, p-menthane-3,8-diol, 6-isopropyl-9-methyl-1,4-dioxaspiro- (4 , 5) -decane-2-methanol, menthyl succinate and its alkaline earth salts, trimethylcyclohexanol, N-ethyl-2-isopropyl-5-methylcyclohexanecarboxamide, 3- (1-menthoxy) -2-methyl- Propane-1,2-diol, menthone glycerol ketal, menthyl lactate, [1'R, 2'S, 5'R] -2- (5'-methyl-2 '-(methylethyl) cyclohexyloxy) ethane-1-ol , [1'R, 2'S, 5'R] -3- (5'-methyl-2 '-(methylethyl) cyclohexyloxy) propan-1-ol, [1'R, 2'S, 5'R] -4 -(5′-methyl-2 ′-(methylethyl) cyclohexyloxy) butan-1-ol and the like can be suitably used in the breath freshener of the present invention.

  In addition, the blending ratio of the refreshing agent in the raw material for producing the oleophilic liquid refreshing agent is usually about 1 to about 20% by weight, preferably about 3 to about 10% by weight, regardless of whether it is naturally derived or synthetic. It is adjusted in the range.

  Moreover, as a fragrance | flavor utilized with a lipophilic liquid refreshing agent, if it is a fragrance | flavor provided for edible, any of a natural fragrance | flavor and an artificial fragrance | flavor can be used. In particular, from the viewpoint of imparting various flavors to the breath freshener that is the final product, blended fragrances, particularly blended fragrances that impart a fruit flavor and / or a cool feeling can be suitably used. Examples of such blended flavors include blended flavors such as peach flavor, apple flavor, strawberry flavor, banana flavor, pineapple flavor, grape flavor, mango flavor, tropical fruit flavor, butter flavor, milk flavor, and fruit mix flavor. Although it can be used, it is not limited to these.

  In addition, the blending ratio of the fragrance in the manufacturing raw material of the lipophilic liquid refreshing agent is usually about 0.1 to about 20% by weight, preferably about 1 to about 15% by weight, regardless of whether it is a natural fragrance or an artificial fragrance. It is adjusted with.

  Next, as the hydrophilic sweetener used in the lipophilic liquid refreshing agent, any sweetener can be used as long as it is soluble in the liquid refreshing agent and has an action of reducing the bitter taste exhibited by the refreshing agent and the fragrance. It can be used. Sweeteners that exhibit such action include, but are not limited to, aspartame, sucralose, acesulfame potassium, stevia, saccharin, thaumatin, and combinations thereof. Among these sweeteners, sucralose having excellent resistance to heat (thermal stability) received during the production process can be advantageously used in the breath freshener of the present invention. In addition to good heat stability, sucralose has the property of exhibiting a preferred sweetness similar to sugar while exhibiting little bitterness. Therefore, paying attention to this point, sucralose can be advantageously used in the breath freshener of the present invention.

  In addition, the blending ratio of the hydrophilic sweetener in the raw material for producing the lipophilic liquid refreshing agent is usually adjusted in the range of about 0.002 to about 0.4% by weight, preferably about 0.01 to about 0.3% by weight.

  As the lipophilic liquid emulsifier used for the lipophilic liquid refreshing agent, any emulsifier that promotes solubilization of the sweetener described below and can be used for food can be used. As the emulsifier satisfying such conditions, propylene glycol fatty acid ester, glycerin fatty acid ester, sucrose fatty acid ester, sorbitan fatty acid ester, lecithin, silicone and combinations thereof can be used in the present invention, but are not limited thereto. Not.

  The blending ratio of the oleophilic liquid emulsifier in the raw material for producing the oleophilic liquid refreshing agent is usually adjusted in the range of about 2.5 to about 90% by weight, preferably about 10 to about 90% by weight.

  Furthermore, as edible fats and oils utilized for a lipophilic liquid refreshing agent, any fats and oils provided for food can be used. However, from the viewpoint of making the final form of the oleophilic refreshing agent liquid (liquid), it is preferable to select fats and oils that are liquid at room temperature. Such oils include soybean oil, rapeseed oil, rice oil, rice bran oil, sunflower oil, sesame oil, wheat germ oil, safflower oil, cottonseed oil, olive oil, safflower oil, peanut oil, corn oil, medium chain fatty acid triglycerides, and These combinations and the like can be used in the present invention, but are not limited thereto.

  In addition, the mixture ratio of the edible fats and oils in the manufacturing raw material of a lipophilic liquid refreshing agent is adjusted about 90 weight% or less normally, Preferably it is the range of about 10 to about 70 weight%.

  On the other hand, the term “soft film material” used in the present specification is a constituent element for forming a film encapsulating an oleophilic liquid refreshing agent in the breath freshener of the present invention, and is water-degradable. Contains polymeric capsule substrate, plasticizer, water, hydrophilic sweetener and colorant.

  As the water-decomposable polymer capsule base material used for the soft film material, any capsule base material generally used as an edible capsule base material can be used. Examples of such capsule base materials include gelatin, agar, xanthan gum, karaya gum, locust bean gum, gum arabic, pullulan, methylcellulose, hydroxyethylcellulose, hydroxypropylmethylcellulose, sodium alginate, and combinations thereof. However, the present invention is not limited to these.

  In addition, the blending ratio of the water-decomposable polymer capsule substrate in the raw material for producing the soft film material is usually adjusted in the range of about 10 to about 80% by weight.

  As the plasticizer used for the soft film material, any plasticizer can be used as long as it promotes plasticization of the capsule base material and can be applied to food and pharmaceutical applications.

  Examples of the plasticizer that satisfies such conditions include glycerin, sorbitol, propylene glycol, and combinations thereof, but are not limited thereto.

  The blending ratio of the plasticizer in the raw material for producing the soft film material is usually adjusted in the range of about 10 to about 50% by weight.

  And as water utilized for manufacture of a soft film material, any water that can be used can be used. For example, in addition to tap water, distilled water, deionized water, alkaline ionized water, etc. Is available. In addition, the amount of water used is appropriately adjusted and added each time a soft film material is produced.

  Next, as the hydrophilic sweetener used for the soft film material, the same hydrophilic sweetener as used above for the lipophilic liquid refreshing agent can be used.

  The blending ratio of the hydrophilic sweetener in the raw material for producing the soft film material is usually adjusted in the range of about 0.01 to about 5% by weight, preferably about 0.5 to about 1.5% by weight.

  The colorant used in the soft film material is an edible colorant for imparting a color to the breath freshener of the present invention, and has a desired color system according to the color imparted to the final product. Food colorants can be selected as appropriate. For example, blue No. 1 is applied for blue color, Red No. 106 for red color, Yellow No. 4 for yellow color, and Green No. Green No. 3 and the like can be suitably used, and it is naturally possible to use these two or more colorants in combination.

  The blending ratio of the colorant in the raw material for producing the soft film material is usually adjusted in the range of about 0.005 to about 0.1% by weight, preferably about 0.01 to about 0.05% by weight.

  Incidentally, at least one of the lipophilic liquid refreshing agent and the soft film material constituting the breath refreshing agent of the present invention, a preservative generally used in the technical field for the purpose of seasoning and solubility adjustment, A sour agent, a bitter agent, a seasoning, an antioxidant and the like can be optionally added. Specifically, as a preservative, benzoic acid (salt), sorbic acid (salt), etc .; as a sour agent, citric acid, malic acid, tartaric acid, fumaric acid, gluconic acid, succinic acid, and other organic acids; as a bitter agent Examples of the seasoning include glutamic acid, glycine, alanine, and arginine; and examples of the antioxidant include vitamin C, vitamin E, and sorbic acid (salt).

  The weight ratio of the oleophilic liquid refreshing agent and the soft film material constituting the breath refreshing agent of the present invention is lyophilic liquid refreshing agent: soft film material = about 19: about 1 to about 1: about 9, preferably , About 19: about 1 to about 4: about 1 in weight ratio.

  In addition, the size (outer diameter) of the breath freshener of the present invention is generally about 0.3 mm to about 20 mm, and preferably about 3 mm to about 10 mm.

  Next, the manufacturing procedure of the breath freshener of the present invention comprising the lipophilic liquid freshener and the soft film material encapsulating it will be described.

  First, a lipophilic liquid refreshing agent is manufactured according to the following series of procedures.

  First, a liquid mixture is prepared by mixing a lipophilic liquid emulsifier and a hydrophilic sweetener. The resulting liquid mixture is then heated for about 10 minutes to about 2 hours, preferably about 1 hour at a temperature of about 70 ° C or higher, preferably about 75 ° C to about 80 ° C. The liquid mixture is then cooled to room temperature. In this step, solubilization of the hydrophilic sweetener is promoted by stirring the liquid mixture of the lipophilic liquid emulsifier and the hydrophilic sweetener under heating. Thereafter, a cooling agent and a fragrance are added to the liquid mixture cooled to room temperature, and then the mixture is stirred for about 10 minutes to about 2 hours, preferably about 30 minutes. ). And edible fats and oils are further added to the liquid mixture in which these additives are dissolved, and stirring is performed. By going through this series of steps, a lipophilic liquid freshener is prepared.

  Alternatively, a liquid mixture that has been cooled to room temperature in the same manner as described above is obtained, and a cooling agent, a fragrance, and edible oils and fats are added to the liquid mixture in a lump, and then this is stirred. Additives (cooling agents, fragrances and edible fats and oils) are dissolved. The lipophilic liquid refreshing agent can also be prepared through this step.

  In any of these production procedures, a lipophilic liquid emulsifier is used, so that the deterioration of fat and oil due to heat observed when using a powdered emulsifier is minimized even after a stirring step under heating. There is an advantage that can be suppressed.

  On the other hand, the soft film material encapsulating the lipophilic liquid refreshing agent is substantially manufactured according to a capsule film manufacturing method known in the art.

  First, a liquid mixture obtained by mixing a plasticizer and water in a water-degradable polymer capsule base material is heated, that is, at a temperature of about 65 ° C. or higher, preferably about 65 ° C. to about 75 ° C., Stirring is carried out for about 30 minutes to about 2 hours, preferably about 1 hour, to obtain a film bulk material. Then, a coloring agent and a hydrophilic sweetener are further added to the original coating material, followed by stirring. A soft film material is manufactured by these series of procedures.

  Then, the lipophilic liquid refreshing agent is encapsulated with a soft film material. As a method for encapsulating an oleophilic liquid refreshing agent with a soft film material, any method known in the art for producing soft capsules (such as a rotary soft encapsulation method or a seamless encapsulation method) can be used. However, it is not limited to these methods. However, from the viewpoint of imparting a beautiful transparency to the breath freshener of the present invention which is the final product, no seam appears on the surface of the breath freshener, that is, the surface of the breath freshener is finished smoothly. The seamless encapsulation method can be suitably used in the present invention.

  The present invention will be described below with reference to examples thereof, but it is needless to say that the present invention should not be construed in a limited manner based on the disclosure of the examples.

  First, a lipophilic liquid emulsifier (about 2 kg) was produced according to the following procedure using the production raw materials for liquid refreshing agents listed in Table 1 below.

はじめに、プロピレングリコール脂肪酸エステル（約450ｇ）とスクラロース（約1.6ｇ）とを混合して液状混合物を調製した。 次に、この液状混合物を、約75℃の温度条件下で、300rpmの回転速度に設定された攪拌機に適用して、１時間かけて攪拌を行った。 その後、攪拌を終えた液状混合物を室温にまで冷却した。

First, a liquid mixture was prepared by mixing propylene glycol fatty acid ester (about 450 g) and sucralose (about 1.6 g). Next, this liquid mixture was applied to a stirrer set at a rotational speed of 300 rpm under a temperature condition of about 75 ° C., and stirred for 1 hour. Thereafter, the liquid mixture after stirring was cooled to room temperature.

  Next, L-menthol crystals (about 75 g), cooling flavor (about 75 g: cooling flavor USJ-2533, manufactured by IF Japan Limited) and peach flavor (about 200 g: white peach) are added to the cooled liquid mixture. Flavor, manufactured by IF Japan Ltd.) and then stirred for about 30 minutes. To the preparation thus obtained, sunflower oil (about 700 g) and medium-chain fatty acid triglyceride (about 500 g) were further added and stirred to obtain an oleophilic liquid refreshing agent.

  On the other hand, the soft film material was manufactured according to the following procedures using the manufacturing raw materials for soft film materials listed in Table 1 above.

  First, glycerin (about 200 g) and sorbitol (about 50 g) and water were added to gelatin (about 1000 g) and dissolved and mixed under temperature conditions of about 65 ° C. to about 75 ° C. To the resulting film base, edible red No. 106 (approx. 0.25 g), sucralose (approx. 7.5 g) and acesulfame potassium (approx. 2.5 g: Thanet, Takeda Kirin Foods Co., Ltd.) were further added and stirred. A soft film material was obtained.

  By applying each of the oleophilic liquid refreshing agent and the soft film material thus prepared to a seamless soft capsule molding machine, it is made of a soft film material encapsulating the oleophilic liquid refreshing agent. A granular breath freshener (particle size: about 5 mm) having a pink color was obtained.

  When this breath freshener was sampled, it melted well in the mouth, and the capsule coating (soft film material) ruptured in the oral cavity, spreading a pleasant peach-flavored cooling sensation throughout the oral cavity. In addition, unpleasant odors in the oral cavity were wiped out, and a refreshing fragrance was included in the sigh after the tasting.

  The breath freshener was manufactured using the manufacturing raw material of Table 2 below.

すなわち、親油性液状清涼剤の製造原料は、ピーチフレーバーに代えて、アップルフレーバー（約200ｇ：アップルフレーバー、アイ・エフ・エフ日本株式会社製）を用いた以外は、実施例１での液状清涼剤用の製造原料と同一とした。 また、軟質膜材用の製造原料は、食用赤色106号に代えて、食用緑色３号（約0.7ｇ）と食用黄色４号（約4.8ｇ）を用いた以外は、実施例１での軟質膜材用の製造原料と同一とした。

That is, the liquid refreshing agent in Example 1 was used except that an apple flavor (about 200 g: Apple flavor, manufactured by IF Japan Limited) was used instead of the peach flavor as a raw material for producing the lipophilic liquid refreshing agent. The same as the manufacturing raw material for the agent. In addition, the soft raw material for the soft film material used in Example 1 except that edible green No. 3 (about 0.7 g) and edible yellow No. 4 (about 4.8 g) were used instead of edible red No. 106. The production raw material for the film material was the same.

  Each of the oleophilic liquid refreshing agent and the soft film material was prepared according to the same procedure as described in Example 1. The thus produced lipophilic liquid refreshing agent and soft film material are applied to a seamless soft capsule molding machine to form a transparent, beautiful green color with a soft film material encapsulating the lipophilic liquid refreshing agent. Of breath freshener (particle size: about 5 mm) was obtained.

  When this breath freshener was sampled, it melted well in the mouth, and the capsule coating (soft film material) burst in the oral cavity, spreading a pleasant apple-flavored cooling sensation throughout the oral cavity. In addition, unpleasant odors in the oral cavity were wiped out, and a refreshing fragrance was included in the sigh after the tasting.

According to the breath freshener of the present invention, it is possible to easily remove unpleasant odor generated from breath odor and exhalation not only after eating and drinking, but also when going out or going out. Moreover, since the breath refreshing agent of the present invention contains a hydrophilic sweetener, the bitterness derived from the refreshing agent and the fragrance is skillfully masked and alleviated, and at the same time, various tastes including sweetness are imparted. It is extremely useful because it can fully respond to changes in consumer tastes, such as success.

Claims (22)

A breath freshener comprising a lipophilic liquid freshener and a soft film material encapsulating the freshener. The breath freshener according to claim 1, wherein the lipophilic liquid freshener comprises a refresher comprising menthol and / or a derivative thereof. The breath freshener according to claim 1 or 2, wherein the lipophilic liquid freshener contains a fragrance. The breath freshener according to any one of claims 1 to 3, wherein the lipophilic liquid freshener contains a hydrophilic sweetener. The breath freshener according to any one of claims 1 to 4, wherein the lipophilic liquid refreshing agent comprises a lipophilic liquid emulsifier. The breath freshener according to any one of claims 1 to 5, wherein the lipophilic liquid freshener contains edible fats and oils. The breath freshener according to any one of claims 3 to 6, wherein the fragrance contains a blended fragrance. The blended flavor is selected from the group consisting of peach flavor, apple flavor, strawberry flavor, banana flavor, pineapple flavor, grape flavor, mango flavor, tropical fruit flavor, butter flavor, milk flavor, fruit mix flavor, and combinations thereof. The breath freshener according to claim 7. The breath freshener according to any one of claims 4 to 8, wherein the hydrophilic sweetener is selected from the group consisting of aspartame, sucralose, acesulfame potassium, stevia, saccharin, thaumatin, and combinations thereof. The mouth according to any one of claims 5 to 9, wherein the lipophilic emulsifier is selected from the group consisting of glycerin fatty acid ester, sucrose fatty acid ester, sorbitan fatty acid ester, propylene glycol fatty acid ester, lecithin, silicone and combinations thereof. Breath freshener. The edible fat is soybean oil, rapeseed oil, rice oil, rice bran oil, sunflower oil, sesame oil, wheat germ oil, safflower oil, cottonseed oil, olive oil, safflower oil, peanut oil, corn oil, medium chain fatty acid triglyceride, and these The breath freshener according to any one of claims 6 to 10, which is selected from the group consisting of combinations. 12. The breath freshener according to claim 1, wherein the soft film material includes a water-decomposable polymer capsule substrate. The capsule base is selected from the group consisting of gelatin, agar, xanthan gum, karaya gum, locust bean gum, gum arabic, pullulan, methylcellulose, hydroxyethylcellulose, hydroxypropylmethylcellulose, sodium alginate, and combinations thereof. The breath freshener described. The breath freshener according to any one of claims 1 to 13, wherein the soft film material includes a plasticizer. 15. The breath freshener according to claim 14, wherein the plasticizer is selected from the group consisting of glycerin, sorbitol, propylene glycol, and combinations thereof. A method for producing a lipophilic liquid refreshing agent comprising the following steps:
(1) Prepare a liquid mixture of lipophilic liquid emulsifier and hydrophilic sweetener,
(2) The liquid mixture is stirred under heating, then cooled to room temperature,
(3) Add cooling agents and perfumes to the cooled liquid mixture, then dissolve with stirring, and
(4) Add edible oils and fats to the solubilized liquid mixture, and then stir.
The manufacturing method of the lipophilic liquid refreshing agent characterized by including a process. A method for producing a lipophilic liquid refreshing agent comprising the following steps:
(a) preparing a liquid mixture of a lipophilic liquid emulsifier and a hydrophilic sweetener;
(b) stirring the liquid mixture under warming, then cooling to room temperature, and
(c) adding a cooling agent, a fragrance and an edible oil to the cooled liquid mixture, and then stirring to dissolve;
The manufacturing method of the lipophilic liquid refreshing agent characterized by including a process. 18. The method for producing a lipophilic liquid refreshing agent according to claim 16, wherein the lipophilic liquid emulsifier is a propylene glycol fatty acid ester. A breath freshener produced by the method according to any one of claims 16 to 18. The breath refreshing agent according to claim 1, wherein the lipophilic liquid refreshing agent is a product produced by the method according to any one of claims 16 to 18. An edible composition comprising a hydrophilic sweetener comprising sucralose and / or acesulfame potassium. An edible composition comprising a refreshing agent comprising menthol and / or a derivative thereof.