JP2003192934A - Natural dye for indigo dyeing using raw leaves of indigo plant as raw material and method for production of the same - Google Patents

Natural dye for indigo dyeing using raw leaves of indigo plant as raw material and method for production of the same

Info

Publication number
JP2003192934A
JP2003192934A JP2001403138A JP2001403138A JP2003192934A JP 2003192934 A JP2003192934 A JP 2003192934A JP 2001403138 A JP2001403138 A JP 2001403138A JP 2001403138 A JP2001403138 A JP 2001403138A JP 2003192934 A JP2003192934 A JP 2003192934A
Authority
JP
Japan
Prior art keywords
leaves
indigo
natural dye
dyeing
raw
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2001403138A
Other languages
Japanese (ja)
Other versions
JP4193166B2 (en
Inventor
Rikuro Funasawa
陸郎 舩澤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to JP2001403138A priority Critical patent/JP4193166B2/en
Publication of JP2003192934A publication Critical patent/JP2003192934A/en
Application granted granted Critical
Publication of JP4193166B2 publication Critical patent/JP4193166B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Landscapes

  • Coloring (AREA)

Abstract

<P>PROBLEM TO BE SOLVED: To produce a natural dye for indigo dyeing by using raw leaves of an indigo plant in a short time and at a low cost without emitting bad odor. <P>SOLUTION: The natural dye useful for indigo dyeing is produced by freezing raw leaves of indigo plant and by thawing the frozen leaves, during its melting, indican contained in the leaves changes to indoxyl owing to action of an enzyme and water contained in the leaves, further it reacts with oxygen in air then forms indigo, therefore it is prepared after drying the leaves by pulverizing them into a powder. <P>COPYRIGHT: (C)2003,JPO

Description

【発明の詳細な説明】 【0001】 【発明の属する技術分野】本発明は,含藍植物である蓼
藍や琉球藍等の生葉を冷凍して解凍した後に乾燥し,粉
末にして得る藍染めの天然染料の製造方法である。 【0002】 【従来の技術】含藍植物である蓼藍等は,収穫した葉を
乾燥させ,特殊な寝床といわれる施設で,水を与えて寝
かせ,加水と切り返しを繰り返して発酵させ,スクモと
いうものに加工して染料を製造するが,この方法は大が
かりな施設設備と高度な技術及び約100日間という期
間を要し,従って,その染料は高価格なものとなってい
る。また,発酵という工程を経るため,独特の臭気を発
し,使用者に嫌われることがある。 【0003】 【本発明が解決しようとする課題】従来の技術で製造さ
れている,スクモという藍染め染料は,大がかりな施設
設備と高度な技術及び約100日間という期間を要し,
従って,その染料は高価格のものとなっている。また,
発酵という工程を経るため,独特の臭気を発し,使用者
に嫌われることがある。そのため,含藍植物の生葉を用
いて,短期間,低コストで,かつ,臭気を発することの
ない藍染めの天然染料を製造することとした。 【0004】 【課題を解決するための手段】以上の課題を解決するた
め,収穫した含藍植物から,葉のみを採取し,新鮮なう
ちに冷凍庫等で完全に凍結させる。凍結した該葉を解凍
させると,該葉は凍結によって組織が損傷を受けている
ため,融解する過程において,含有されるインジカンが
該葉中の酵素と水分の作用で加水分解されてインドキシ
ルとなり,更にインドキシルは空気中の酸素と化合して
インジゴが生成される。この工程においては,該葉を平
面に広げ,全体が空気に触れるよう攪拌を繰り返して酸
化を促す作業を行うのが好ましい。このようにしてイン
ジゴが生成された該葉を乾燥させた後に任意の方法で粉
末にすると藍染めの天然染料が完成する。 【0005】 【発明の実施の形態】収穫した含藍植物から,葉のみを
採取し,新鮮なうちに冷凍庫等で完全に凍結させる。凍
結した該葉を解凍させると,該葉は凍結によって組織が
損傷を受けているため,融解する過程において,含有さ
れるインジカンが該葉中の酵素と水分の作用で加水分解
されてインドキシルとなり,更にインドキシルは空気中
の酸素と化合してインジゴが生成される。この工程にお
いては,該葉を平面に広げ,全体が空気に触れるよう攪
拌を繰り返して酸化を促す作業を行うのが好ましい。こ
のようにしてインジゴが生成された該葉を乾燥させた後
に任意の方法で粉末にすると藍染めの天然染料が完成す
る。葉の採取から染料の完成までに要する期間は5日程
度であり,完成した染料は,乾燥藍葉の仄かな香りを発
する。該染料を用いた藍染め方法の例を示せば。1リ
ットル当たり2.5グラムの苛性ソーダを溶解させた水
40リットルに該染料約2.5キログラムを入れて攪拌
した後,ハイドロサルファイトナトリウム約200グラ
ムを投入して攪拌し,1時間以上,好ましくは数時間静
置すると,インジゴがロイコインジゴに還元されて染液
が完成する。なお,苛性ソーダに代えて約8倍量のソー
ダ灰を用いてもよい。水で濡らした布を均一に絞った
ものを染液中に入れ,約3分後に取り出し,均一に絞っ
て空気中に晒すと,ロイコインジゴが空気中の酸素と化
合してインジゴとなり青色に発色する。前記を繰り
返し,好みの色になったら,水洗い,乾燥する。なお,
染液中の染料量を増やすことによって,更に濃い色を得
ることができる。 【0006】 【実施形態の効果】この実施形態によれば,含藍植物の
生葉を用いて,短期間,低コストで,臭気を発すること
のない藍染めの天然染料を製造することができる。 【0007】 【発明の効果】以上説明したように,この発明によれ
ば,含藍植物の生葉を用いて,短期間,低コストで,臭
気を発することのない藍染めの天然染料を製造すること
ができる。
Description: BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an indigo dye obtained by freezing and thawing fresh leaves of indigo plants such as Tateai and Ryukyu indigo, followed by drying and powdering. Is a method for producing a natural dye. 2. Description of the Related Art Indigo plants, such as the indigo plant, are used to dry the harvested leaves, give them water, lay them down, ferment them repeatedly by adding water and turning them back, and call them Sukumo. This process requires extensive facility equipment, advanced technology and a period of about 100 days, and thus the dye is expensive. In addition, since it goes through a fermentation process, it emits a unique odor and may be disliked by users. [0003] The indigo dye called Sukumo, which is manufactured by conventional techniques, requires extensive facility equipment, advanced technology, and a period of about 100 days.
Therefore, the dye is expensive. Also,
Due to the fermentation process, it emits a unique odor and may be hated by users. For this reason, we decided to use natural leaves of indigo plants to produce natural dyes of indigo dyeing at low cost for a short period of time and without odor. [0004] In order to solve the above-mentioned problems, only leaves are collected from the harvested indigo plants and completely frozen in a freezer or the like while fresh. When the frozen leaves are thawed, the indicans contained in the leaves are hydrolyzed by the action of enzymes and water in the leaves to indoxyl during the thawing process because the leaves are damaged by freezing. Indoxyl combines with oxygen in the air to form indigo. In this step, it is preferable to spread the leaves in a plane and repeat the stirring so that the whole is in contact with air to promote the oxidation. The leaves, on which the indigo has been formed in this way, are dried and then powdered by any method to complete the indigo-dyed natural dye. [0005] From the harvested indigo plants, only leaves are collected and completely frozen in a freezer or the like while fresh. When the frozen leaves are thawed, the indicans contained in the leaves are hydrolyzed by the action of enzymes and water in the leaves to indoxyl during the thawing process because the leaves are damaged by freezing. Indoxyl combines with oxygen in the air to form indigo. In this step, it is preferable to spread the leaves in a plane and repeat the stirring so that the whole is in contact with air to promote the oxidation. The leaves, on which the indigo has been formed in this way, are dried and then powdered by any method to complete the indigo-dyed natural dye. The time required from the collection of the leaves to the completion of the dye is about 5 days, and the completed dye emits a faint scent of dried indigo leaves. What is an example of the indigo dyeing method using this dye? About 2.5 kg of the dye is added to 40 liters of water in which 2.5 g of caustic soda is dissolved per liter, and the mixture is stirred. Then, about 200 g of sodium hydrosulfite is added and stirred. After standing for several hours, the indigo is reduced to Leucoin digo to complete the dyeing liquor. Instead of caustic soda, about 8 times the amount of soda ash may be used. A cloth squeezed uniformly with water is squeezed into a dye solution, taken out after about 3 minutes, squeezed evenly, and exposed to air. Leucoin digo combines with oxygen in the air to become indigo and develops a blue color. I do. Repeat the above, when the desired color is obtained, wash with water and dry. In addition,
A darker color can be obtained by increasing the amount of dye in the liquor. According to this embodiment, an indigo-dyeing natural dye which does not emit odor can be produced in a short period of time at low cost using fresh leaves of an indigo plant. As described above, according to the present invention, a natural dye of indigo dyeing which does not emit odor is produced in a short period of time and at low cost using fresh leaves of an indigo plant. be able to.

Claims (1)

【特許請求の範囲】 【請求項1】 含藍植物の生葉を冷凍して解凍した後に
乾燥し,粉末にして得る藍染めの天然染料の製造方法
Claims: 1. A method for producing an indigo-dyeing natural dye obtained by freezing and thawing fresh leaves of an indigo plant and then drying and powdering the leaves.
JP2001403138A 2001-12-26 2001-12-26 Natural dye of indigo dyeing made from raw leaves of indigo plant and production method thereof Expired - Fee Related JP4193166B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2001403138A JP4193166B2 (en) 2001-12-26 2001-12-26 Natural dye of indigo dyeing made from raw leaves of indigo plant and production method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2001403138A JP4193166B2 (en) 2001-12-26 2001-12-26 Natural dye of indigo dyeing made from raw leaves of indigo plant and production method thereof

Publications (2)

Publication Number Publication Date
JP2003192934A true JP2003192934A (en) 2003-07-09
JP4193166B2 JP4193166B2 (en) 2008-12-10

Family

ID=27605884

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2001403138A Expired - Fee Related JP4193166B2 (en) 2001-12-26 2001-12-26 Natural dye of indigo dyeing made from raw leaves of indigo plant and production method thereof

Country Status (1)

Country Link
JP (1) JP4193166B2 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005220328A (en) * 2004-02-09 2005-08-18 Ai:Kk Method for producing additive containing indigo, indirubin or isatin
JP2005336632A (en) * 2004-05-25 2005-12-08 Kagoshima Prefecture Indigo-dyeing method from indigo plant
JP2008240162A (en) * 2007-03-23 2008-10-09 Hirosaki Univ Indigo dyeing method
KR100983379B1 (en) * 2008-04-10 2010-09-20 전남대학교산학협력단 The indigo leaf powder dye which it prepares from the fresh leaves of Polygonum tintorium and the manufacturing and dyeing method
CN102127309A (en) * 2010-12-10 2011-07-20 盐城纺织职业技术学院 Preparation method and application of natural plant dye solution of Phytolacca acinosa berries
JP2016113737A (en) * 2014-12-11 2016-06-23 有限会社岩崎呉服店 Indigo blue interior using indigo leaf

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005220328A (en) * 2004-02-09 2005-08-18 Ai:Kk Method for producing additive containing indigo, indirubin or isatin
JP2005336632A (en) * 2004-05-25 2005-12-08 Kagoshima Prefecture Indigo-dyeing method from indigo plant
JP4660640B2 (en) * 2004-05-25 2011-03-30 鹿児島県 Indigo dyeing from indigo plants
JP2008240162A (en) * 2007-03-23 2008-10-09 Hirosaki Univ Indigo dyeing method
KR100983379B1 (en) * 2008-04-10 2010-09-20 전남대학교산학협력단 The indigo leaf powder dye which it prepares from the fresh leaves of Polygonum tintorium and the manufacturing and dyeing method
CN102127309A (en) * 2010-12-10 2011-07-20 盐城纺织职业技术学院 Preparation method and application of natural plant dye solution of Phytolacca acinosa berries
JP2016113737A (en) * 2014-12-11 2016-06-23 有限会社岩崎呉服店 Indigo blue interior using indigo leaf

Also Published As

Publication number Publication date
JP4193166B2 (en) 2008-12-10

Similar Documents

Publication Publication Date Title
KR101030954B1 (en) Natural dyeing method of fiber using indigoplant
CN103027276A (en) Method for producing low-salt fast fermented fish sauce
CN105454658A (en) Preparation method of feather fermentation protein feed
CN107266203A (en) It is a kind of for vegetable cultivation matrix of balcony and preparation method thereof
JP2003192934A (en) Natural dye for indigo dyeing using raw leaves of indigo plant as raw material and method for production of the same
KR100264675B1 (en) Preparation method of natural indigo from polygoum tinctorlum
CN105601361A (en) Method for producing organic fertilizer from chicken manure, straws and traditional Chinese medicine residues
CN108840775A (en) A kind of organic agriculture charcoal base manure material and preparation method thereof
KR101101401B1 (en) Jjokpul use of natural indigo powder manufacturing method
CA1276121C (en) Method of dyeing cotton and other substrates with a microorganism biomass containing indigo
CN105859352A (en) Bitter gourd seedling medium and preparation method thereof
CN105585362A (en) Special biogas slurry organic liquid fertilizer for rice and production method
CN110511100A (en) A kind of fermentation bacterial manure and preparation method thereof for soil hardening reparation
AU2021101031A4 (en) Biological fertilizer for increasing rice yield and preparation method thereof
JPH10237341A (en) Continuous indigo dyeing of textile material using natural indigo dye
JP2008240162A (en) Indigo dyeing method
CN110257305A (en) The breeding method of the Shewanella of high yield alkali protein
US3950221A (en) Process for improving the quality of microbial rennet
CN106063438A (en) A kind of paddy rice planting method of green volume increase
CN108314577A (en) A kind of tree peony compost and preparation method thereof
CN114634961B (en) Preparation method of oyster oligopeptide powder with multiple bioactivity functions
JPH08308378A (en) Cultivation of mushroom
WO2019056200A1 (en) Method for dyeing cloth
CN108651125A (en) A kind of raspberry process for breeding and culturing
CN109220706A (en) A kind of plant culture produced using the dregs of a decoction

Legal Events

Date Code Title Description
A621 Written request for application examination

Effective date: 20041221

Free format text: JAPANESE INTERMEDIATE CODE: A621

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20080513

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20080527

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Effective date: 20080909

Free format text: JAPANESE INTERMEDIATE CODE: A01

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20080911

R150 Certificate of patent (=grant) or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (prs date is renewal date of database)

Year of fee payment: 3

Free format text: PAYMENT UNTIL: 20111003

LAPS Cancellation because of no payment of annual fees