HUP9803026A2 - Eljárás L-aszparaginsav előállítására - Google Patents
Eljárás L-aszparaginsav előállításáraInfo
- Publication number
- HUP9803026A2 HUP9803026A2 HU9803026A HUP9803026A HUP9803026A2 HU P9803026 A2 HUP9803026 A2 HU P9803026A2 HU 9803026 A HU9803026 A HU 9803026A HU P9803026 A HUP9803026 A HU P9803026A HU P9803026 A2 HUP9803026 A2 HU P9803026A2
- Authority
- HU
- Hungary
- Prior art keywords
- acid
- aspartic acid
- acetic acid
- producing
- reaction
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- CKLJMWTZIZZHCS-UHFFFAOYSA-N D-OH-Asp Natural products OC(=O)C(N)CC(O)=O CKLJMWTZIZZHCS-UHFFFAOYSA-N 0.000 title 1
- CKLJMWTZIZZHCS-UWTATZPHSA-N L-Aspartic acid Natural products OC(=O)[C@H](N)CC(O)=O CKLJMWTZIZZHCS-UWTATZPHSA-N 0.000 title 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 title 1
- 229960005261 aspartic acid Drugs 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 9
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 4
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 abstract 4
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 abstract 3
- 235000019253 formic acid Nutrition 0.000 abstract 3
- 229910021529 ammonia Inorganic materials 0.000 abstract 2
- 239000001530 fumaric acid Substances 0.000 abstract 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 abstract 2
- 239000001729 Ammonium fumarate Substances 0.000 abstract 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 235000019297 ammonium fumarate Nutrition 0.000 abstract 1
- 239000000908 ammonium hydroxide Substances 0.000 abstract 1
- CKKXWJDFFQPBQL-SEPHDYHBSA-N azane;(e)-but-2-enedioic acid Chemical compound N.N.OC(=O)\C=C\C(O)=O CKKXWJDFFQPBQL-SEPHDYHBSA-N 0.000 abstract 1
- 238000006555 catalytic reaction Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000012452 mother liquor Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P13/00—Preparation of nitrogen-containing organic compounds
- C12P13/04—Alpha- or beta- amino acids
- C12P13/20—Aspartic acid; Asparagine
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biotechnology (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Microbiology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Peptides Or Proteins (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
Abstract
A találmány tárgya javított eljárás I-aszparaginsav előállításárafumársavnak ammónium-hidroxiddal, enzimmel katalizált reagáltatásaútján, melynek során a reakció befejezése után a reakcióelegyből azammóniafelesleget eltávolítják, az I-aszparaginsavat ecetsav vagyhangyasav hozzáadásával kicsapják, majd az anyalúgból fumársavhozzáadásával a hangyasavat és az ecetsavat újra felszabadítják és alehasított ammóniát, valamint a felszabadított hangyasavat, ecetsavatés a felszabadításnál képződött ammónium-fumarátot a következőciklusokban ismét felhasználják. Ó
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AT0219197A AT407050B (de) | 1997-12-29 | 1997-12-29 | Verfahren zur herstellung von l-asparaginsäure |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| HU9803026D0 HU9803026D0 (en) | 1999-02-01 |
| HUP9803026A2 true HUP9803026A2 (hu) | 2001-11-28 |
| HU221639B1 HU221639B1 (hu) | 2002-12-28 |
Family
ID=3529668
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HU9803026A HU221639B1 (hu) | 1997-12-29 | 1998-12-28 | Eljárás L-aszparaginsav előállítására |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US5952206A (hu) |
| EP (1) | EP0931838B1 (hu) |
| AT (2) | AT407050B (hu) |
| CZ (1) | CZ412598A3 (hu) |
| DE (1) | DE59803064D1 (hu) |
| DK (1) | DK0931838T3 (hu) |
| ES (1) | ES2172081T3 (hu) |
| HR (1) | HRP980643B1 (hu) |
| HU (1) | HU221639B1 (hu) |
| PT (1) | PT931838E (hu) |
| SK (1) | SK282923B6 (hu) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT408755B (de) * | 1998-05-22 | 2002-03-25 | Dsm Fine Chem Austria Gmbh | Verfahren zur herstellung von l-asparaginsäure |
| DE10108225A1 (de) * | 2001-02-21 | 2002-10-10 | Basf Ag | Verfahren zur Herstellung von D-Pantothensäure und/oder deren Salze als Zusatz zu Tierfuttermitteln |
| JP2004523237A (ja) * | 2001-02-21 | 2004-08-05 | ビーエーエスエフ アクチェンゲゼルシャフト | 動物飼料添加剤としてのｄ−パントテン酸および／またはその塩の製造方法 |
| DE10108223A1 (de) * | 2001-02-21 | 2002-10-10 | Basf Ag | Verfahren zur Herstellung von D-Pantothensäure und/oder deren Salze als Zusatz zu Tierfuttermitteln |
| PL364087A1 (en) * | 2001-02-21 | 2004-12-13 | Basf Aktiengesellschaft | Method for the production of d-pantothenic acid and/or salts thereof as adjunct for animal feedstuffs |
| DE102004027022A1 (de) * | 2004-06-02 | 2006-01-05 | Basf Ag | Verfahren zur Abtrennung von Ammoniak und Wasser aus Lactam-haltigen Gemischen |
| CN110016137A (zh) * | 2019-03-21 | 2019-07-16 | 河北协同环保科技股份有限公司 | 一种天冬氨酸制备过程产生母液的处理方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5626196A (en) * | 1979-08-10 | 1981-03-13 | Mitsubishi Petrochem Co Ltd | Preparation of l-aspartic acid |
| US4560653A (en) * | 1983-06-06 | 1985-12-24 | W. R. Grace & Co. | Process for preparing L-aspartic acid |
| JPS59232088A (ja) * | 1983-06-15 | 1984-12-26 | Tanabe Seiyaku Co Ltd | Ｌ−アスパラギン酸の製法 |
| JP2804005B2 (ja) * | 1994-05-20 | 1998-09-24 | 株式会社日本触媒 | Ｌ−アスパラギン酸の製造方法 |
| JP2664648B2 (ja) * | 1994-05-20 | 1997-10-15 | 株式会社日本触媒 | Ｌ−アスパラギン酸の製造方法 |
| WO1996017950A1 (fr) * | 1994-12-09 | 1996-06-13 | Mitsubishi Chemical Corporation | Procede de production d'acide l-aspartique |
-
1997
- 1997-12-29 AT AT0219197A patent/AT407050B/de not_active IP Right Cessation
-
1998
- 1998-12-14 CZ CZ984125A patent/CZ412598A3/cs unknown
- 1998-12-18 SK SK1763-98A patent/SK282923B6/sk unknown
- 1998-12-22 EP EP98124397A patent/EP0931838B1/de not_active Expired - Lifetime
- 1998-12-22 ES ES98124397T patent/ES2172081T3/es not_active Expired - Lifetime
- 1998-12-22 AT AT98124397T patent/ATE213270T1/de not_active IP Right Cessation
- 1998-12-22 PT PT98124397T patent/PT931838E/pt unknown
- 1998-12-22 DK DK98124397T patent/DK0931838T3/da active
- 1998-12-22 DE DE59803064T patent/DE59803064D1/de not_active Expired - Fee Related
- 1998-12-28 HU HU9803026A patent/HU221639B1/hu not_active IP Right Cessation
- 1998-12-29 US US09/222,350 patent/US5952206A/en not_active Expired - Fee Related
- 1998-12-29 HR HR980643A patent/HRP980643B1/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| ES2172081T3 (es) | 2002-09-16 |
| US5952206A (en) | 1999-09-14 |
| EP0931838B1 (de) | 2002-02-13 |
| DE59803064D1 (de) | 2002-03-21 |
| ATE213270T1 (de) | 2002-02-15 |
| SK176398A3 (en) | 1999-07-12 |
| CZ412598A3 (cs) | 1999-07-14 |
| PT931838E (pt) | 2002-05-31 |
| HRP980643A2 (en) | 1999-10-31 |
| AT407050B (de) | 2000-11-27 |
| HU221639B1 (hu) | 2002-12-28 |
| SK282923B6 (sk) | 2003-01-09 |
| DK0931838T3 (da) | 2002-04-02 |
| HU9803026D0 (en) | 1999-02-01 |
| ATA219197A (de) | 2000-04-15 |
| EP0931838A3 (de) | 1999-11-24 |
| EP0931838A2 (de) | 1999-07-28 |
| HRP980643B1 (en) | 2001-08-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ATE241343T1 (de) | Verfahren zur herstellung von transdermalen therapeutischen systemen unter verwendung von basischen alkalimetallsalzen zur umwandlung von wirkstoffsalzen in die freien basen | |
| HK1042483A1 (en) | Method for the production of thiazolidin | |
| HUP0002032A2 (hu) | Eljárás amino-karbonsavak előállítására | |
| HUP9803026A2 (hu) | Eljárás L-aszparaginsav előállítására | |
| HUP0201152A2 (hu) | Eljárás nem proteinogén L-aminosavak előállítására | |
| DE69808086D1 (de) | Ein verfahren zur herstellung von 1,4,7,10-tetraazacyclododecan-1,4,7-triessigsäure und deren derivaten | |
| CY1112047T1 (el) | Διαδικασια για την παρασκευη γκαμπαπεντινης | |
| ATE207861T1 (de) | Verfahren zur herstellung von tetrabrombisphenol- a | |
| BG103857A (en) | Method for the preparation of sertindol | |
| ATE66465T1 (de) | Verfahren zur herstellung von iminodiacetonitril. | |
| ATE339400T1 (de) | Verfahren zur herstellung von 1-(aminomethyl) cyclohexanessigsäure | |
| EP1336603A4 (en) | METHOD OF INTRODUCING AMINO GROSSPS AND METHOD FOR SYNTHESIS OF AMINO ACIDS | |
| DE69709952D1 (de) | Verbessertes verfahren zur herstellung von l-asparaginsäure | |
| HUP9901699A2 (hu) | Eljárás L-aszparaginsav előállítására | |
| HUP0303352A2 (hu) | Javított eljárás gabapentin intermedier előállítására | |
| SE8502315D0 (sv) | Improved transamination process for producing amino acids | |
| DE69905880T2 (de) | Verfahren zur herstellung von hydrazinhydrat | |
| ATE301637T1 (de) | Verfahren zur herstellung von n-geschützten azetidin-2-carbonsäuren | |
| ATE431820T1 (de) | Verfahren zur herstellung von 4-amino-5-chlor-1- phenylpyridazinon | |
| MY122674A (en) | Method for the production of polyamides | |
| HUP0302864A2 (hu) | Eljárás enantiomerben dúsított aminosavak előállítására | |
| ATE376984T1 (de) | Verfahren und vorrichtung zur herstellung von harnstoff | |
| ATE418535T1 (de) | Verbessertes verfahren zur herstellung von gabapentin | |
| HUP9900215A2 (hu) | Eljárás Z-L-aszparaginsav-dinátriumsó előállítására fumársavból | |
| DE50001638D1 (de) | Verfahren zur herstellung von 4,6-dichlorpyrimidin |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| HMM4 | Cancellation of final prot. due to non-payment of fee |