JP2004290144A - Extermination material for vermin - Google Patents

Extermination material for vermin Download PDF

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Publication number
JP2004290144A
JP2004290144A JP2003090256A JP2003090256A JP2004290144A JP 2004290144 A JP2004290144 A JP 2004290144A JP 2003090256 A JP2003090256 A JP 2003090256A JP 2003090256 A JP2003090256 A JP 2003090256A JP 2004290144 A JP2004290144 A JP 2004290144A
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JP
Japan
Prior art keywords
pest
present
compound
pest control
controlling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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JP2003090256A
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Japanese (ja)
Inventor
Tomohiro Teramae
朋浩 寺前
Shigeyuki Sasaki
重幸 佐々木
Masato Mizutani
水谷  理人
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
Sumika Life Tech Co Ltd
Original Assignee
Sumitomo Chemical Co Ltd
Sumika Life Tech Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to JP2003090256A priority Critical patent/JP2004290144A/en
Publication of JP2004290144A publication Critical patent/JP2004290144A/en
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a vermin extermination material suitable for the extermination of crawling vermin and containing 2,3,5,6-tetrafluoro-4-methoxymethylbenzyl-2,2-dimethyl-3-(prop-1-enyl)cyclopropanecarboxylate, and provide a vermin extermination method. <P>SOLUTION: The vermin extermination material is an opened base material having a bottom face, a top face and at least one side face and at least the inner surface of the bottom face holds 2,3,5,6-tetrafluoro-4-methoxymethylbenzyl 2,2-dimethyl-3-(prop-1-enyl)cyclopropanecarboxylate. <P>COPYRIGHT: (C)2005,JPO&NCIPI

Description

【0001】
【発明の属する技術分野】
本発明は、匍匐害虫の駆除に適した害虫駆除材、及び害虫駆除方法に関する。
【0002】
【従来の技術】
従来、殺虫活性化合物が処理された害虫駆除材が知られている(例えば、特許文献1〜4参照)。
一方、新しい殺虫活性化合物として、式(1)で示される2,3,5,6−テトラフルオロ−4−メトキシメチルベンジル 2,2−ジメチル−3−(プロプ−1−エニル)シクロプロパンカルボキシレートが提案されている(例えば、特許文献5参照)。

Figure 2004290144
【0003】
【特許文献1】
特表平10−502537号公報
【特許文献2】
特開平10−14465号公報
【特許文献3】
特開平10−23851号公報
【特許文献4】
特開2001−61397号公報
【特許文献5】
特開2000−63329号公報
【0004】
【発明が解決しようとする課題】
しかしながら、前記の害虫駆除材の害虫駆除効果は必ずしも十分ではない場合があった。
本発明は、匍匐害虫の駆除に適した害虫駆除材及び害虫駆除方法を提供することを課題とする。
【0005】
【課題を解決するための手段】
本発明は、底面、上面、及び少なくとも一つの側面を有する開放された基材であって、少なくとも該基材の底面内部に2,3,5,6−テトラフルオロ−4−メトキシメチルベンジル 2,2−ジメチル−3−(プロプ−1−エニル)シクロプロパンカルボキシレート(以下、本化合物と記す。)が保持されてなる害虫駆除材、及び該害虫駆除材を匍匐害虫が生息する場所又は匍匐害虫の通り道に設置する害虫駆除方法を提供する。
【0006】
【発明の実施の形態】
本発明において用いられる本化合物は特許文献5(特開2001−61397号公報)に記載された化合物であり、該公報の記載にしたがって製造することができる。なお、本化合物にはシクロプロパン環及び二重結合に基づく立体異性体が存在するが、任意の活性な異性体又は異性体混合物を使用することができる。
【0007】
本発明の害虫駆除材の本体は、底面、上面、及び少なくとも一つの側面を有する開放された基材である。本発明の害虫駆除材の本体の材質は、例えば紙、木、樹脂(例えばポリエチレン、ポリプロピレン、ポリスチレン等のポリオレフィン、ポリエチレンテレフタレート等のポリエステル)、ガラス、金属(例えば、アルミニウム)及びこれらの複合した材質が挙げられる。中でも、本発明の害虫駆除材本体の成型性、価格等の点から紙又は樹脂が好ましい。
【0008】
本発明の害虫駆除材の形状は、底面、上面、及び少なくとも一つの側面を有し、匍匐害虫が入ることができる様に開放された構造であれば特に制限されない。即ち、ここで開放されたとは底面、上面、及び側面が閉空間を形成するものではなく、匍匐害虫が入ることのできる構造であることを意味する。
そのような形状としては、例えば、板状の材質を2箇所で折り曲げたコの字型の形状が挙げられる。本発明の害虫駆除材の底面と上面とは略平行であることが好ましい。本発明の害虫駆除材の形状が、コの字型の形状である場合には、折り曲げ部の角度は通常30〜150°の範囲である。
【0009】
本発明の害虫駆除材の大きさは、本発明の害虫駆除材により匍匐害虫を駆除しようとする場所に応じて適宜選択できるが、例えば縦1〜20cm、横1〜300cm、高さ0.5〜5cm;好ましくは縦3〜10cm、横3〜100cm、高さ0.5〜5cm程度である。(例えば、図1参照)
【0010】
本発明の害虫駆除材は、本化合物が害虫駆除材本体の底面内部に保持されてなるものである。なお、本化合物は害虫駆除材の底部内面の他、害虫駆除材本体の側面内部、上面内部、及び外部にも保持されていてもよい。
【0011】
本発明の害虫駆除材本体に本化合物を保持させる方法としては、例えば本化合物又はその溶液を害虫駆除材本体に刷毛若しくは噴霧器等で塗布又は滴下等する方法、害虫駆除材本体を本化合物溶液に浸漬処理する方法、さらに害虫駆除材本体の材質が樹脂である場合に本化合物又はその溶液を害虫駆除材本体に練り込む方法が挙げられる。
また、平板状の基材に本化合物を上記の方法で保持させた後に、基材を本発明の害虫駆除材の形状にしてもよい。
【0012】
上記の本化合物の溶液において、用いられる溶剤としては、例えばアセトン、メチルエチルケトン等のケトン類、エタノール、イソプロパノール等のアルコール類、トルエン、キシレン等の芳香族炭化水素類が挙げられる。本化合物を溶解する溶液には塗料も含まれる。該溶液中の本化合物の濃度は通常0.001〜20重量%であり、害虫駆除材本体に該溶液が塗布等の処理をされた後には、通常乾燥される。
本発明の害虫駆除材において、本化合物は匍匐害虫を駆除するための有効量が保持され、本発明の害虫駆除材のうち本化合物が保持されている面1mあたり本化合物が通常1〜20000mg、好ましくは10〜10000mgの割合で保持されている。
【0013】
本発明の害虫駆除材には、本化合物に加えてさらに他の殺虫活性成分が保持されていてもよい。かかる他の殺虫活性成分としては、例えばヒドラメチルノン、ホウ酸の他、ジクロルボス、フェンチオン、フェニトロチオン等の有機リン化合物、プロポキスル、フェノブカルブ等のカーバメート化合物、フェノトリン、トラロメトリン、シフェノトリン、ペルメトリン、エトフェンプロクス、シラフルオフェン等のピレスロイド化合物、ニテンピラム等のネオニコチノイド化合物、フェニルピラゾール系化合物、フェニルピロール系化合物、ジフルベンズロン、ルフェヌロン、メトプレン、ピリプロキシフェン等の昆虫成長制御活性化合物が挙げられる。
【0014】
また、ピペロニルブトキサイド、N−(2−エチルヘキシル)ビシクロ[2,2,1]ヘプタ−5−エン−2,3−ジカルボキシイミド等の効力共力剤を混合して用いることも有効である。
【0015】
本発明の害虫駆除材はアリ、ゴキブリ、チャタテムシ、イガ幼虫、コイガ幼虫、ノミ幼虫などの匍匐害虫を駆除するのに有効であり、特にツヤシリアゲアリ(Crematogaster laboriosa)、アミメアリ(Pristomyrmex pungens)、イエヒメアリ(Monomorium pharaonis)、ヒメアリ(Monomorium intrudens)、オオズアリ(Pheidole nodus)、トビイロシワアリ(Tetramorium caespitum)、ハキリアリ(Atta cephalotis)、アカカミアリ(Solenopsis geminata)等のフタフシアリ亜科、オオハリアリ(Brachyponea chinensis)、アギトアリ(Odontomachus monticola)等のハリアリ亜科、クロヤマアリ(Formica japonica)、クロオオアリ(Camponotus japonicus)、カーペンターアント(Camponotus pennsylvanicus)、トビイロケアリ(Lasius niger)等のヤマアリ亜科、ルリアリ(Iridomyrmex itoi)等のカタアリ亜科、グンタイアリ(Eciton burchelli)等のサスライアリ亜科などのアリを駆除するのに有効である。
【0016】
本発明の害虫駆除材は、匍匐害虫が生息する場所又は匍匐害虫の通り道に、底面外部が設置場所の床面と接触するように載置されて使用され、これにより対象となる害虫を駆除することができる。本発明の害虫駆除材の設置方法としては、例えば匍匐害虫の侵入を防止したい区域の周りを囲むように設置する方法、及び匍匐害虫の侵入を防止したい建物の出入り口に設置する方法が挙げられる。本発明の害虫駆除材の設置個数は、駆除対象害虫、対象場所により適宜決めることができるが、1箇所について通常1〜10個程度設置される。
【0017】
【実施例】
次に、製造例、試験例により本発明をさらに詳しく説明するが、本発明はこれらの例に限定されるものではない。
【0018】
製造例1
2,3,5,6−テトラフルオロ−4−メトキシメチルベンジル 1R−trans−3−(1−プロペニル)−2,2−ジメチルシクロプロパンカルボキシラート(1−プロペニル基の幾何異性体比率はE/Z=約8/1;以下、化合物1と記す。)の2mg/mlアセトン溶液4mlを縦8.5cm×横20cm×厚さ0.4mmのポリプロピレン板の片面に均一に塗布し、風乾した。次いで、長辺側から4cm及び5.5cmの位置に長辺と平行に折り目を入れ、化合物1を塗布した面が内側となり、底面と上面とが略平行になるように折り曲げ(図2参照)、本発明の害虫駆除材を得た。
【0019】
製造例2
本化合物1の2mg/mlアセトン溶液の代わりに本化合物1の20mg/mlアセトン溶液を用いた以外は製造例1と同様にして、本発明の害虫駆除材を得た。
【0020】
製造例3
市販の塗料(ポリエスダイヤDX60;サカタインクス株式会社製)に化合物1を10重量%の割合で混合した。この塗料を、厚さ0.4mmのポリプロピレン板の片面に、化合物1が400mg/mとなるようにバーコーター(RDS03 R.D.S.Webster,N.Y.)で塗布し、風乾した。このポリプロピレン板を縦8.5cm×横20cmの大きさに切断した。次いで、長辺側から4cm及び5.5cmの位置に長辺と平行に折り目を入れ、塗料を塗布した面が内側となり、底面と上面とが略平行になるように折り曲げ(図2参照)、本発明の害虫駆除材を得た。
【0021】
試験例
試験容器(20cm×20cm)内に製造例3で得られた本発明の害虫駆除材とピーナッツバターを置いた濾紙とを、図3に示すように配置した。次いで、図3に示す場所にトビイロシワアリ50頭を放し、所定時間後にピーナッツバター周辺に移動したトビイロシワアリの数とノックダウンしてトビイロシワアリの数とを数えた。一方、製造例3で得られた本発明の害虫駆除材の代わりに、薬剤を処理していない図2の形状の基材を用いて同様に試験を行った。
結果を表1に示す。
【0022】
【表1】
Figure 2004290144
製剤例3で得られた本発明の害虫駆除材を使用した試験では、供試したトビイロシワアリがピーナッツバター周辺に移動することを阻害し、ピーナッツバター周辺に移動したトビイロシワアリは全てノックダウンしていた。
【0023】
【発明の効果】
本発明の害虫駆除材は害虫の侵入路に設置することにより、匍匐害虫、特にアリの侵入を防止、駆除することができる。
【図面の簡単な説明】
【図1】本発明の害虫駆除材の一形態を示す斜視図
【図2】製造例において製造した本発明の害虫駆除材の斜視図
【図3】試験例における害虫駆除試験の方法を示す断面図[0001]
TECHNICAL FIELD OF THE INVENTION
TECHNICAL FIELD The present invention relates to a pest control material and a pest control method suitable for controlling a creeping pest.
[0002]
[Prior art]
BACKGROUND ART Conventionally, pest control materials treated with an insecticidal active compound are known (for example, see Patent Documents 1 to 4).
On the other hand, as a new insecticidal active compound, 2,3,5,6-tetrafluoro-4-methoxymethylbenzyl 2,2-dimethyl-3- (prop-1-enyl) cyclopropanecarboxylate represented by the formula (1) Has been proposed (for example, see Patent Document 5).
Figure 2004290144
[0003]
[Patent Document 1]
Japanese Patent Publication No. 10-502537 [Patent Document 2]
JP-A-10-14465 [Patent Document 3]
JP-A-10-23851 [Patent Document 4]
JP 2001-61397 A [Patent Document 5]
JP 2000-63329 A
[Problems to be solved by the invention]
However, the pest-controlling effect of the above-mentioned pest-controlling material may not always be sufficient.
An object of the present invention is to provide a pest control material and a pest control method suitable for controlling a crawling pest.
[0005]
[Means for Solving the Problems]
The present invention provides an open substrate having a bottom surface, a top surface, and at least one side surface, wherein at least the inside of the substrate has 2,3,5,6-tetrafluoro-4-methoxymethylbenzyl 2,2 Pest control material in which 2-dimethyl-3- (prop-1-enyl) cyclopropanecarboxylate (hereinafter referred to as the present compound) is retained, and a place where the crawling pest inhabits or the crawling pest is used as the pest controlling material Provide a pest control method to be installed on the path of the pest.
[0006]
BEST MODE FOR CARRYING OUT THE INVENTION
The present compound used in the present invention is a compound described in Patent Document 5 (JP-A-2001-61397), and can be produced according to the description in the publication. The present compound has a stereoisomer based on a cyclopropane ring and a double bond, and any active isomer or a mixture of isomers can be used.
[0007]
The body of the pest control material of the present invention is an open substrate having a bottom surface, a top surface, and at least one side surface. The material of the main body of the pest control material of the present invention is, for example, paper, wood, resin (for example, polyolefin such as polyethylene, polypropylene and polystyrene, polyester such as polyethylene terephthalate), glass, metal (for example, aluminum), and a composite material thereof. Is mentioned. Above all, paper or resin is preferred from the viewpoint of moldability, cost, and the like of the pesticidal material of the present invention.
[0008]
The shape of the insect pest-controlling material of the present invention is not particularly limited as long as it has a bottom surface, an upper surface, and at least one side surface and is open so that a creeping pest can enter. That is, being opened here means that the bottom surface, the top surface, and the side surface do not form a closed space, but have a structure in which a creeping pest can enter.
As such a shape, for example, a U-shaped shape in which a plate-shaped material is bent at two places is exemplified. It is preferable that the bottom surface and the top surface of the pesticidal material of the present invention are substantially parallel. When the pest-controlling material of the present invention has a U-shape, the angle of the bent portion is usually in the range of 30 to 150 °.
[0009]
The size of the pesticidal material of the present invention can be appropriately selected depending on the place where the creeping pest is to be controlled by the pesticidal material of the present invention. 55 cm; preferably about 3 to 10 cm in length, 3 to 100 cm in width, and about 0.5 to 5 cm in height. (For example, see FIG. 1)
[0010]
The pesticidal material of the present invention comprises the present compound held inside the bottom surface of the pesticidal material main body. In addition, this compound may be hold | maintained in the inside of the side surface, the inside of the upper surface, and the exterior of the pest control material other than the bottom inner surface of the pest control material.
[0011]
As a method for retaining the present compound in the pesticidal material body of the present invention, for example, a method of applying or dropping the present compound or a solution thereof to the pesticidal material body with a brush or a sprayer, etc., A method of immersion treatment, and a method of kneading the present compound or a solution thereof in the case where the material of the pesticidal material is a resin is used.
Further, after the present compound is held on a flat base material by the above method, the base material may be formed into the shape of the pesticidal material of the present invention.
[0012]
Examples of the solvent used in the solution of the present compound include ketones such as acetone and methyl ethyl ketone, alcohols such as ethanol and isopropanol, and aromatic hydrocarbons such as toluene and xylene. The solution in which the compound is dissolved includes a paint. The concentration of the present compound in the solution is usually 0.001 to 20% by weight, and the solution is usually dried after the solution is applied to the insect-controlling material itself.
In pest control material of the present invention, the compound is retained effective amount for combating creeping pests, the compounds per surface 1 m 2 of the compound is retained within the pest control material of the present invention is usually 1~20000mg , Preferably 10 to 10000 mg.
[0013]
The pesticidal material of the present invention may further contain other pesticidally active ingredients in addition to the present compound. Examples of such other insecticidally active ingredients include, for example, hydramethylnon, boric acid, dichlorvos, phenthione, fenitrothion, and other organic phosphorus compounds, propoxur, carbamate compounds such as fenobcarb, phenothrin, tralomethrin, cyphenothrin, permethrin, etofenprox. And pyrethroid compounds such as silafluofen, neonicotinoid compounds such as nitenpyram, phenylpyrazole compounds, phenylpyrrole compounds, diflubenzuron, lufenuron, methoprene, and pyriproxyfen.
[0014]
It is also effective to use a mixture of potent synergists such as piperonyl butoxide and N- (2-ethylhexyl) bicyclo [2,2,1] hept-5-ene-2,3-dicarboximide. It is.
[0015]
The insect pest-controlling material of the present invention is effective for controlling creeping pests such as ants, cockroaches, chatterbugs, iga larvae, kiga larvae, and flea larvae, and is particularly effective for Crematogaster labriosa, Pristomyrmex pungens, (Monomorium pharaonis), Himeari (Monomorium intrudens), Pheidole noda (Pheidole nodus), Tobiiroshiwaari (Tetramorium caespitum), Hakiriari (Atta cephalotis), Akakamiari (Solenopsis geminata) Futafushiari subfamily such, Oohariari (Brachyponea chinensis), Agitoari (Odontoma hus monticola), black ants (Formica japonica), black ants (Camponotus japonicus), carpenter ant (Camponotus pennsylvanicus); It is effective in controlling ants such as the subfamily Sasarai ant, such as the Echiton burchelli.
[0016]
The pest control material of the present invention is used by being placed on a place where a creeping pest inhabits or on a path of a creeping pest so that the bottom surface is in contact with the floor surface of the installation place, thereby controlling the target pest. be able to. Examples of the method for installing the insect pest-controlling material of the present invention include a method of installing the material around the area where the invasion of the creeping pest is to be prevented, and a method of installing the material at the entrance of the building where the invasion of the creeping pest is to be prevented. The number of the insect-controlling materials of the present invention can be appropriately determined depending on the insect-controlling pest and the target place, but usually 1 to 10 pieces are installed at one place.
[0017]
【Example】
Next, the present invention will be described in more detail with reference to production examples and test examples, but the present invention is not limited to these examples.
[0018]
Production Example 1
2,3,5,6-tetrafluoro-4-methoxymethylbenzyl 1R-trans-3- (1-propenyl) -2,2-dimethylcyclopropanecarboxylate (geometric isomer ratio of 1-propenyl group is E / Z = about 8/1; hereinafter, referred to as compound 1) was uniformly applied to one surface of a polypropylene plate having a length of 8.5 cm × 20 cm × 0.4 mm in thickness and air-dried. Next, a fold is made at 4 cm and 5.5 cm from the long side in parallel with the long side, and the compound 1 is applied so that the surface to which the compound 1 is applied is inside and the bottom surface and the top surface are substantially parallel (see FIG. 2). Thus, a pest control material of the present invention was obtained.
[0019]
Production Example 2
A pest control material of the present invention was obtained in the same manner as in Production Example 1 except that a 20 mg / ml acetone solution of the present compound 1 was used instead of the 2 mg / ml acetone solution of the present compound 1.
[0020]
Production Example 3
Compound 1 was mixed with a commercially available coating material (Polydias DX60; manufactured by Sakata Inx Co., Ltd.) at a ratio of 10% by weight. This coating material was applied on one side of a polypropylene plate having a thickness of 0.4 mm with a bar coater (RDS03 RDS Webster, NY) so that the content of Compound 1 was 400 mg / m 2, and air-dried. . This polypropylene plate was cut into a size of 8.5 cm long × 20 cm wide. Next, folds were made at 4 cm and 5.5 cm from the long side in parallel with the long side, and the surface was coated so that the surface coated with paint was on the inside and the bottom surface and the top surface were substantially parallel (see FIG. 2). The pest control material of the present invention was obtained.
[0021]
Test Example The pest-controlling material of the present invention obtained in Production Example 3 and a filter paper on which peanut butter was obtained were placed in a test container (20 cm × 20 cm) as shown in FIG. Next, 50 termites were released to the place shown in FIG. 3, and after a predetermined time, the number of termites that had moved around the peanut butter was knocked down, and the number of termites was counted. On the other hand, instead of the pest-controlling material of the present invention obtained in Production Example 3, a test was carried out in the same manner using a substrate having the shape shown in FIG.
Table 1 shows the results.
[0022]
[Table 1]
Figure 2004290144
In a test using the insect-controlling material of the present invention obtained in Formulation Example 3, the tested termites stopped moving around the peanut butter, and all the termites moved around the peanut butter were knocked down.
[0023]
【The invention's effect】
The pest-controlling material of the present invention can prevent and control the invasion of creeping pests, especially ants, by being installed in the infestation path of pests.
[Brief description of the drawings]
FIG. 1 is a perspective view showing an embodiment of the pest control material of the present invention. FIG. 2 is a perspective view of the pest control material of the present invention manufactured in the production example. FIG. 3 is a cross-section showing a method of pest control test in a test example. Figure

Claims (5)

底面、上面、及び少なくとも一つの側面を有する開放された基材であって、少なくとも該基材の底面内部に2,3,5,6−テトラフルオロ−4−メトキシメチルベンジル 2,2−ジメチル−3−(プロプ−1−エニル)シクロプロパンカルボキシレートが保持されてなる害虫駆除材。An open substrate having a bottom surface, a top surface, and at least one side surface, wherein at least a bottom surface of the substrate has 2,3,5,6-tetrafluoro-4-methoxymethylbenzyl 2,2-dimethyl- A pest control material containing 3- (prop-1-enyl) cyclopropanecarboxylate. 匍匐害虫を駆除するための請求項1記載の害虫駆除材。The pest-controlling material according to claim 1, for controlling a creeping pest. 匍匐害虫がアリである請求項2記載の害虫駆除材。The pest control material according to claim 2, wherein the creeping pest is an ant. 請求項1〜3いずれか1項記載の害虫駆除材を、匍匐害虫が生息する場所又は匍匐害虫の通り道に設置する害虫駆除方法。A pest control method, wherein the pest control material according to any one of claims 1 to 3 is installed in a place where a crawling pest inhabits or a path of a crawling pest. 匍匐害虫がアリである請求項4記載の害虫駆除方法。The pest control method according to claim 4, wherein the creeping pest is an ant.
JP2003090256A 2003-03-28 2003-03-28 Extermination material for vermin Pending JP2004290144A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008110958A (en) * 2006-06-29 2008-05-15 Sumitomo Chemical Garden Products Inc Noxious insect repellent
JP6200126B1 (en) * 2016-12-27 2017-09-20 一般財団法人カケンテストセンター Insect repellent test apparatus and insect repellent test method
WO2023074396A1 (en) * 2021-10-29 2023-05-04 信越化学工業株式会社 Ant control agent and ant control method

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008110958A (en) * 2006-06-29 2008-05-15 Sumitomo Chemical Garden Products Inc Noxious insect repellent
JP6200126B1 (en) * 2016-12-27 2017-09-20 一般財団法人カケンテストセンター Insect repellent test apparatus and insect repellent test method
WO2018122952A1 (en) * 2016-12-27 2018-07-05 一般財団法人カケンテストセンター Device and method for testing insect repellency
CN110072387A (en) * 2016-12-27 2019-07-30 一般财团法人化检检验机构 Insect prevention experimental rig and insect prevention test method
CN110072387B (en) * 2016-12-27 2022-02-25 一般财团法人化检检验机构 Insect resistance test device and insect resistance test method
US11266130B2 (en) 2016-12-27 2022-03-08 Kaken Test Center Device and method for testing insect repellency
WO2023074396A1 (en) * 2021-10-29 2023-05-04 信越化学工業株式会社 Ant control agent and ant control method

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