IN2014CN03665A - - Google Patents

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Publication number
IN2014CN03665A
IN2014CN03665A IN3665CHN2014A IN2014CN03665A IN 2014CN03665 A IN2014CN03665 A IN 2014CN03665A IN 3665CHN2014 A IN3665CHN2014 A IN 3665CHN2014A IN 2014CN03665 A IN2014CN03665 A IN 2014CN03665A
Authority
IN
India
Prior art keywords
ions
filtrate
dissolved
water soluble
aqueous solution
Prior art date
Application number
Other languages
English (en)
Inventor
Thomas H Neuman
Richard W Chastain
Donial M Felton
Daniel C Neuman
Otto C Schnauber
Original Assignee
Intercontinental Potash Corp Usa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Intercontinental Potash Corp Usa filed Critical Intercontinental Potash Corp Usa
Publication of IN2014CN03665A publication Critical patent/IN2014CN03665A/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0018Evaporation of components of the mixture to be separated
    • B01D9/0031Evaporation of components of the mixture to be separated by heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0059General arrangements of crystallisation plant, e.g. flow sheets
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D5/00Sulfates or sulfites of sodium, potassium or alkali metals in general

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
IN3665CHN2014 2011-11-14 2012-11-06 IN2014CN03665A (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201161559488P 2011-11-14 2011-11-14
PCT/US2012/063687 WO2013074328A1 (en) 2011-11-14 2012-11-06 Methods of processing polyhalite ore, methods of producing potassium sulfate, and related systems

Publications (1)

Publication Number Publication Date
IN2014CN03665A true IN2014CN03665A (ru) 2015-07-03

Family

ID=48280832

Family Applications (1)

Application Number Title Priority Date Filing Date
IN3665CHN2014 IN2014CN03665A (ru) 2011-11-14 2012-11-06

Country Status (6)

Country Link
US (1) US8551429B2 (ru)
EP (1) EP2780286A4 (ru)
CN (1) CN103930371B (ru)
CA (1) CA2855492A1 (ru)
IN (1) IN2014CN03665A (ru)
WO (1) WO2013074328A1 (ru)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IN2015KN00624A (ru) * 2012-09-12 2015-07-17 Intercontinental Potash Corp
WO2015016607A1 (en) * 2013-07-31 2015-02-05 Research Institute Of Industrial Science & Technology Apparatus for manufacturing potassium compound and method of recovering potassium compound from brine
CN103896683B (zh) * 2014-04-14 2015-09-30 国投新疆罗布泊钾盐有限责任公司 一种水溶性速溶硫酸钾肥料
GB2522492B (en) 2014-06-02 2020-07-15 York Potash Ltd Dry powder processing
GB2522490B (en) 2014-06-02 2015-12-09 Sirius Minerals Plc Fertiliser product
GB2530757B (en) 2014-09-30 2019-04-24 York Potash Ltd Pelletising process
CN105036156A (zh) * 2015-08-27 2015-11-11 莫红兵 一种硫酸钾晶体生长促进剂及其应用
CN105110352B (zh) * 2015-08-27 2017-01-04 莫红兵 一种以含钾、氯离子的固废物为原料生产硫酸钾的方法
CN105648239A (zh) * 2016-01-25 2016-06-08 化工部长沙设计研究院 一种杂卤石浸取可溶钾的工艺
CN106380233A (zh) * 2016-08-29 2017-02-08 化工部长沙设计研究院 一种用杂卤石制备钾镁肥的工艺
CN106379917B (zh) * 2016-08-29 2017-11-24 化工部长沙设计研究院 一种用杂卤石制备硫酸钾的工艺
JOP20170077B1 (ar) * 2016-09-13 2021-08-17 Veolia Water Tech Inc طريقة لإنتاج كبريتات البوتاسيوم من كلوريد البوتاسيوم و حمض كبريتيك
GB2560026A (en) 2017-02-27 2018-08-29 Sirius Minerals Plc Forming evaporite mineral products
GB2560025A (en) 2017-02-27 2018-08-29 Sirius Minerals Plc Forming evaporite mineral products
GB2560027B (en) 2017-02-27 2022-09-07 York Potash Ltd Forming evaporite mineral products
CN107522220A (zh) * 2017-09-05 2017-12-29 中国科学院青海盐湖研究所 一种杂卤石溶浸剂及其应用
DE102017010086A1 (de) 2017-10-30 2019-05-02 K+S Aktiengesellschaft Granulate, enthaltend Polyhalit
DE102017010085A1 (de) 2017-10-30 2019-05-02 K+S Aktiengesellschaft Verfahren zur Herstellung kalziniert-polyhalithaltiger Düngemittelgranulate
DE102017125467A1 (de) 2017-10-30 2019-05-02 K+S Aktiengesellschaft Verfahren zur Herstellung Kalium, Magnesium und Sulfat enthaltender Granulate
US20220298084A1 (en) * 2019-08-22 2022-09-22 Icl Europe Cooperatief U.A. Granules of polyhalite, potash and ammonium sulphate and a compaction process for the production thereof
GB2588601B (en) 2019-10-25 2023-11-01 Anglo American Woodsmith Ltd Composite fertiliser systems
CN111905400A (zh) * 2020-07-15 2020-11-10 浙江嘉化新材料有限公司 一种粗晶体重结晶装置
GB2602962A (en) 2020-12-23 2022-07-27 York Potash Ltd Manufacturing a composite fertiliser pellet
WO2024031139A1 (en) * 2022-08-11 2024-02-15 Reward Minerals Limited A process for recovering potassium sulphate

Family Cites Families (47)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1812497A (en) * 1927-06-22 1931-06-30 Humble Oil & Refining Company Recovery of potassium sulphate from polyhalite
US2020322A (en) * 1927-08-11 1935-11-12 Rita Vinay Process of treatment of complex materials containing potassium salts
US1794552A (en) * 1928-12-29 1931-03-03 Eugene P Schoch Process of recovering salts from minerals
US1924519A (en) * 1930-09-03 1933-08-29 Eugene P Schoch Treatment of minerals
US1952289A (en) * 1932-04-11 1934-03-27 Eugene P Schoch Process of extracting salts from minerals
US2033149A (en) 1934-07-18 1936-03-10 Usa Process for the recovery of potassium salts from minerals
US2902334A (en) 1953-01-29 1959-09-01 American Viscose Corp Coagulation of cellulosic colloids
US2862788A (en) 1955-05-03 1958-12-02 Int Minerals & Chem Corp Process for purifying impure solid-phase kainite
US2895794A (en) 1955-05-03 1959-07-21 Int Minerals & Chem Corp Process for recovering potassium values from kainite
US2860951A (en) * 1955-07-28 1958-11-18 Horizons Inc Recovery of values in naturally occurring alkali metal sulfate minerals
US3004826A (en) 1957-07-22 1961-10-17 Montedison Spa Process for obtaining schoenite by direct treatment of kainite containing sodium chloride as an impurity
US3058806A (en) 1959-01-16 1962-10-16 Metallgesellschaft Ag Method of preparing potassium sulfate from kainite
US3110561A (en) 1960-03-19 1963-11-12 Wintershall Ag Process for the production of potassium sulfate
DE1159414B (de) 1961-05-05 1963-12-19 Wintershall Ag Verfahren zur Herstellung von Kaliumsulfat
US3271106A (en) 1963-10-09 1966-09-06 Int Minerals & Chem Corp Production of potassium sulfate and potassium chloride
CH431576A (de) 1964-01-07 1967-03-15 Inventa Ag Verfahren zum Granulieren von stickstoffhaltigen Düngemitteln
US3528767A (en) 1966-03-16 1970-09-15 Donald E Garrett Production of potassium chloride,potassium sulfate and sodium sulfate from brines and the like containing potassium,chloride and sulfate
GB1183938A (en) 1966-09-21 1970-03-11 Fisons Ltd Prilling
US3630713A (en) 1968-07-22 1971-12-28 Duval Corp Method of producing fertilizer granules
US3634041A (en) 1969-02-14 1972-01-11 Great Salt Lake Minerals Method for the production of potassium sulfate from potassium-containing double salts of magnesium sulfate
US3617243A (en) 1970-03-23 1971-11-02 Great Salt Lake Minerals Process for the production of anhydrous potassium magnesium sulfate material with low hygroscopicity from hydrated potassium magnesium sulfate material
US3843772A (en) 1972-09-14 1974-10-22 Int Minerals & Chem Corp Production of white potassium sulfate crystals
US3926609A (en) 1974-04-18 1975-12-16 Kali & Salz Ag Granular mgo-containing potassium salt fertilizers and process for their manufacture
US4026696A (en) 1975-02-24 1977-05-31 Union Oil Company Of California Particulate multicomponent soil additive
US4045335A (en) 1976-03-10 1977-08-30 Duval Corporation Beneficiation of kieserite and langbeinite from a langbeinite ore
US4183738A (en) 1977-05-09 1980-01-15 International Fertilizer Development Center Granulation process and products produced thereby
US4306880A (en) 1978-09-22 1981-12-22 Garrett Donald E Recovering by-products from sea water brines and the like
DE2966435D1 (en) 1978-12-22 1983-12-29 Adelaide & Wallaroo Fertilizer Improvements in and relating to granulation
US4246019A (en) 1979-02-21 1981-01-20 Sokolov Igor D Method of producing a complex mineral fertilizer
NL184769C (nl) 1981-07-03 1989-11-01 Azote Sa Cie Neerlandaise Werkwijze voor het vervaardigen van ureumkorrels.
FR2523114A1 (fr) 1982-03-11 1983-09-16 Alsace Mines Potasse Procede de fabrication de sulfate de potassium a partir de solutions contenant du chlorure de magnesium et de chlorure de potassium
DE3332250C1 (de) 1983-09-07 1984-10-25 Kali Und Salz Ag, 3500 Kassel Verwendung einer Langbeinit-Trübe als Bindemittel
US4554151A (en) * 1983-09-27 1985-11-19 Prodeco, Inc. Process for producing K3 H(SO4)2 crystals and potassium sulfate crystals
DE3435124C2 (de) 1984-09-25 1987-03-05 Kali Und Salz Ag, 3500 Kassel Verfahren zur Herstellung von Kaliumchlorid mit über 55 Gew.-%K↓2↓O aus dem Feinzersetzungssalz der Carnallitzersetzung
US4815790A (en) 1988-05-13 1989-03-28 Natec, Ltd. Nahcolite solution mining process
US5078779A (en) 1988-12-01 1992-01-07 Martin Marietta Magnesia Specialties Inc. Binder for the granulation of fertilizers such as ammonium sulfate
US5246273A (en) 1991-05-13 1993-09-21 Rosar Edward C Method and apparatus for solution mining
ES2185924T3 (es) 1996-04-19 2003-05-01 Airborne Ind Minerals Inc Metodo de granulacion.
FI981490A (fi) 1998-06-29 1999-12-30 Kemira Agro Oy Menetelmä seoslannoitteiden valmistamiseksi
WO2000067550A1 (en) 1999-05-05 2000-11-16 Airborne Industrial Minerals Inc. Compost granulation method
WO2001062071A1 (en) 2000-02-23 2001-08-30 Encap, Llc Fortified mulch
US7611208B2 (en) 2004-08-17 2009-11-03 Sesqui Mining, Llc Methods for constructing underground borehole configurations and related solution mining methods
CA2542289A1 (en) 2005-04-07 2006-10-07 The Mosaic Company Use of urea-formaldehyde resin in potash ore processing
CN100360693C (zh) * 2005-09-08 2008-01-09 成都理工大学 对杂卤石矿中钾的溶浸开采方法
FI118598B (fi) 2006-05-17 2008-01-15 Kemira Growhow Oyj Lannoiterae ja menetelmä sen valmistamiseksi
DE102007058666B4 (de) * 2007-12-19 2010-11-25 K-Utec Ag Salt Technologies Verfahren zur Verarbeitung von Polyhalit zum Zweck der Herstellung von Langbeinit, Kaliumsulfat und Flüssigdünger
CN102596856A (zh) 2009-06-25 2012-07-18 Imitami院研发有限公司 自杂卤石制备商业级质量的硝酸钾的方法

Also Published As

Publication number Publication date
CA2855492A1 (en) 2013-05-23
WO2013074328A1 (en) 2013-05-23
CN103930371B (zh) 2016-09-14
US20130121900A1 (en) 2013-05-16
US8551429B2 (en) 2013-10-08
EP2780286A4 (en) 2015-08-12
CN103930371A (zh) 2014-07-16
EP2780286A1 (en) 2014-09-24

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