JP2000281376A - Production of preform for optical fiber - Google Patents

Production of preform for optical fiber

Info

Publication number
JP2000281376A
JP2000281376A JP9065499A JP9065499A JP2000281376A JP 2000281376 A JP2000281376 A JP 2000281376A JP 9065499 A JP9065499 A JP 9065499A JP 9065499 A JP9065499 A JP 9065499A JP 2000281376 A JP2000281376 A JP 2000281376A
Authority
JP
Japan
Prior art keywords
soot preform
heating furnace
preform
heating
traverse
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP9065499A
Other languages
Japanese (ja)
Inventor
Akitoshi Awamura
哲利 粟村
Tatsuya Sakano
達也 坂野
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujikura Ltd
Original Assignee
Fujikura Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fujikura Ltd filed Critical Fujikura Ltd
Priority to JP9065499A priority Critical patent/JP2000281376A/en
Publication of JP2000281376A publication Critical patent/JP2000281376A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/014Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/01446Thermal after-treatment of preforms, e.g. dehydrating, consolidating, sintering
    • C03B37/0146Furnaces therefor, e.g. muffle tubes, furnace linings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Thermal Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)

Abstract

PROBLEM TO BE SOLVED: To sufficiently heat upper part of a soot preform so as to dehydrate by adjusting and controlling traverse speed or adjusting and controlling the temp. of a heater of a heating furnace when at least upper end part of the soot preform suspended in the heating furnace approaches the heating area of the heating furnace. SOLUTION: The traverse of a soot preform suspended in a heating furnace in the dehydration process is carried out by three steps of the upward traversing, waiting for chance and the downward traversing. The speeds of upward and downward traverses are set to be nearly constant. The speed of the soot preform at the time of downward traversing is allowed to be reduced by providing a speed reduction control process slightly before a conical taper part of the upper end of the soot preform approaches the heating area of the heating furnace and enters the waiting process. Thereby, the upper end part of the soot preform is sufficiently heated in the speed reduction control process and the waiting process. In the case of the transition from the waiting process to the upward traversing process, the speed of the soot preform is gradually accelerated by providing an acceleration control process. It is preferable that the conical taper part of the lower end of the soot preform is heated by the same process as the process mentioned above.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、スートプリフォー
ムの脱水の改善を図った光ファイバ用母材の製造方法に
関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a preform for an optical fiber in which dewatering of a soot preform is improved.

【0002】[0002]

【従来の技術】従来から、気相軸付け法(VAD法)に
より製造された外付けのスートプリフォームにあって
は、焼結による透明ガラス化に先立って、その内部に含
まれる水分(主にOH基)を除去するため、加熱炉(脱
水炉)中に垂下させ、トラバースさせつつ加熱して脱水
させている。
2. Description of the Related Art Conventionally, in an external soot preform manufactured by a vapor phase axial method (VAD method), prior to the vitrification by sintering, the moisture (primarily) contained in the inside is reduced. In order to remove the OH group, the solution is suspended in a heating furnace (dehydration furnace) and is heated and dehydrated while traversing.

【0003】この脱水工程では、通常スートプリフォー
ムを加熱炉内に挿入して、次第に下降させる下トラバー
スと、この下トラバースの終了位置(最下端位置)から
次第に上昇させる上トラバースの1往復で行っている。
[0003] In this dewatering step, the soot preform is usually inserted into a heating furnace and performed in one reciprocation of a lower traverse which is gradually lowered and an upper traverse which is gradually raised from the end position (lowest lower end position) of the lower traverse. ing.

【0004】実際には、例えば図4に示すように、加熱
炉の筒型などの加熱部(電熱ヒータ)10部分にダミー
ロッド21に垂下されたスートプリフォーム20を挿入
し、上記のように上下のトラバースを1往復させて行っ
ている。
In practice, as shown in FIG. 4, for example, a soot preform 20 suspended from a dummy rod 21 is inserted into a heating section (electric heater) 10 such as a cylindrical shape of a heating furnace, and The upper and lower traverses are reciprocated once.

【0005】[0005]

【発明が解決しようとする課題】ところが、VAD法に
よる外付けのスートプリフォーム20の場合、ダミーロ
ッド21との接続部分である根元の上端部分20aにあ
っては、スートの堆積形状が下向きに次第に広がる円錐
形状(テーパー形状)となっているため、特にこの上端
部分20aでは、従来加熱が不十分となり易かった。
However, in the case of the external soot preform 20 by the VAD method, the soot deposition shape is downward at the upper end portion 20a at the base, which is the connection portion with the dummy rod 21. Because of the gradually expanding conical shape (tapered shape), the conventional heating tends to be insufficient particularly at the upper end portion 20a.

【0006】というのは、この上端部分20aでは、図
5に示すように、スート表面と加熱部10間の距離が、
スートプリフォーム20の有効径部分20bに対して、
大きくなり、また、加熱部10の間の上方側に大きな隙
間が生じるため、熱が上方に逃げ易くなるからと考えら
れる。なお、円錐形状のテーパー部分は、スートプリフ
ォーム20の下端側にもあるが、下端側では、この下端
側より上側部分が有効径部分20bであるため、熱の逃
げ道(隙間)が狭くなり、十分加熱されるので、上端部
分20aほど問題とはならない。
In the upper end portion 20a, as shown in FIG. 5, the distance between the soot surface and the heating section 10 is
For the effective diameter portion 20b of the soot preform 20,
This is considered to be due to the fact that heat becomes easy to escape upward due to the increase in size and the formation of a large gap on the upper side between the heating units 10. The conical tapered portion is also at the lower end side of the soot preform 20, but at the lower end side, the portion above the lower end side is the effective diameter portion 20b, so the escape path (gap) for heat becomes narrower, Since the heating is sufficiently performed, there is no problem as much as the upper end portion 20a.

【0007】そこで、従来にあっても、トラバース速度
は、ほぼ一定に保っているものの、スートプリフォーム
20の上端部分20aが加熱部10に達し、その加熱エ
リア内に入った後は、しばらく待機させた後上トラバー
スを開始させている。
Therefore, although the traverse speed is kept almost constant even in the prior art, the upper end portion 20a of the soot preform 20 reaches the heating section 10 and waits for a while after entering the heating area. After that, the upper traverse is started.

【0008】しかしながら、このような待機による加熱
を行っても、得られた光ファイバの伝送損失特性からす
ると、脱水が未だ不十分であることが判った。
[0008] However, even if such standby heating is performed, it has been found that dehydration is still insufficient from the transmission loss characteristics of the obtained optical fiber.

【0009】本発明は、このような観点に立ってなされ
たもので、スートプリフォームの少なくとも上端部分が
加熱炉の加熱エリアに接近する際、トラバース速度を調
整制御したり、或いは加熱炉のヒーター温度を調整制御
したりして、十分な加熱が行われるようにした光ファイ
バ用母材の製造方法を提供せんとするものである。
SUMMARY OF THE INVENTION The present invention has been made in view of the above. When at least the upper end portion of the soot preform approaches the heating area of the heating furnace, the traverse speed is adjusted and controlled, or the heater of the heating furnace is controlled. It is an object of the present invention to provide a method of manufacturing a preform for optical fiber in which sufficient heating is performed by adjusting and controlling the temperature.

【0010】[0010]

【課題を解決するための手段】請求項1記載の本発明
は、加熱炉中に垂下させたスートプリフォームをトラバ
ースさせて脱水する工程において、前記スートプリフォ
ームの少なくとも上端部分が前記加熱炉の加熱エリアに
接近する際、前記スートプリフォームのトラバース速度
を調整制御することを特徴とする光ファイバ用母材の製
造方法にある。
According to a first aspect of the present invention, in the step of traversing a soot preform suspended in a heating furnace and dewatering the soot preform, at least an upper end portion of the soot preform is formed of the heating furnace. A method of manufacturing a preform for optical fiber, comprising adjusting and controlling a traverse speed of the soot preform when approaching a heating area.

【0011】請求項2記載の本発明は、加熱炉中に垂下
させたスートプリフォームをトラバースさせて脱水する
工程において、前記スートプリフォームの少なくとも上
端部分が前記加熱炉の加熱エリアに接近する際、前記加
熱炉のヒーター温度を調整制御することを特徴とする光
ファイバ用母材の製造方法にある。
According to a second aspect of the present invention, in the step of traversing and dewatering a soot preform suspended in a heating furnace, at least an upper end portion of the soot preform approaches a heating area of the heating furnace. And a method for producing a preform for an optical fiber, wherein a heater temperature of the heating furnace is adjusted and controlled.

【0012】[0012]

【発明の実施の形態】先ず、上記請求項1記載の本発明
では、図1に示すように、スートプリフォームの脱水に
あったて、下トラバース工程T1,待機工程T2,上ト
ラバースT3の各工程を行うものとする。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS First, in the present invention, as shown in FIG. 1, each of a lower traverse step T1, a standby step T2, and an upper traverse T3 in dehydrating a soot preform. Steps shall be performed.

【0013】そして、上下のトラバース速度は、ほぼ一
定(V1、例えば600mm/h程度)として設定して
あるものの、少なくとも下トラバース工程T1の待機工
程T2に至る少々前には、減速調整工程T1aを設け
て、減速させる。この減速は、図示のように徐々に行う
ことが理想的であるが、例えばこの期間400mm/h
程度で定速で減速させたり、階段状に複数回に渡って減
速させてもよい。
Although the upper and lower traverse speeds are set to be substantially constant (V1, for example, about 600 mm / h), the deceleration adjustment process T1a is performed at least slightly before the standby process T2 of the lower traverse process T1. Provide and decelerate. Ideally, this deceleration is performed gradually as shown in the figure.
The speed may be decelerated at a constant speed, or may be decelerated a plurality of times stepwise.

【0014】この待機工程T2に至る前の減速調整工程
T1aによって、スートプリフォームの上端部分は、多
くの熱の供給を受けて待機工程T2に入る。このため、
結果として、十分な加熱が行われ、従来のような加熱不
十分は解消される。
In the deceleration adjusting step T1a before the standby step T2, the upper end portion of the soot preform receives a large amount of heat and enters the standby step T2. For this reason,
As a result, sufficient heating is performed, and conventional insufficient heating is eliminated.

【0015】一方、本発明では、好ましいケースとし
て、待機工程T2から開始される上トラバース工程T3
の際にも、加速調整工程T3aを設けて、徐々に加速さ
せるようにしている。原理的には、上記減速調整工程T
1aの採用によって、十分な加熱が可能となるが、この
加速調整工程T3aを併用すれば、これと、上記減速調
整工程T1a、及び待機工程T2の3工程間での組み合
わせによって、各工程での加熱分担の調整などが楽にな
り、バランスの取れた工程制御が可能となる。
On the other hand, in the present invention, as a preferable case, the upper traverse step T3 started from the standby step T2
Also in this case, an acceleration adjustment step T3a is provided to gradually accelerate. In principle, the deceleration adjustment step T
The use of 1a enables sufficient heating. However, if this acceleration adjustment step T3a is used in combination, the combination of the acceleration adjustment step T3a, the deceleration adjustment step T1a, and the standby step T2 allows the heating in each step. Adjustment of the heating allotment becomes easy, and balanced process control becomes possible.

【0016】なお、上述したように、円錐形状のテーパ
ー部分は、スートプリフォームの下端側にもあるので、
必要により、この下端部分が加熱炉の加熱エリアに接近
する際にも、上記と同様の減速調整工程や加速調整工程
を設けることが可能である。これによって、下端部分側
にあっても、上記と同様の効果が得られる。
As described above, since the conical tapered portion is also at the lower end of the soot preform,
If necessary, even when the lower end portion approaches the heating area of the heating furnace, the same deceleration adjustment step and acceleration adjustment step as described above can be provided. As a result, the same effect as above can be obtained even at the lower end portion side.

【0017】因みに、本発明の方法により得られた母材
(全長=1400mm、母材直径=160mm、ダミー
ロッド直径=25mm、テーパー部分の長さ=200m
m)を用いた光ファイバと、従来方法により得られた母
材(全長など各データは上記本発明の母材とほぼ同様の
もの)を用いた光ファイバの各伝送損失特性とを比較し
たところ、図2の如くであった。
Incidentally, the base material obtained by the method of the present invention (total length = 1400 mm, base material diameter = 160 mm, dummy rod diameter = 25 mm, length of tapered portion = 200 m)
Comparison between the transmission loss characteristics of the optical fiber using m) and the optical fiber using the preform obtained by the conventional method (each data such as the overall length is substantially the same as the preform of the present invention). FIG.

【0018】つまり、従来方法による光ファイバの伝送
特性曲線IIによると、波長が1380nmの部分に大
きな損失増大部IIaが見られるの対して、本発明の方
法による光ファイバの伝送特性曲線Iでは、この間の損
失増大部Iaが小さく、大幅に改善されていることが判
る。
That is, according to the transmission characteristic curve II of the optical fiber according to the conventional method, a large loss increasing portion IIa is observed at the wavelength of 1380 nm, whereas the transmission characteristic curve I of the optical fiber according to the method of the present invention is: It can be seen that the loss increasing portion Ia during this period is small and greatly improved.

【0019】次に、この請求項1記載の本発明では、ト
ラバース速度の調整制御によって、スートプリフォーム
側の温度制御を行っているが、このような温度制御は、
トラバース速度が一定であっても、スートプリフォーム
の上端部分が加熱炉の加熱エリアに接近するときに合わ
せて、加熱炉側の加熱温度の制御によっても、可能とな
る。
Next, in the present invention according to the first aspect, the temperature control on the soot preform side is performed by controlling the traverse speed.
Even if the traverse speed is constant, the heating temperature can be controlled by controlling the heating temperature on the heating furnace side when the upper end portion of the soot preform approaches the heating area of the heating furnace.

【0020】上記請求項2記載の本発明は、このような
観点に立って、図3に示すように、スートプリフォーム
の脱水にあたって、上記と同様、下トラバース工程T
1,待機工程T2,上トラバースT3の各工程を設ける
一方、少なくとも下トラバース工程T1の待機工程T2
に至る少々前には、昇温させる昇温調整工程T1bを設
けてある。また、必要により、待機工程T2から開始さ
れる上トラバース工程T3にも、温度を低下させる降温
調整工程T3bを設けてある。なお、図中、t1は通常
トラバース時の温度、t2は待機工程時の温度である。
In view of the above, according to the present invention, as shown in FIG. 3, the dehydration of the soot preform is performed in the same manner as described above in the lower traverse step T.
1, a standby step T2 and an upper traverse step T3, while at least a standby step T2 of the lower traverse step T1
Slightly before reaching, a temperature raising adjustment step T1b for raising the temperature is provided. If necessary, the upper traverse step T3 started from the standby step T2 is also provided with a temperature lowering adjustment step T3b for lowering the temperature. In the drawing, t1 is the temperature during the normal traverse, and t2 is the temperature during the standby process.

【0021】つまり、スートプリフォームの上端部分が
加熱炉の加熱エリアに接近する際に、スートプリフォー
ムの加熱温度を昇温させたり、降温させたりしている。
この昇温や降温も徐々に行っり、階段状などに行っても
よい。いずれにしても、これからの温度制御によって、
上記のトラバース速度制御の場合とほぼ同様の効果が得
られる。
That is, when the upper end portion of the soot preform approaches the heating area of the heating furnace, the heating temperature of the soot preform is raised or lowered.
The temperature increase and the temperature decrease may be performed gradually, and may be performed in a step-like manner. Either way, with future temperature control,
Almost the same effects as in the case of the above traverse speed control can be obtained.

【0022】さらに、また、本発明では、上記トラバー
ス速度の調整制御と加熱炉側の加熱温度の調整制御とを
適宜組み合わせた製造方法とすることも可能である。
Further, according to the present invention, it is also possible to provide a manufacturing method in which the above-described control for adjusting the traverse speed and the control for adjusting the heating temperature on the heating furnace side are appropriately combined.

【0023】[0023]

【発明の効果】以上の説明から明らかなように、本発明
に係る光ファイバ用母材の製造方法によれば、従来加熱
不足となり易かったスートプリフォームの少なくとも上
端部分に対して、トラバース速度制御や加熱炉の加熱温
度制御によって、十分な加熱が行われるため、結果とし
て、スートプリフォームの全長に渡って良好な脱水が行
われる。
As is apparent from the above description, according to the method of manufacturing the optical fiber preform according to the present invention, the traverse speed control is performed on at least the upper end portion of the soot preform which has been apt to be insufficiently heated. Sufficient heating is performed by controlling the heating temperature of the heating furnace and the heating furnace. As a result, good dehydration is performed over the entire length of the soot preform.

【図面の簡単な説明】[Brief description of the drawings]

【図1】 本発明に係る光ファイバ用母材の製造方法に
おける各工程を説明した概略説明図である。
FIG. 1 is a schematic explanatory view illustrating each step in a method for manufacturing an optical fiber preform according to the present invention.

【図2】 図1の本発明による母材を用いた光ファイバ
と従来方法による母材を用いた光ファイバの各伝送特性
曲線を示したグラフである。
2 is a graph showing transmission characteristic curves of the optical fiber using the preform according to the present invention and the optical fiber using the preform according to the conventional method of FIG. 1;

【図3】 本発明に係る他の光ファイバ用母材の製造方
法における各工程を説明した概略説明図である。
FIG. 3 is a schematic explanatory view illustrating each step in a method for manufacturing another optical fiber preform according to the present invention.

【図4】 光ファイバ用母材の脱水工程を示した概略説
明図である。
FIG. 4 is a schematic explanatory view showing a dehydrating step of an optical fiber preform.

【図5】 図4の脱水工程における加熱炉とスートプリ
フォームの上端部分との関係を示した概略説明図であ
る。
FIG. 5 is a schematic explanatory view showing a relationship between a heating furnace and an upper end portion of a soot preform in a dehydrating step of FIG.

【符号の説明】[Explanation of symbols]

10 加熱部 20 スートプリフォーム 20a 上端部分 T1 下トラバース工程 T2 待機工程 T3 上トラバース工程 T1a 減速調整工程 T3a 加速調整工程 T1b 昇温調整工程 T3b 降温調整工程 Reference Signs List 10 heating section 20 soot preform 20a upper end portion T1 lower traverse step T2 standby step T3 upper traverse step T1a deceleration adjustment step T3a acceleration adjustment step T1b temperature increase adjustment step T3b temperature decrease adjustment step

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 加熱炉中に垂下させたスートプリフォー
ムをトラバースさせて脱水する工程において、前記スー
トプリフォームの少なくとも上端部分が前記加熱炉の加
熱エリアに接近する際、前記スートプリフォームのトラ
バース速度を調整制御することを特徴とする光ファイバ
用母材の製造方法。
In the step of traversing and dehydrating a soot preform suspended in a heating furnace, when at least an upper end portion of the soot preform approaches a heating area of the heating furnace, the soot preform is traversed. A method for manufacturing a preform for an optical fiber, wherein the speed is adjusted and controlled.
【請求項2】 加熱炉中に垂下させたスートプリフォー
ムをトラバースさせて脱水する工程において、前記スー
トプリフォームの少なくとも上端部分が前記加熱炉の加
熱エリアに接近する際、前記加熱炉のヒーター温度を調
整制御することを特徴とする光ファイバ用母材の製造方
法。
2. In the step of traversing and dewatering a soot preform suspended in a heating furnace, when at least an upper end portion of the soot preform approaches a heating area of the heating furnace, a heater temperature of the heating furnace is reduced. A method for producing a preform for an optical fiber, comprising:
JP9065499A 1999-03-31 1999-03-31 Production of preform for optical fiber Pending JP2000281376A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP9065499A JP2000281376A (en) 1999-03-31 1999-03-31 Production of preform for optical fiber

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