GB1165831A - Process for the Production of Isocyanates and Carbamyl Chlorides - Google Patents
Process for the Production of Isocyanates and Carbamyl ChloridesInfo
- Publication number
- GB1165831A GB1165831A GB396167A GB396167A GB1165831A GB 1165831 A GB1165831 A GB 1165831A GB 396167 A GB396167 A GB 396167A GB 396167 A GB396167 A GB 396167A GB 1165831 A GB1165831 A GB 1165831A
- Authority
- GB
- United Kingdom
- Prior art keywords
- reactor
- isocyanates
- isocyanate
- carbamyl chlorides
- jan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1,165,831. Preparation of organic isocyanates and carbamyl chlorides. IMPERIAL CHEMICAL INDUSTRIES Ltd. 5 Jan., 1968 [26 Jan, 1967], No. 3961/67. Heading C2C. A process for the manufacture of organic isocyanates and carbamyl chlorides comprises reacting primary or secondary amines with phosgene in the vapour phase in a reactor provided with means for agitation of the vapours as they pass through the reactor, the process including a degassing stage when used for the manufacture of an isocyanate. Thus the reactor may be tubular and provided with a rapidly rotating shaft aligned centrally within, carrying blades, arms or sweeps which rotate about the central shaft. The amine vapour may be diluted with an inert gas e.g. nitrogen or with a vapourized inert solvent and the hot vapours emerging from the reactor, which is preferably at a temperature of from 160-300‹ C., are cooled by contact with a liquid cooling agent, preferably an inert organic solvent from which the isocyanate may subsequently be distilled. The preparation of p-tolyl isocyanate is described. A list of isocyanates prepared in this way is given.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB396167A GB1165831A (en) | 1967-01-26 | 1967-01-26 | Process for the Production of Isocyanates and Carbamyl Chlorides |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB396167A GB1165831A (en) | 1967-01-26 | 1967-01-26 | Process for the Production of Isocyanates and Carbamyl Chlorides |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1165831A true GB1165831A (en) | 1969-10-01 |
Family
ID=9768155
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB396167A Expired GB1165831A (en) | 1967-01-26 | 1967-01-26 | Process for the Production of Isocyanates and Carbamyl Chlorides |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1165831A (en) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0289840A1 (en) * | 1987-04-30 | 1988-11-09 | Bayer Ag | Process for the preparation of (cyclo)aliphatic diisocyanates |
EP0593334A1 (en) * | 1992-10-16 | 1994-04-20 | Rhone-Poulenc Chimie | Process for the preparation of aromatic isocyanate compounds in gazeous phase |
EP1275640A1 (en) | 2001-07-11 | 2003-01-15 | Bayer Ag | Process for the preparation of (cyclo)aliphatic isocyanates |
WO2008037173A1 (en) | 2006-09-28 | 2008-04-03 | Ningbo Wanhua Polyurethanes Co., Ltd. | A hole jet reactor and a process for the preparation of an isocyanate using the reactor |
EP2199277A1 (en) * | 2008-12-18 | 2010-06-23 | Bayer MaterialScience AG | Method for manufacturing isocyanates in the gaseous phase |
WO2011003532A1 (en) | 2009-07-09 | 2011-01-13 | Bayer Materialscience Ag | Method for producing isocyanates |
WO2013139703A1 (en) | 2012-03-19 | 2013-09-26 | Bayer Intellectual Property Gmbh | Method for producing isocyanates |
WO2016042124A1 (en) | 2014-09-19 | 2016-03-24 | Covestro Deutschland Ag | Method for producing isocyanates in the gas phase |
-
1967
- 1967-01-26 GB GB396167A patent/GB1165831A/en not_active Expired
Cited By (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0289840A1 (en) * | 1987-04-30 | 1988-11-09 | Bayer Ag | Process for the preparation of (cyclo)aliphatic diisocyanates |
US4847408A (en) * | 1987-04-30 | 1989-07-11 | Bayer Aktiengesellschaft | Process for the preparation of (cyclo)aliphatic diisocyanates |
EP0593334A1 (en) * | 1992-10-16 | 1994-04-20 | Rhone-Poulenc Chimie | Process for the preparation of aromatic isocyanate compounds in gazeous phase |
FR2697017A1 (en) * | 1992-10-16 | 1994-04-22 | Rhone Poulenc Chimie | Process for the preparation of compounds of the aromatic isocyanate type in the gas phase. |
US5391683A (en) * | 1992-10-16 | 1995-02-21 | Rhone-Poulenc Chimie | Preparation of aromatic polyisocyanates |
EP1275640A1 (en) | 2001-07-11 | 2003-01-15 | Bayer Ag | Process for the preparation of (cyclo)aliphatic isocyanates |
US6706913B2 (en) * | 2001-07-11 | 2004-03-16 | Bayer Aktiengesellschaft | Process for preparing (cyclo)aliphatic isocyanates |
AU2002300069B2 (en) * | 2001-07-11 | 2008-04-10 | Bayer Aktiengesellschaft | Process for preparing (cyclo)aliphatic isocyanates |
WO2008037173A1 (en) | 2006-09-28 | 2008-04-03 | Ningbo Wanhua Polyurethanes Co., Ltd. | A hole jet reactor and a process for the preparation of an isocyanate using the reactor |
US8333927B2 (en) | 2006-09-28 | 2012-12-18 | Ningbo Wanhua Polyurethanes Co., Ltd. | Hole jet reactor and a process for the preparation of an isocyanate using the reactor |
DE102008063728A1 (en) | 2008-12-18 | 2010-06-24 | Bayer Materialscience Ag | Process for the preparation of isocyanates in the gas phase |
EP2199277A1 (en) * | 2008-12-18 | 2010-06-23 | Bayer MaterialScience AG | Method for manufacturing isocyanates in the gaseous phase |
RU2528336C2 (en) * | 2008-12-18 | 2014-09-10 | Байер Матириальсайенс Аг | Method of obtaining primary isocyanates |
TWI464139B (en) * | 2008-12-18 | 2014-12-11 | Bayer Materialscience Ag | Process for the preparation of isocyanates in the gas phase |
WO2011003532A1 (en) | 2009-07-09 | 2011-01-13 | Bayer Materialscience Ag | Method for producing isocyanates |
DE102009032413A1 (en) | 2009-07-09 | 2011-01-13 | Bayer Materialscience Ag | Process for the preparation of isocyanates |
US8563768B2 (en) | 2009-07-09 | 2013-10-22 | Bayer Materialscience Ag | Process for the preparation of isocyanates |
WO2013139703A1 (en) | 2012-03-19 | 2013-09-26 | Bayer Intellectual Property Gmbh | Method for producing isocyanates |
US9593075B2 (en) | 2012-03-19 | 2017-03-14 | Covestro Deutschland Ag | Method for producing isocyanates |
US9695115B2 (en) | 2012-03-19 | 2017-07-04 | Covestro Deutschland Ag | Method for producing isocyanates |
WO2016042124A1 (en) | 2014-09-19 | 2016-03-24 | Covestro Deutschland Ag | Method for producing isocyanates in the gas phase |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLNP | Patent lapsed through nonpayment of renewal fees |