IN2014DN07241A - - Google Patents

Info

Publication number
IN2014DN07241A
IN2014DN07241A IN7241DEN2014A IN2014DN07241A IN 2014DN07241 A IN2014DN07241 A IN 2014DN07241A IN 7241DEN2014 A IN7241DEN2014 A IN 7241DEN2014A IN 2014DN07241 A IN2014DN07241 A IN 2014DN07241A
Authority
IN
India
Prior art keywords
crude liquid
liquid isocyanate
isocyanate stream
phosgenating
phosgenation
Prior art date
Application number
Inventor
Rainer Bruns
Wolfgang Lorenz
Andreas Karl Rausch
Stefan Wershofen
Tim Loddenkemper
Original Assignee
Bayer Ip Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Ip Gmbh filed Critical Bayer Ip Gmbh
Publication of IN2014DN07241A publication Critical patent/IN2014DN07241A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00Preparation of derivatives of isocyanic acid
    • C07C263/10Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00Preparation of derivatives of isocyanic acid
    • C07C263/18Separation; Purification; Stabilisation; Use of additives
    • C07C263/20Separation; Purification
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Abstract

The invention relates to a method for producing isocyanates by phosgenating the corresponding amines wherein low boiling secondary components excessive phosgene and the coupling product hydrogen chloride are separated from the crude liquid isocyanate stream which is obtained after the phosgenation has occurred within a maximum of 60 minutes. The crude liquid isocyanate stream is not exposed to temperatures above 250 °C until said separation.
IN7241DEN2014 2012-03-19 2013-03-15 IN2014DN07241A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12160168 2012-03-19
PCT/EP2013/055411 WO2013139703A1 (en) 2012-03-19 2013-03-15 Method for producing isocyanates

Publications (1)

Publication Number Publication Date
IN2014DN07241A true IN2014DN07241A (en) 2015-04-24

Family

ID=47882196

Family Applications (1)

Application Number Title Priority Date Filing Date
IN7241DEN2014 IN2014DN07241A (en) 2012-03-19 2013-03-15

Country Status (10)

Country Link
US (2) US9593075B2 (en)
EP (1) EP2828235B1 (en)
JP (1) JP6113824B2 (en)
KR (1) KR102020697B1 (en)
CN (2) CN104203910A (en)
ES (1) ES2658214T3 (en)
HU (1) HUE035678T2 (en)
IN (1) IN2014DN07241A (en)
PT (1) PT2828235T (en)
WO (1) WO2013139703A1 (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20160138410A (en) 2014-03-27 2016-12-05 코베스트로 도이칠란트 아게 Method for operating a gas-phase phosgenation plant
KR20160137544A (en) 2014-03-27 2016-11-30 코베스트로 도이칠란트 아게 Process for operating a gas phase phosgenation plant
US10513487B2 (en) 2014-06-24 2019-12-24 Covestro Deutschland Ag Methods for producing chemical products with operation interruptions
HUE055741T2 (en) 2016-08-17 2021-12-28 Covestro Intellectual Property Gmbh & Co Kg Method and device for the production of various chemical products
HUE053661T2 (en) * 2016-12-21 2021-07-28 Covestro Intellectual Property Gmbh & Co Kg Method for drying of tdi remnants
EP3634947B1 (en) * 2017-06-08 2022-09-07 Covestro Intellectual Property GmbH & Co. KG Method for the production of isocyanates in the gasphase
JP6839621B2 (en) * 2017-06-22 2021-03-10 本田技研工業株式会社 Gas-liquid separator
CN107353231A (en) * 2017-07-17 2017-11-17 薛永和 A kind of method for preparing organic isocyanate
CN111496949A (en) * 2020-03-20 2020-08-07 广西丰林木业集团股份有限公司 Formaldehyde-free moisture-proof shaving board and preparation process thereof
KR20220095869A (en) * 2020-12-30 2022-07-07 한화솔루션 주식회사 Method for preparing isocyanate compound
KR20220095867A (en) * 2020-12-30 2022-07-07 한화솔루션 주식회사 Method for preparing isocyanate compound
KR20220095865A (en) * 2020-12-30 2022-07-07 한화솔루션 주식회사 Method for preparing isocyanate compound
CN114149345B (en) * 2021-12-09 2023-04-21 万华化学集团股份有限公司 Method for preparing isocyanate

Family Cites Families (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2471134A (en) 1946-07-17 1949-05-24 Standard Oil Dev Co Fractionation apparatus
GB736465A (en) * 1952-08-14 1955-09-07 Du Pont Preparation of aromatic isocyanates
GB1165831A (en) 1967-01-26 1969-10-01 Ici Ltd Process for the Production of Isocyanates and Carbamyl Chlorides
GB1238669A (en) 1968-03-12 1971-07-07
DE1923214B2 (en) 1969-05-07 1973-08-02 PROCESS FOR THE SIMULTANEOUS PREPARATION OF PURE 4,4'-DIPHENYLMETHANE DIISOCYANATE AND A POLYPHENYL-POLYMETHYLENE-POLYISOCYANATE MIXTURE, POLYPHENYL-POLYMETHYLENE-POLYISOCYANATE, AND THE USE OF POLYPHENYL-POLYMETHYLENE-POLYISOCYANATE
US3713833A (en) 1970-10-28 1973-01-30 Eastman Kodak Co Preparation of silver salts in an organic liquid medium
US3987075A (en) * 1972-01-03 1976-10-19 Olin Corporation Solvent extraction and distillation technique for purification of organic isocyanates
US4118286A (en) * 1974-09-25 1978-10-03 Texaco Development Corp. Process for reducing the acidity of organic polymeric isocyanates
DE2844591A1 (en) 1978-10-13 1980-04-24 Texaco Development Corp Purification of polymethylene poly:phenyl isocyanate by distn. - with distn. residue held hot and recycled
US4289732A (en) 1978-12-13 1981-09-15 The Upjohn Company Apparatus for intimately admixing two chemically reactive liquid components
DE3121036A1 (en) 1981-05-27 1982-12-16 Bayer Ag, 5090 Leverkusen METHOD FOR THE CONTINUOUS PRODUCTION OF ORGANIC MONO- OR POLYISOCYANATES
DE3714439A1 (en) 1987-04-30 1988-11-10 Bayer Ag METHOD FOR PRODUCING (CYCLO) ALIPHATIC DIISOCYANATES
DE3717058A1 (en) 1987-05-21 1988-12-08 Bayer Ag MIXER FOR MIXING AT LEAST TWO FLOWABLE SUBSTANCES, ESPECIALLY UNDERSTANDING OR. INITIATING A REACTION DURING MIXING
DE3717057A1 (en) 1987-05-21 1988-12-01 Bayer Ag METHOD FOR PRODUCING ISOCYANATES
DE4217019A1 (en) 1992-05-22 1993-11-25 Bayer Ag Process for the preparation of aromatic diisocyanates
FR2697017B1 (en) 1992-10-16 1995-01-06 Rhone Poulenc Chimie Process for the preparation of compounds of the aromatic isocyanate type in the gas phase.
PL180229B1 (en) * 1994-11-17 2001-01-31 Bayer Ag Method of obtaining isocyanates
DE19638567A1 (en) 1996-09-20 1998-03-26 Bayer Ag Mixer reactor and process for carrying out reactions, in particular the phosgenation of primary amines
US20030047438A1 (en) 1998-05-06 2003-03-13 Sumitomo Heavy Industries, Ltd. Distillation apparatus and distillation method
EP1371633A1 (en) 2002-06-14 2003-12-17 Bayer Ag Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column
EP1371634A1 (en) 2002-06-14 2003-12-17 Bayer Ag Process for the purification of mixtures of toluenediisocyanate
DE10245584A1 (en) 2002-09-27 2004-04-08 Basf Ag Processing of reaction discharges from phosgenation reactors
ES2271171T3 (en) 2002-10-22 2007-04-16 Bayer Materialscience Ag PROCEDURE FOR THE PURIFICATION OF TOLUENDIISOCIANATE THAT INCORPORATES A DIVISORY WALL DISTILLATION COLUMN FOR FINAL PURIFICATION.
DE10260093A1 (en) 2002-12-19 2004-07-01 Basf Ag Process for the separation of isocyanates from a reaction mixture
DE10260027A1 (en) 2002-12-19 2004-07-08 Basf Ag Process for the separation and purification of solvents from a reaction mixture from an isocyanate synthesis
DE10260092A1 (en) 2002-12-19 2004-07-01 Basf Ag Process for the purification of isocyanates
DE10261187A1 (en) * 2002-12-20 2004-07-08 Basf Ag Process for the preparation of isocyanates
DE10307141A1 (en) 2003-02-20 2004-09-02 Bayer Ag Process for the preparation of (poly) isocyanates in the gas phase
DE10310888A1 (en) 2003-03-11 2004-09-23 Basf Ag Production of polyisocyanates useful for polyurethane production comprises reacting an amine with phosgene in a tubular reactor and passing the reactor effluent to a distillation column
EP1475367B1 (en) 2003-05-08 2010-07-07 Bayer MaterialScience AG Distillation process for separating diisocyanatodiphenylmethane isomers
US20070232827A1 (en) * 2004-05-25 2007-10-04 Basf Aktiengesellschaft Isocyanate Production Method
DE102006022448A1 (en) 2006-05-13 2007-11-15 Bayer Materialscience Ag Process for the preparation of isocyanates
US7547801B2 (en) 2006-06-26 2009-06-16 Bayer Materialscience Llc Process for the continuous preparation of isocyanates
EP2197836B1 (en) 2007-08-31 2013-04-24 Basf Se Method for the production of isocyanates
JP5479675B2 (en) 2007-11-14 2014-04-23 三井化学株式会社 Method for producing toluene diisocyanate
CN102224132B (en) 2008-10-02 2013-09-11 陶氏环球技术有限责任公司 Apparatus, systems, and methods for purification of isocyanate mixtures
DE102008061686A1 (en) 2008-12-11 2010-06-17 Bayer Materialscience Ag Process for the preparation of isocyanates in the gas phase
DE102008063728A1 (en) 2008-12-18 2010-06-24 Bayer Materialscience Ag Process for the preparation of isocyanates in the gas phase

Also Published As

Publication number Publication date
PT2828235T (en) 2018-02-07
WO2013139703A1 (en) 2013-09-26
KR102020697B1 (en) 2019-09-10
US9593075B2 (en) 2017-03-14
US20150291512A1 (en) 2015-10-15
KR20140136456A (en) 2014-11-28
CN104203910A (en) 2014-12-10
ES2658214T3 (en) 2018-03-08
US9695115B2 (en) 2017-07-04
JP6113824B2 (en) 2017-04-12
HUE035678T2 (en) 2018-05-28
EP2828235B1 (en) 2017-11-22
EP2828235A1 (en) 2015-01-28
US20160376228A1 (en) 2016-12-29
CN110437108A (en) 2019-11-12
JP2015514065A (en) 2015-05-18

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