IL26281A - Preparation of polyboric esters - Google Patents
Preparation of polyboric estersInfo
- Publication number
- IL26281A IL26281A IL26281A IL2628166A IL26281A IL 26281 A IL26281 A IL 26281A IL 26281 A IL26281 A IL 26281A IL 2628166 A IL2628166 A IL 2628166A IL 26281 A IL26281 A IL 26281A
- Authority
- IL
- Israel
- Prior art keywords
- polyboric
- esters
- acid
- reaction
- alcohol
- Prior art date
Links
- 150000002148 esters Chemical class 0.000 title claims description 9
- 238000002360 preparation method Methods 0.000 title claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 238000006243 chemical reaction Methods 0.000 claims description 16
- 239000002253 acid Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 7
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 5
- 239000000725 suspension Substances 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 4
- 230000018044 dehydration Effects 0.000 claims description 4
- 238000006297 dehydration reaction Methods 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 2
- 238000005292 vacuum distillation Methods 0.000 claims description 2
- 150000002989 phenols Chemical class 0.000 claims 1
- 235000019441 ethanol Nutrition 0.000 description 15
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical group [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 9
- 229910052796 boron Inorganic materials 0.000 description 7
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 7
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 3
- 150000008064 anhydrides Chemical class 0.000 description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- -1 alkyl borates Chemical class 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/02—Boron compounds
- C07F5/04—Esters of boric acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Measuring Volume Flow (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT1824965 | 1965-08-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IL26281A true IL26281A (en) | 1970-05-21 |
Family
ID=11152471
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL26281A IL26281A (en) | 1965-08-11 | 1966-08-07 | Preparation of polyboric esters |
Country Status (11)
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5984241A (ja) * | 1982-11-05 | 1984-05-15 | Fuji Photo Film Co Ltd | 感光性平版印刷版の現像液 |
| US4519926A (en) * | 1983-02-18 | 1985-05-28 | Standard Oil Company (Indiana) | Polyborate esters and their use in lubricants |
-
1966
- 1966-08-05 NL NL6611060A patent/NL6611060A/xx unknown
- 1966-08-07 IL IL26281A patent/IL26281A/en unknown
- 1966-08-08 LU LU51718A patent/LU51718A1/xx unknown
- 1966-08-08 GB GB35478/66A patent/GB1156980A/en not_active Expired
- 1966-08-09 BE BE685288D patent/BE685288A/xx unknown
- 1966-08-09 NO NO164241A patent/NO122242B/no unknown
- 1966-08-10 CH CH1150766A patent/CH484196A/de not_active IP Right Cessation
- 1966-08-10 DE DE1593060A patent/DE1593060C3/de not_active Expired
- 1966-08-10 ES ES0330514A patent/ES330514A1/es not_active Expired
- 1966-08-11 SE SE10863/66A patent/SE336778B/xx unknown
-
1970
- 1970-02-10 US US00009118A patent/US3755408A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| GB1156980A (en) | 1969-07-02 |
| SE336778B (US06252093-20010626-C00008.png) | 1971-07-19 |
| CH484196A (de) | 1970-01-15 |
| DE1593060C3 (de) | 1975-07-17 |
| DE1593060A1 (de) | 1970-04-16 |
| NO122242B (US06252093-20010626-C00008.png) | 1971-06-07 |
| BE685288A (US06252093-20010626-C00008.png) | 1967-01-16 |
| DE1593060B2 (US06252093-20010626-C00008.png) | 1974-11-14 |
| US3755408A (en) | 1973-08-28 |
| LU51718A1 (US06252093-20010626-C00008.png) | 1966-10-10 |
| ES330514A1 (es) | 1967-06-16 |
| NL6611060A (US06252093-20010626-C00008.png) | 1967-02-13 |
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