JP2002348660A - Method for manufacturing product of magnesium or magnesium alloy - Google Patents

Method for manufacturing product of magnesium or magnesium alloy

Info

Publication number
JP2002348660A
JP2002348660A JP2001149692A JP2001149692A JP2002348660A JP 2002348660 A JP2002348660 A JP 2002348660A JP 2001149692 A JP2001149692 A JP 2001149692A JP 2001149692 A JP2001149692 A JP 2001149692A JP 2002348660 A JP2002348660 A JP 2002348660A
Authority
JP
Japan
Prior art keywords
magnesium
vapor deposition
product
processed
processed product
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2001149692A
Other languages
Japanese (ja)
Other versions
JP4651854B2 (en
Inventor
Katsuhiro Nishiyama
勝廣 西山
Akinori Nakayama
明典 中山
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NISSANKI KK
Original Assignee
NISSANKI KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NISSANKI KK filed Critical NISSANKI KK
Priority to JP2001149692A priority Critical patent/JP4651854B2/en
Publication of JP2002348660A publication Critical patent/JP2002348660A/en
Application granted granted Critical
Publication of JP4651854B2 publication Critical patent/JP4651854B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Physical Vapour Deposition (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide a method for manufacturing products of magnesium or magnesium alloys, which can inexpensively impart them the equivalent corrosion resistance to those with high purity magnesium of 99.9999%, and employ inexpensive magnesium or magnesium alloys including impurities. SOLUTION: The method for manufacturing products of magnesium or magnesium alloys comprises a step of working magnesium or the magnesium alloys into a product shape, and a step of forming a magnesium vapor-deposited layer on the surface of the workpiece manufactured in the working step, with a vapor deposition method employing magnesium or the magnesium alloy as a vapor depositing metal, in a vacuum condition with an atmospheric pressure of 1 or lower and at 650 deg.C or lower.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明はマグネシウム、マグ
ネシウム合金製品の製造方法に関する。
The present invention relates to a method for producing magnesium and magnesium alloy products.

【0002】[0002]

【従来の技術】従来、マグネシウム、マグネシウム合金
製品は製品形状に加工した後、化成処理、メッキや塗装
等の表面処理を施している。
2. Description of the Related Art Conventionally, magnesium and magnesium alloy products are processed into product shapes and then subjected to surface treatments such as chemical conversion treatment, plating and painting.

【0003】[0003]

【発明が解決しようとする課題】従来のマグネシウム、
マグネシウム合金製品の化成処理、メッキや塗装等の表
面処理は、手数がかかりコスト高になったり、十分な耐
蝕性の改善を図ることができないという欠点があった。
SUMMARY OF THE INVENTION Conventional magnesium,
The surface treatments such as chemical conversion treatment, plating and painting of magnesium alloy products are troublesome and costly, and have the drawback that sufficient corrosion resistance cannot be improved.

【0004】本発明は以上のような従来の欠点に鑑み、
99.9999%の高純度のマグネシウムを用いた場合
と同等な耐蝕性の改善を、低コストで図ることができる
とともに、安価な不純物を含むマグネシウム、マグネシ
ウム合金を用いることができるマグネシウム、マグネシ
ウム合金製品の製造方法を提供することを目的としてい
る。
The present invention has been made in view of the above-mentioned conventional drawbacks,
Magnesium and magnesium alloy products that can improve corrosion resistance equivalent to the case of using 99.9999% high-purity magnesium at low cost, and can use magnesium or magnesium alloy containing inexpensive impurities. The purpose of the present invention is to provide a manufacturing method.

【0005】本発明の前記ならびにそのほかの目的と新
規な特徴は次の説明を添付図面と照らし合わせて読む
と、より完全に明らかになるであろう。ただし、図面は
もっぱら解説のためのものであって、本発明の技術的範
囲を限定するものではない。
The above and other objects and novel features of the present invention will become more completely apparent when the following description is read in conjunction with the accompanying drawings. However, the drawings are merely for explanation and do not limit the technical scope of the present invention.

【0006】[0006]

【課題を解決するための手段】上記目的を達成するため
に、本発明はマグネシウム、マグネシウム合金を用いて
製品形状に加工する加工工程と、この加工工程で加工さ
れた加工製品を気圧が1気圧以下で、温度が650℃以
下の真空中でマグネシウム、マグネシウム合金を蒸着金
属として用いた蒸着によって表面にマグネシウム蒸着層
を形成するマグネシウム蒸着工程とでマグネシウム、マ
グネシウム合金製品の製造方法を構成している。
In order to achieve the above-mentioned object, the present invention provides a processing step of processing a product shape using magnesium or a magnesium alloy, and a pressure of 1 atm for the processed product processed in the processing step. Hereinafter, a method of manufacturing a magnesium or magnesium alloy product is constituted by a magnesium deposition step of forming a magnesium deposition layer on a surface by vapor deposition using a magnesium or magnesium alloy as a deposition metal in a vacuum at a temperature of 650 ° C. or less. .

【0007】[0007]

【発明の実施の形態】以下、図面に示す実施の形態によ
り、本発明を詳細に説明する。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention will be described below in detail with reference to the embodiments shown in the drawings.

【0008】図1ないし図5に示す本発明の第1の実施
の形態において、1はマグネシウム、マグネシウム合金
を用いて製品形状に加工して加工製品2を製造する加工
工程で、この加工工程1では金属を製品形状に加工す
る、従来から一般に使用されているダイカスト成型、機
械加工等の加工作業によって行なう。
In the first embodiment of the present invention shown in FIGS. 1 to 5, reference numeral 1 denotes a processing step of manufacturing a processed product 2 by processing into a product shape using magnesium or a magnesium alloy. In this method, the metal is processed into a product shape by a conventionally used processing operation such as die casting or machining.

【0009】3は前記加工工程1で加工された加工製品
2をマグネシウム、マグネシウム合金を蒸着金属4とし
て用いた、蒸着によって表面にマグネシウム蒸着層5を
形成するマグネシウム蒸着工程で、このマグネシウム蒸
着工程3でのマグネシウムの蒸着は、図4に示すように
本願発明者が実験結果で得られた蒸着金属4の気圧と温
度との関係で、蒸着金属4が固体、液体、ガスとなる部
分の、経済的にガスとなる気圧が1気圧以下、好ましく
は10−3〜10−7mmHgで、温度が650℃以下
の真空中で蒸着を行なう。
Reference numeral 3 denotes a magnesium vapor deposition step in which the processed product 2 processed in the processing step 1 is formed of magnesium and a magnesium alloy as a vapor deposition metal 4 to form a magnesium vapor deposition layer 5 on the surface by vapor deposition. As shown in FIG. 4, the vapor deposition of magnesium is carried out according to the relationship between the atmospheric pressure and the temperature of the vapor-deposited metal 4 obtained by the present inventor based on the experimental results. The vapor deposition is performed in a vacuum at a pressure of 1 atm or less, preferably 10-3 to 10-7 mmHg, and at a temperature of 650 ° C or less.

【0010】この蒸着は図5に示すように、真空ポンプ
6によって真空状態にすることができる開閉扉7を有す
る真空蒸着室8が形成された真空蒸着炉本体9と、この
真空蒸着炉本体9内に設けられた、前記蒸着金属4を6
50℃程度に加熱する電気炉10と、この電気炉10か
ら蒸発する純マグネシウム4aを蒸着されるように、前
記加工製品2を支持する加工製品支持体11とで構成さ
れた蒸着装置12を用いて行なう。
As shown in FIG. 5, a vacuum evaporation furnace main body 9 in which a vacuum evaporation chamber 8 having an opening / closing door 7 which can be evacuated by a vacuum pump 6 is formed, as shown in FIG. The deposited metal 4 provided in
Using a vapor deposition device 12 composed of an electric furnace 10 for heating to about 50 ° C. and a processed product support 11 for supporting the processed product 2 so that pure magnesium 4a evaporated from the electric furnace 10 is deposited. Do it.

【0011】上記のようなマグネシウム、マグネシウム
合金製品の製造方法で製造されたマグネシウム、マグネ
シウム合金製品13は、加工製品2の表面に純マグネシ
ウムのマグネシウム蒸着層5が形成されているため、9
9.9999%のマグネシウムと同等の耐蝕性が得られ
る。このため、加工製品2を不純物が含まれている安価
なマグネシウム、マグネシウム合金を用いることがで
き、安価に製造することができる。
In the magnesium and magnesium alloy product 13 manufactured by the above-described method for manufacturing a magnesium and magnesium alloy product, since the magnesium deposition layer 5 of pure magnesium is formed on the surface of the processed product 2, 9
Corrosion resistance equivalent to 9.9999% magnesium is obtained. Therefore, the processed product 2 can be made of inexpensive magnesium or magnesium alloy containing impurities, and can be manufactured at low cost.

【0012】[0012]

【発明の異なる実施の形態】次に、図6ないし図10に
示す本発明の異なる実施の形態につき説明する。なお、
この本発明の異なる実施の形態の説明に当って、前記本
発明の第1の実施の形態と同一構成部分には同一符号を
付して重複する説明を省略する。
Next, different embodiments of the present invention shown in FIGS. 6 to 10 will be described. In addition,
In the description of the different embodiments of the present invention, the same components as those in the first embodiment of the present invention are denoted by the same reference numerals, and redundant description will be omitted.

【0013】図6ないし図10に示す本発明の第2の実
施の形態において、前記本発明の第1の実施の形態と主
に異なる点は、ダイカスト成型された加工製品2Aを真
空状態にしたバリ取り室内14に収納し、マグネシウ
ム、マグネシウム合金で形成した投射材15をインペラ
ー16を用いた投射機17で該加工製品2Aに投射し、
バリの除去および投射材15とインペラー16の衝撃お
よび摩擦による熱で気化マグネシウム4aを発生させ、
該気化マグネシウム4aを加工製品2Aの表面に蒸着さ
せてマグネシウム蒸着層5を形成するマグネシウム蒸着
工程3Aを行なった点で、このようなマグネシウム蒸着
工程3Aを用いたマグネシウム、マグネシウム合金製品
の製造方法を用いることにより、加工製品2Aのバリの
除去と、マグネシウム蒸着層5の形成とを同時に行なう
ことができる。
In the second embodiment of the present invention shown in FIGS. 6 to 10, the main difference from the first embodiment of the present invention is that the processed product 2A formed by die casting is in a vacuum state. It is housed in the deburring chamber 14, and a projection material 15 formed of magnesium or a magnesium alloy is projected on the processed product 2 </ b> A by a projector 17 using an impeller 16,
Removal of burrs and generation of vaporized magnesium 4a by heat due to impact and friction between the projectile 15 and the impeller 16,
The method of manufacturing a magnesium or magnesium alloy product using the magnesium vapor deposition step 3A is different from the magnesium vapor deposition step 3A in which the vaporized magnesium 4a is vapor-deposited on the surface of the processed product 2A to form the magnesium vapor deposition layer 5. By using this, the removal of burrs of the processed product 2A and the formation of the magnesium vapor deposition layer 5 can be performed simultaneously.

【0014】なお、前記マグネシウム蒸着工程3Aは図
8および図9に示す、バリ取り蒸着装置18を用いて行
なう。このバリ取り蒸着工程18は真空ポンプ6によっ
て、バリ取り室内14を真空にすることができる開閉扉
19を備えるケース体20と、このケース体20内に設
けられた投射材15が通過するメッシュ状の加工製品支
持台21と、この加工製品支持台21に支持された加工
製品2Aへ投射材15を投射できるように、前記ケース
体20に設けられたインペラー16を用いた投射機17
と、この投射機17へ投射材15を供給する投射材供給
装置22とで構成されている。
The magnesium vapor deposition step 3A is performed using a deburring vapor deposition apparatus 18 shown in FIGS. This deburring vapor deposition step 18 includes a case body 20 having an opening / closing door 19 capable of evacuating the deburring chamber 14 by the vacuum pump 6 and a mesh-like body through which the blast material 15 provided in the case body 20 passes. And a projector 17 using an impeller 16 provided in the case body 20 so that the projectile 15 can be projected onto the processed product 2A supported by the processed product support 21.
And a projecting material supply device 22 for supplying the projecting material 15 to the projector 17.

【0015】なお、前記本発明の各実施の形態では真空
蒸着について説明したが、本発明はこれに限らず、電子
ビーム蒸着によって加工製品2、2Aの表面に純マグネ
シウム蒸着層を形成してもよい。
In each of the embodiments of the present invention, the description has been given of the vacuum deposition. However, the present invention is not limited to this, and a pure magnesium vapor deposition layer may be formed on the surfaces of the processed products 2 and 2A by electron beam vapor deposition. Good.

【0016】[0016]

【発明の効果】以上の説明から明らかなように、本発明
にあっては次に列挙する効果が得られる。
As apparent from the above description, the following effects can be obtained in the present invention.

【0017】(1)マグネシウム、マグネシウム合金を
用いて製品形状に加工する加工工程と、この加工工程で
加工された加工製品を気圧が1気圧以下で、温度が65
0℃以下の真空中でマグネシウム、マグネシウム合金を
蒸着金属として用いた蒸着によって表面にマグネシウム
蒸着層を形成するマグネシウム蒸着工程とからなるの
で、マグネシウム蒸着層は純マグネシウムになるので、
99.9999%の高純度のマグネシウムと同等の耐蝕
性が得られる。したがって、耐蝕性が問題で使用されな
かった分野の金属製品にも十分に使用することができ
る。
(1) A processing step of processing into a product shape using magnesium or a magnesium alloy, and the processed product processed in this processing step has a pressure of 1 atm or less and a temperature of 65 atm.
Magnesium in a vacuum of 0 ° C. or less, a magnesium vapor deposition step of forming a magnesium vapor deposition layer on the surface by vapor deposition using a magnesium alloy as a vapor deposition metal, so that the magnesium vapor deposition layer becomes pure magnesium,
Corrosion resistance equivalent to high-purity 99.9999% magnesium is obtained. Therefore, it can be sufficiently used for metal products in fields where corrosion resistance was not used due to a problem.

【0018】(2)前記(1)によって、加工製品は高
純度のマグネシウム、マグネシウム合金を用いなくても
よく、安価な材料でマグネシウム、マグネシウム合金製
品を製造することができる。
(2) According to the above (1), it is not necessary to use high-purity magnesium or magnesium alloy as a processed product, and it is possible to manufacture a magnesium or magnesium alloy product with an inexpensive material.

【0019】(3)前記(1)によって、マグネシウ
ム、マグネシウム合金で加工した加工製品の表面に純マ
グネシウム蒸着層を形成しているので、リサイクルする
場合、不純物が含まれておらず、容易に再利用を図るこ
とができる。
(3) According to the above (1), a pure magnesium vapor-deposited layer is formed on the surface of a processed product processed with magnesium or a magnesium alloy. Therefore, when recycled, it does not contain impurities and can be easily recycled. It can be used.

【0020】(4)請求項2も前記(1)〜(3)と同
様な効果が得られる。
(4) Claim 2 has the same effect as (1) to (3).

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の第1の実施の形態の工程図。FIG. 1 is a process chart of a first embodiment of the present invention.

【図2】本発明の第1の実施の形態の加工製品の断面
図。
FIG. 2 is a cross-sectional view of the processed product according to the first embodiment of the present invention.

【図3】マグネシウム蒸着層を形成した製品の断面図。FIG. 3 is a cross-sectional view of a product having a magnesium vapor-deposited layer formed thereon.

【図4】マグネシウムの気圧と温度の関係を示す説明
図。
FIG. 4 is an explanatory diagram showing the relationship between the atmospheric pressure and the temperature of magnesium.

【図5】本発明の第1の実施の形態の蒸着装置の説明
図。
FIG. 5 is an explanatory diagram of a vapor deposition device according to the first embodiment of the present invention.

【図6】本発明の第2の実施の形態の工程図。FIG. 6 is a process chart of a second embodiment of the present invention.

【図7】本発明の第2の実施の形態の加工製品の説明
図。
FIG. 7 is an explanatory view of a processed product according to a second embodiment of the present invention.

【図8】マグネシウム蒸着層を形成した製品の断面図。FIG. 8 is a cross-sectional view of a product having a magnesium vapor-deposited layer formed thereon.

【図9】本発明の第2の実施の形態のバリ取り蒸着装置
の断面図。
FIG. 9 is a sectional view of a deburring deposition apparatus according to a second embodiment of the present invention.

【図10】本発明の第2の実施の形態のバリ取り蒸着装
置の正面図。
FIG. 10 is a front view of a deburring deposition apparatus according to a second embodiment of the present invention.

【符号の説明】[Explanation of symbols]

1:加工工程、 2、2A:加工製品、3:マ
グネシウム蒸着工程、4:蒸着金属、 5:マ
グネシウム蒸着層、6:真空ポンプ、 7:開閉
扉、8:真空蒸着室、 9:真空蒸着炉本体、1
0:電気炉、 11:加工製品支持体、12:
蒸着装置、13:マグネシウム、マグネシウム合金製
品、14:バリ取り室内、 15:投射材、16:イ
ンペラー、 17:投射機、18:バリ取り蒸着装
置、19:開閉扉、20:ケース体、 21:加
工製品支持台、22:投射材供給装置。
1: processing step, 2A: processed product, 3: magnesium deposition step, 4: metal deposition, 5: magnesium deposition layer, 6: vacuum pump, 7: door, 8: vacuum deposition chamber, 9: vacuum deposition furnace Body, 1
0: electric furnace, 11: processed product support, 12:
Vapor deposition device, 13: magnesium, magnesium alloy product, 14: deburring room, 15: projectile material, 16: impeller, 17: projector, 18: deburring vapor deposition device, 19: opening / closing door, 20: case body, 21: Processed product support 22: Projectile material supply device.

───────────────────────────────────────────────────── フロントページの続き Fターム(参考) 4K029 AA02 BA01 BA21 BC01 CA01 CA17 DB03 DB04 DB17 JA01 ──────────────────────────────────────────────────続 き Continued on the front page F term (reference) 4K029 AA02 BA01 BA21 BC01 CA01 CA17 DB03 DB04 DB17 JA01

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 マグネシウム、マグネシウム合金を用い
て製品形状に加工する加工工程と、この加工工程で加工
された加工製品を気圧が1気圧以下で、温度が650℃
以下の真空中でマグネシウム、マグネシウム合金を蒸着
金属として用いた蒸着によって表面にマグネシウム蒸着
層を形成するマグネシウム蒸着工程とを含むことを特徴
とするマグネシウム、マグネシウム合金製品の製造方
法。
1. A processing step of processing a product shape using magnesium or a magnesium alloy, and a pressure of a pressure of 1 atm or less and a temperature of 650 ° C. of a processed product processed in the processing step.
A magnesium vapor deposition step of forming a magnesium vapor deposition layer on the surface by vapor deposition using magnesium or a magnesium alloy as a vapor deposition metal in a vacuum as described below.
【請求項2】 マグネシウム、マグネシウム合金を用い
てダイカスト成型により製品形状に加工する加工工程
と、この加工工程で加工された加工製品を真空状態にし
たバリ取り室内に収納し、マグネシウム、マグネシウム
合金で形成した投射材をインペラーを用いた投射機で該
加工製品に投射し、バリの除去および投射材とインペラ
ーの衝撃および摩擦による熱で気化マグネシウムを発生
させ、該気化マグネシウムを加工製品の表面に蒸着にさ
せてマグネシウム蒸着層を形成するマグネシウム蒸着工
程とを含むことを特徴とするマグネシウム、マグネシウ
ム合金製品の製造方法。
2. A processing step of processing into a product shape by die casting using magnesium and a magnesium alloy, and the processed product processed in this processing step is housed in a deburring chamber in a vacuum state. The formed blasting material is projected onto the processed product with a projector using an impeller to remove burrs and generate magnesium vaporized by heat due to the impact and friction of the projected material and the impeller, and the vaporized magnesium is deposited on the surface of the processed product A magnesium vapor deposition step of forming a magnesium vapor deposited layer.
JP2001149692A 2001-05-18 2001-05-18 Manufacturing method of magnesium and magnesium alloy products Expired - Fee Related JP4651854B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2001149692A JP4651854B2 (en) 2001-05-18 2001-05-18 Manufacturing method of magnesium and magnesium alloy products

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2001149692A JP4651854B2 (en) 2001-05-18 2001-05-18 Manufacturing method of magnesium and magnesium alloy products

Publications (2)

Publication Number Publication Date
JP2002348660A true JP2002348660A (en) 2002-12-04
JP4651854B2 JP4651854B2 (en) 2011-03-16

Family

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Country Status (1)

Country Link
JP (1) JP4651854B2 (en)

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* Cited by examiner, † Cited by third party
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JP2005240067A (en) * 2004-02-24 2005-09-08 Ulvac Japan Ltd Mg-VAPOR DEPOSITION METHOD

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