IL26677A - Mercapto-trithiomethylene and process for the preparation thereof - Google Patents
Mercapto-trithiomethylene and process for the preparation thereofInfo
- Publication number
- IL26677A IL26677A IL26677A IL2667766A IL26677A IL 26677 A IL26677 A IL 26677A IL 26677 A IL26677 A IL 26677A IL 2667766 A IL2667766 A IL 2667766A IL 26677 A IL26677 A IL 26677A
- Authority
- IL
- Israel
- Prior art keywords
- process according
- solution
- mercapto
- maintained
- hcho
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 28
- 238000002360 preparation method Methods 0.000 title claims description 11
- -1 Mercapto-trithiomethylene Chemical group 0.000 title claims description 10
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 75
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 20
- 239000000126 substance Substances 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- 150000001875 compounds Chemical class 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 239000005864 Sulphur Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 235000019256 formaldehyde Nutrition 0.000 description 17
- 239000000047 product Substances 0.000 description 14
- 238000006243 chemical reaction Methods 0.000 description 11
- 239000007787 solid Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- DBTDEFJAFBUGPP-UHFFFAOYSA-N Methanethial Chemical compound S=C DBTDEFJAFBUGPP-UHFFFAOYSA-N 0.000 description 4
- 239000008098 formaldehyde solution Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000012429 reaction media Substances 0.000 description 3
- BVOMRRWJQOJMPA-UHFFFAOYSA-N 1,2,3-trithiane Chemical compound C1CSSSC1 BVOMRRWJQOJMPA-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000001923 cyclic compounds Chemical class 0.000 description 2
- 239000012263 liquid product Substances 0.000 description 2
- INBDPOJZYZJUDA-UHFFFAOYSA-N methanedithiol Chemical compound SCS INBDPOJZYZJUDA-UHFFFAOYSA-N 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 1
- 241001408449 Asca Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- PXQLVRUNWNTZOS-UHFFFAOYSA-N sulfanyl Chemical class [SH] PXQLVRUNWNTZOS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR36187A FR1465475A (fr) | 1965-10-26 | 1965-10-26 | Mercapto trithiométhylène et sa préparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IL26677A true IL26677A (en) | 1970-09-17 |
Family
ID=8591184
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL26677A IL26677A (en) | 1965-10-26 | 1966-10-12 | Mercapto-trithiomethylene and process for the preparation thereof |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3509219A (enExample) |
| AT (1) | AT266806B (enExample) |
| BE (1) | BE688826A (enExample) |
| CH (1) | CH459989A (enExample) |
| DE (1) | DE1268615B (enExample) |
| ES (1) | ES332236A1 (enExample) |
| FR (1) | FR1465475A (enExample) |
| GB (1) | GB1162145A (enExample) |
| IL (1) | IL26677A (enExample) |
| NL (1) | NL6614606A (enExample) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1991765A (en) * | 1932-01-23 | 1935-02-19 | Dupont Viscoloid Company | Aldehyde-hydrogen sulphide reaction product |
| US3056841A (en) * | 1961-09-06 | 1962-10-02 | Du Pont | Process for preparing mercapto-terminated thiomethylene compounds |
| FR1362500A (fr) * | 1963-03-21 | 1964-06-05 | Aquitaine Petrole | Polythioformaldéhydes liquides |
-
1965
- 1965-10-26 FR FR36187A patent/FR1465475A/fr not_active Expired
-
1966
- 1966-10-10 GB GB45124/66A patent/GB1162145A/en not_active Expired
- 1966-10-12 US US586038A patent/US3509219A/en not_active Expired - Lifetime
- 1966-10-12 IL IL26677A patent/IL26677A/en unknown
- 1966-10-12 CH CH1473066A patent/CH459989A/fr unknown
- 1966-10-14 ES ES0332236A patent/ES332236A1/es not_active Expired
- 1966-10-14 DE DEP1268A patent/DE1268615B/de active Pending
- 1966-10-18 NL NL6614606A patent/NL6614606A/xx unknown
- 1966-10-24 AT AT989266A patent/AT266806B/de active
- 1966-10-25 BE BE688826D patent/BE688826A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GB1162145A (en) | 1969-08-20 |
| AT266806B (de) | 1968-12-10 |
| ES332236A1 (es) | 1967-07-16 |
| CH459989A (fr) | 1968-07-31 |
| BE688826A (enExample) | 1967-04-25 |
| US3509219A (en) | 1970-04-28 |
| FR1465475A (fr) | 1967-01-13 |
| DE1268615B (de) | 1968-05-22 |
| NL6614606A (enExample) | 1967-04-27 |
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