IT1163540B - Procedimento per la purificazione dello sciroppo di lattulosio - Google Patents
Procedimento per la purificazione dello sciroppo di lattulosioInfo
- Publication number
- IT1163540B IT1163540B IT21689/83A IT2168983A IT1163540B IT 1163540 B IT1163540 B IT 1163540B IT 21689/83 A IT21689/83 A IT 21689/83A IT 2168983 A IT2168983 A IT 2168983A IT 1163540 B IT1163540 B IT 1163540B
- Authority
- IT
- Italy
- Prior art keywords
- anionic resin
- purification
- resin
- syrup
- strong
- Prior art date
Links
- JCQLYHFGKNRPGE-FCVZTGTOSA-N lactulose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 JCQLYHFGKNRPGE-FCVZTGTOSA-N 0.000 title abstract 2
- 229960000511 lactulose Drugs 0.000 title abstract 2
- PFCRQPBOOFTZGQ-UHFFFAOYSA-N lactulose keto form Natural products OCC(=O)C(O)C(C(O)CO)OC1OC(CO)C(O)C(O)C1O PFCRQPBOOFTZGQ-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 239000006188 syrup Substances 0.000 title abstract 2
- 235000020357 syrup Nutrition 0.000 title abstract 2
- 238000000746 purification Methods 0.000 title 1
- 239000011347 resin Substances 0.000 abstract 5
- 229920005989 resin Polymers 0.000 abstract 5
- 125000000129 anionic group Chemical group 0.000 abstract 3
- 125000002091 cationic group Chemical group 0.000 abstract 2
- JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 abstract 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical group OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 abstract 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 238000006056 electrooxidation reaction Methods 0.000 abstract 1
- 239000003456 ion exchange resin Substances 0.000 abstract 1
- 229920003303 ion-exchange polymer Polymers 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
- C07H3/04—Disaccharides
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/005—Lactulose
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Jellies, Jams, And Syrups (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT21689/83A IT1163540B (it) | 1983-06-20 | 1983-06-20 | Procedimento per la purificazione dello sciroppo di lattulosio |
| AT84104558T ATE26130T1 (de) | 1983-06-20 | 1984-04-22 | Verfahren zur reinigung von lactulosesirup. |
| DE8484104558T DE3462801D1 (en) | 1983-06-20 | 1984-04-22 | Process for purifying lactulose syrup |
| EP84104558A EP0132509B1 (en) | 1983-06-20 | 1984-04-22 | Process for purifying lactulose syrup |
| US06/621,542 US4555271A (en) | 1983-06-20 | 1984-06-18 | Process for purifying lactulose syrup |
| CA000456855A CA1223581A (en) | 1983-06-20 | 1984-06-19 | Process for purifying lactulose syrup |
| GB08415701A GB2143826B (en) | 1983-06-20 | 1984-06-20 | Purifying lactulose syrups |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT21689/83A IT1163540B (it) | 1983-06-20 | 1983-06-20 | Procedimento per la purificazione dello sciroppo di lattulosio |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IT8321689A0 IT8321689A0 (it) | 1983-06-20 |
| IT1163540B true IT1163540B (it) | 1987-04-08 |
Family
ID=11185427
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IT21689/83A IT1163540B (it) | 1983-06-20 | 1983-06-20 | Procedimento per la purificazione dello sciroppo di lattulosio |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4555271A (it) |
| EP (1) | EP0132509B1 (it) |
| AT (1) | ATE26130T1 (it) |
| CA (1) | CA1223581A (it) |
| DE (1) | DE3462801D1 (it) |
| GB (1) | GB2143826B (it) |
| IT (1) | IT1163540B (it) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113150042A (zh) * | 2021-04-16 | 2021-07-23 | 大连美罗中药厂有限公司 | 一种乳果糖的制备方法 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3608322A1 (de) * | 1986-03-13 | 1987-10-01 | Fritz Guht | Verfahren zur gewinnung von milchzucker aus molke unter verwendung von zeolithen |
| IT1223398B (it) * | 1987-12-01 | 1990-09-19 | Sirac Spa | Procedimento per la preparazione di lattulosio cristallino ad alta purezza |
| IT1224438B (it) * | 1987-12-30 | 1990-10-04 | Sirac Srl | Processo per l'ottenimento di sciroppi di lattulosio ad elevata purezza e sciroppo cosi' ottenuto |
| DK170977B1 (da) * | 1988-04-28 | 1996-04-09 | Duphar Int Res | Fremgangsmåde til fremstilling af lactulose |
| DK249789A (da) * | 1988-05-26 | 1989-11-27 | Duphar Int Res | Praeparat med anti-endotoxisk aktivitet |
| EP0357068A3 (en) * | 1988-09-01 | 1991-07-24 | Ault Foods Limited | Production process of high-purity lactulose syrup |
| ATE104306T1 (de) * | 1988-12-21 | 1994-04-15 | Duphar Int Res | Verfahren zur herstellung von lactulose. |
| IT1271449B (it) * | 1993-04-28 | 1997-05-28 | Inalco Spa | Procedimento per la preparazione di lattulosio cristallino da sciroppi commerciali |
| FR2710922B1 (fr) * | 1993-10-05 | 1996-01-05 | Univ Rennes | Procédé de cristallisation du lactulose. |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB865594A (en) * | 1956-03-10 | 1961-04-19 | Tervalon Nv | Improvements in or relating to producing crystalline lactulose |
| US3546206A (en) * | 1967-09-20 | 1970-12-08 | Kraftco Corp | Method of making lactulose |
| US3505309A (en) * | 1967-09-25 | 1970-04-07 | Research Corp | Process for lactulose |
| AT288595B (de) * | 1969-02-07 | 1971-03-10 | Laevosan Gmbh & Co Kg | Verfahren zur Herstellung von Lactulose-Konzentrat |
| IT1023006B (it) * | 1969-07-31 | 1978-05-10 | Hayashibara Co | Procedimento per la produzione di lattulosio da lattosio e prodotto relativo |
| JPS5420578B1 (it) * | 1970-12-09 | 1979-07-24 | ||
| JPS522984B1 (it) * | 1971-05-22 | 1977-01-25 | ||
| JPS4944331B1 (it) * | 1971-05-31 | 1974-11-27 | ||
| US4394178A (en) * | 1981-12-10 | 1983-07-19 | Union Carbide Corporation | Bulk lactulose/lactose separation by selective adsorption on zeolitic molecular sieves |
-
1983
- 1983-06-20 IT IT21689/83A patent/IT1163540B/it active
-
1984
- 1984-04-22 EP EP84104558A patent/EP0132509B1/en not_active Expired
- 1984-04-22 AT AT84104558T patent/ATE26130T1/de not_active IP Right Cessation
- 1984-04-22 DE DE8484104558T patent/DE3462801D1/de not_active Expired
- 1984-06-18 US US06/621,542 patent/US4555271A/en not_active Expired - Fee Related
- 1984-06-19 CA CA000456855A patent/CA1223581A/en not_active Expired
- 1984-06-20 GB GB08415701A patent/GB2143826B/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113150042A (zh) * | 2021-04-16 | 2021-07-23 | 大连美罗中药厂有限公司 | 一种乳果糖的制备方法 |
| CN113150042B (zh) * | 2021-04-16 | 2022-11-08 | 大连美罗中药厂有限公司 | 一种乳果糖的制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0132509B1 (en) | 1987-03-25 |
| GB2143826A (en) | 1985-02-20 |
| ATE26130T1 (de) | 1987-04-15 |
| GB8415701D0 (en) | 1984-07-25 |
| US4555271A (en) | 1985-11-26 |
| GB2143826B (en) | 1986-04-30 |
| DE3462801D1 (en) | 1987-04-30 |
| IT8321689A0 (it) | 1983-06-20 |
| EP0132509A1 (en) | 1985-02-13 |
| CA1223581A (en) | 1987-06-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| TA | Fee payment date (situation as of event date), data collected since 19931001 |
Effective date: 19970630 |