JP2003139753A5 - - Google Patents
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- Publication number
- JP2003139753A5 JP2003139753A5 JP2001338441A JP2001338441A JP2003139753A5 JP 2003139753 A5 JP2003139753 A5 JP 2003139753A5 JP 2001338441 A JP2001338441 A JP 2001338441A JP 2001338441 A JP2001338441 A JP 2001338441A JP 2003139753 A5 JP2003139753 A5 JP 2003139753A5
- Authority
- JP
- Japan
- Prior art keywords
- organic solvent
- bile acids
- water
- composition
- simultaneous analysis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000003613 bile acid Substances 0.000 claims 9
- 239000000203 mixture Substances 0.000 claims 6
- 238000004458 analytical method Methods 0.000 claims 5
- 239000003960 organic solvent Substances 0.000 claims 5
- 239000007864 aqueous solution Substances 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 4
- HSINOMROUCMIEA-FGVHQWLLSA-N (2s,4r)-4-[(3r,5s,6r,7r,8s,9s,10s,13r,14s,17r)-6-ethyl-3,7-dihydroxy-10,13-dimethyl-2,3,4,5,6,7,8,9,11,12,14,15,16,17-tetradecahydro-1h-cyclopenta[a]phenanthren-17-yl]-2-methylpentanoic acid Chemical compound C([C@@]12C)C[C@@H](O)C[C@H]1[C@@H](CC)[C@@H](O)[C@@H]1[C@@H]2CC[C@]2(C)[C@@H]([C@H](C)C[C@H](C)C(O)=O)CC[C@H]21 HSINOMROUCMIEA-FGVHQWLLSA-N 0.000 claims 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical group CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- 238000010828 elution Methods 0.000 claims 2
- 238000000589 high-performance liquid chromatography-mass spectrometry Methods 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 238000000034 method Methods 0.000 claims 2
- 239000000243 solution Substances 0.000 claims 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 1
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 claims 1
- 239000005695 Ammonium acetate Substances 0.000 claims 1
- 229940043376 ammonium acetate Drugs 0.000 claims 1
- 235000019257 ammonium acetate Nutrition 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001338441A JP2003139753A (ja) | 2001-11-02 | 2001-11-02 | 胆汁酸１８成分の一斉分析法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001338441A JP2003139753A (ja) | 2001-11-02 | 2001-11-02 | 胆汁酸１８成分の一斉分析法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2003139753A JP2003139753A (ja) | 2003-05-14 |
| JP2003139753A5 true JP2003139753A5 (https=) | 2005-07-07 |
Family
ID=19152935
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2001338441A Pending JP2003139753A (ja) | 2001-11-02 | 2001-11-02 | 胆汁酸１８成分の一斉分析法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2003139753A (https=) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4966780B2 (ja) * | 2007-07-30 | 2012-07-04 | 株式会社日立ハイテクノロジーズ | 液体クロマトグラフ／質量分析計を用いた分析方法 |
| JP5270684B2 (ja) * | 2007-11-02 | 2013-08-21 | メタボロン、インコーポレイテッド | 脂肪肝疾患用のバイオマーカー及びその使用方法 |
| JP5624709B2 (ja) * | 2008-03-13 | 2014-11-12 | 大日本住友製薬株式会社 | 内因性代謝物の分析方法 |
| CN102798672A (zh) * | 2011-05-21 | 2012-11-28 | 中国科学院大连化学物理研究所 | 一种检测血中gcdcs和gcdca的试剂盒 |
| JP6082328B2 (ja) * | 2013-07-31 | 2017-02-15 | 株式会社Ｌｓｉメディエンス | 胆汁酸同時分析方法 |
| JP6706497B2 (ja) * | 2015-12-24 | 2020-06-10 | 昭和電工株式会社 | 親水性化合物の分離分析方法 |
| CN108072704B (zh) * | 2016-11-08 | 2021-05-11 | 中国科学院大连化学物理研究所 | 基于液相色谱质谱联用的粪便中胆汁酸的检测方法 |
| CN106885867A (zh) * | 2017-03-30 | 2017-06-23 | 杭州佰辰医学检验所有限公司 | 高效液相色谱串联质谱检测血清中五种牛磺结合型胆汁酸的方法 |
| KR20230054473A (ko) * | 2020-09-04 | 2023-04-24 | 주식회사 아데랑스 | 담즙산류, 스테롤류 및 호르몬류의 분석 방법 및 분석 시스템 |
| JP6806948B1 (ja) * | 2020-09-04 | 2021-01-06 | 株式会社アデランス | 胆汁酸類、ステロール類、及びホルモン類の分析方法及び分析システム |
| CN113945668A (zh) * | 2021-09-15 | 2022-01-18 | 天津科技大学 | 一种靶向检测啮齿类动物非结合型胆汁酸的方法及其检测试剂盒 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60224061A (ja) * | 1984-04-23 | 1985-11-08 | Hitachi Ltd | 胆祇酸の分析装置 |
| JPS61264255A (ja) * | 1985-05-20 | 1986-11-22 | Hitachi Ltd | 胆汁酸の分析法 |
| JPS6287859A (ja) * | 1985-10-14 | 1987-04-22 | Asahi Chem Ind Co Ltd | 胆汁酸の分析方法 |
| JPH0339096A (ja) * | 1989-07-04 | 1991-02-20 | Sekisui Chem Co Ltd | 固定化酵素利用高速液体クロマトグラフィー |
| JP2570021B2 (ja) * | 1991-06-12 | 1997-01-08 | 東京田辺製薬株式会社 | 胆汁酸の一斉分析法 |
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2001
- 2001-11-02 JP JP2001338441A patent/JP2003139753A/ja active Pending
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