HRP20200365T1 - Postupak povećavanja brzine nastajanja produkta reakcije karboksilne kiseline s ureom dodavanjem kiseline - Google Patents
Postupak povećavanja brzine nastajanja produkta reakcije karboksilne kiseline s ureom dodavanjem kiseline Download PDFInfo
- Publication number
- HRP20200365T1 HRP20200365T1 HRP20200365TT HRP20200365T HRP20200365T1 HR P20200365 T1 HRP20200365 T1 HR P20200365T1 HR P20200365T T HRP20200365T T HR P20200365TT HR P20200365 T HRP20200365 T HR P20200365T HR P20200365 T1 HRP20200365 T1 HR P20200365T1
- Authority
- HR
- Croatia
- Prior art keywords
- acid
- substituted
- reaction product
- formulation
- group
- Prior art date
Links
- 239000002253 acid Substances 0.000 title claims 9
- 239000007795 chemical reaction product Substances 0.000 title claims 7
- 238000000034 method Methods 0.000 title claims 7
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title claims 5
- 239000004202 carbamide Substances 0.000 title claims 5
- 230000015572 biosynthetic process Effects 0.000 title claims 2
- 230000002708 enhancing effect Effects 0.000 title 1
- 238000009472 formulation Methods 0.000 claims 9
- 239000000203 mixture Substances 0.000 claims 9
- 125000000217 alkyl group Chemical group 0.000 claims 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 4
- 125000004432 carbon atom Chemical group C* 0.000 claims 4
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 4
- 229910052739 hydrogen Inorganic materials 0.000 claims 4
- 239000001257 hydrogen Substances 0.000 claims 4
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical group [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- 150000004820 halides Chemical class 0.000 claims 3
- 150000002431 hydrogen Chemical class 0.000 claims 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 3
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical group CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- 235000019253 formic acid Nutrition 0.000 claims 2
- 239000003002 pH adjusting agent Substances 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims 2
- 229920002554 vinyl polymer Polymers 0.000 claims 2
- BMYNFMYTOJXKLE-UHFFFAOYSA-N 3-azaniumyl-2-hydroxypropanoate Chemical compound NCC(O)C(O)=O BMYNFMYTOJXKLE-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 125000003545 alkoxy group Chemical group 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 150000001413 amino acids Chemical class 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
- 229910001507 metal halide Inorganic materials 0.000 claims 1
- 150000005309 metal halides Chemical class 0.000 claims 1
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 claims 1
- DWTMJZUGKDTNRU-UHFFFAOYSA-N n-(formylcarbamoyl)formamide Chemical compound O=CNC(=O)NC=O DWTMJZUGKDTNRU-UHFFFAOYSA-N 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 230000008635 plant growth Effects 0.000 claims 1
- 229920000137 polyphosphoric acid Polymers 0.000 claims 1
- 125000004385 trihaloalkyl group Chemical group 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
- C07C273/1854—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety
- C07C273/1863—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety from urea
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C275/00—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C275/46—Derivatives of urea, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups containing any of the groups, X being a hetero atom, Y being any atom, e.g. acylureas
- C07C275/48—Y being a hydrogen or a carbon atom
- C07C275/50—Y being a hydrogen or an acyclic carbon atom
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Claims (12)
1. Postupak dobivanja produkta reakcije povećanom brzinom nastajanja, naznačen time što se sastoji u
osiguravanju otopine koja sadrži karboksilnu kiselinu i ureu;
dodavanju najmanje jedne kiseline u navedenu otopinu kako bi se dobilo produkt reakcije koji ima formulu
[image]
,
gdje su R1 i R2 isti ili različiti i bira ih se iz skupine koju čine vodik ili supstituirani i nesupstituirani alkil, a R3 i R4 su isti ili različiti i bira ih se iz skupine koju čine vodik, supstituirane i nesupstituirane alkilne, alilne, vinilne i alkoksilne skupine s od 1-6 atoma ugljika, supstituirane i nesupstituirane fenilne skupine i halogenidi.
2. Postupak u skladu s patentnim zahtjevom 1, naznačen time što je navedena karboksilna kiselina mravlja kiselina.
3. Postupak u skladu s patentnim zahtjevom 1, naznačen time što navedena karboksilna kiselina ima formulu RCOOH, gdje se R bira iz skupine koju čine vodik, supstituirane i nesupstituirane alkilne, alilne, vinilne i alkoksilne skupine s od 1 do 6 atoma ugljika, supstituirane i nesupstituirane fenilne skupine i halogenidi.
4. Postupak u skladu s bilo kojim od patentnih zahtjeva 1-3, naznačen time što navedena urea ima formulu (NHR′)2CO, gdje je svaki R′ isti ili različiti i bira se iz skupine koju čine vodik, supstituirane i nesupstituirane alkilne skupine s od 1 do 6 atoma ugljika, supstituirane i nesupstituirane alkoksilne skupine s od 1 do 6 atoma ugljika, supstituirane i nesupstituirane fenilne skupine i halogenidi.
5. Postupak u skladu s bilo kojim od patentnih zahtjeva 1-4, naznačen time što navedena otopina sadrži 0,1-20%, težinski, navedene najmanje jedne kiseline; ili
što navedena otopina sadrži 0,1-10%, težinski, navedene najmanje jedne kiseline.
6. Postupak u skladu s bilo kojim od patentnih zahtjeva 1-5, naznačen time što se N,N′-diformilureu kao produkt reakcije dobiva osiguravanjem otopine koja sadrži mravlju kiselinu kao navedenu karboksilnu kiselinu i ureu kao navedenu ureu.
7. Formulacija za poboljšavanje rasta biljaka
naznačena time što sadrži najmanje jedno otapalo i
navedeni produkt reakcije u skladu s bilo kojim od patentnih zahtjeva 1-6, gdje navedena formulacija ne sadrži ikakve modifikatore pH koji su spojevi koji sadrže hidroksid.
8. Formulacija u skladu s patentnim zahtjevom 7, naznačena time što je navedeni modifikator pH kalijev hidroksid.
9. Formulacija u skladu s bilo kojim od patentnih zahtjeva 7 ili 8, naznačena time što je navedeno najmanje jedno otapalo N-metilpirolidon (NMP).
10. Formulacija u skladu s bilo kojim od patentnih zahtjeva 7-9, naznačena time što
navedena formulacija sadrži 0,001-1,0 M produkta reakcije; ili
što navedena formulacija sadrži 0,001-0,050 M produkta reakcije.
11. Formulacija u skladu s bilo kojim od patentnih zahtjeva 7-10, naznačena time što se navedenu najmanje jednu kiselinu bira iz skupine koju čine sumporna kiselina, sulfaminska kiselina, klorovodična kiselina, bromovodična kiselina, fluorovodična kiselina, dušična kiselina, fosforna kiselina, polifosforna kiselina, metalni halogenidi, alkil- i arilsulfonske kiseline, aminokiseline, trihalogenalkil kiseline, te organotitanati.
12. Formulacija u skladu s bilo kojim od patentnih zahtjeva 7-10, naznačena time što je navedena najmanje jedna kiselina sumporna kiselina.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201462098180P | 2014-12-30 | 2014-12-30 | |
PCT/US2015/067992 WO2016109622A1 (en) | 2014-12-30 | 2015-12-30 | Method for enhancing the rate of the formation of the reaction product of a carboylic acid and a urea via acid addition |
EP15876223.7A EP3240774B1 (en) | 2014-12-30 | 2015-12-30 | Method for enhancing the rate of the formation of the reaction product of a carboylic acid and a urea via acid addition |
Publications (1)
Publication Number | Publication Date |
---|---|
HRP20200365T1 true HRP20200365T1 (hr) | 2020-08-21 |
Family
ID=56163422
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HRP20200365TT HRP20200365T1 (hr) | 2014-12-30 | 2020-03-04 | Postupak povećavanja brzine nastajanja produkta reakcije karboksilne kiseline s ureom dodavanjem kiseline |
Country Status (24)
Country | Link |
---|---|
US (1) | US9920001B2 (hr) |
EP (1) | EP3240774B1 (hr) |
KR (1) | KR102654043B1 (hr) |
CN (1) | CN107108484B (hr) |
AR (1) | AR103335A1 (hr) |
AU (1) | AU2015374094B2 (hr) |
CA (1) | CA2962148C (hr) |
CL (1) | CL2017000861A1 (hr) |
CO (1) | CO2017004933A2 (hr) |
CR (1) | CR20170295A (hr) |
EC (1) | ECSP17035769A (hr) |
ES (1) | ES2776426T3 (hr) |
HR (1) | HRP20200365T1 (hr) |
HU (1) | HUE047943T2 (hr) |
LT (1) | LT3240774T (hr) |
MX (1) | MX2017008810A (hr) |
NI (1) | NI201700084A (hr) |
PE (1) | PE20171065A1 (hr) |
PH (1) | PH12017501227A1 (hr) |
PL (1) | PL3240774T3 (hr) |
PT (1) | PT3240774T (hr) |
RS (1) | RS60620B1 (hr) |
WO (1) | WO2016109622A1 (hr) |
ZA (1) | ZA201704904B (hr) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110372541A (zh) * | 2019-07-26 | 2019-10-25 | 南通市争妍新材料科技有限公司 | 一种羧酸和尿素高效固相合成酰胺衍生物的方法 |
CN115024389A (zh) * | 2022-07-06 | 2022-09-09 | 青岛元农生物科技有限公司 | 一种缓释非蛋白氮添加剂及其制备和使用方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DD87780A (hr) | 1971-11-17 | 1972-11-12 | ||
US773251A (en) * | 1903-03-09 | 1904-10-25 | Firm Of E Merck | Ureide of dialkyl-acetic and process of making same. |
ES2243993T3 (es) * | 1996-04-10 | 2005-12-01 | Stoller Enterprises, Inc. | Diformilurea y productos de reaccion de urea y acidos carboxilicos. |
US6040273A (en) * | 1997-04-09 | 2000-03-21 | Stoller Enterprises, Inc. | Diformylurea and reaction products of urea and carboxylic acids |
EP2185505A2 (en) | 2007-06-25 | 2010-05-19 | Yissum Research Development Company of the Hebrew University of Jerusalem Ltd | Acyl-urea derivatives and uses thereof |
JP6117226B2 (ja) * | 2011-11-03 | 2017-04-19 | バイエル クロップサイエンス エルピーBayer Cropscience Lp | 植物の質を向上させるための組成物及び方法 |
-
2015
- 2015-12-30 MX MX2017008810A patent/MX2017008810A/es unknown
- 2015-12-30 RS RS20200158A patent/RS60620B1/sr unknown
- 2015-12-30 KR KR1020177021082A patent/KR102654043B1/ko active IP Right Grant
- 2015-12-30 EP EP15876223.7A patent/EP3240774B1/en active Active
- 2015-12-30 AU AU2015374094A patent/AU2015374094B2/en active Active
- 2015-12-30 CR CR20170295A patent/CR20170295A/es unknown
- 2015-12-30 PL PL15876223T patent/PL3240774T3/pl unknown
- 2015-12-30 AR ARP150104353A patent/AR103335A1/es active IP Right Grant
- 2015-12-30 LT LTEP15876223.7T patent/LT3240774T/lt unknown
- 2015-12-30 CN CN201580071463.XA patent/CN107108484B/zh active Active
- 2015-12-30 CA CA2962148A patent/CA2962148C/en active Active
- 2015-12-30 HU HUE15876223A patent/HUE047943T2/hu unknown
- 2015-12-30 PE PE2017000567A patent/PE20171065A1/es unknown
- 2015-12-30 ES ES15876223T patent/ES2776426T3/es active Active
- 2015-12-30 PT PT158762237T patent/PT3240774T/pt unknown
- 2015-12-30 US US14/984,049 patent/US9920001B2/en active Active
- 2015-12-30 WO PCT/US2015/067992 patent/WO2016109622A1/en active Application Filing
-
2017
- 2017-04-07 CL CL2017000861A patent/CL2017000861A1/es unknown
- 2017-05-17 CO CONC2017/0004933A patent/CO2017004933A2/es unknown
- 2017-06-08 EC ECIEPI201735769A patent/ECSP17035769A/es unknown
- 2017-06-26 NI NI201700084A patent/NI201700084A/es unknown
- 2017-06-30 PH PH12017501227A patent/PH12017501227A1/en unknown
- 2017-07-19 ZA ZA2017/04904A patent/ZA201704904B/en unknown
-
2020
- 2020-03-04 HR HRP20200365TT patent/HRP20200365T1/hr unknown
Also Published As
Publication number | Publication date |
---|---|
HUE047943T2 (hu) | 2020-05-28 |
EP3240774A1 (en) | 2017-11-08 |
US9920001B2 (en) | 2018-03-20 |
US20160185715A1 (en) | 2016-06-30 |
PE20171065A1 (es) | 2017-07-21 |
CO2017004933A2 (es) | 2017-07-28 |
WO2016109622A1 (en) | 2016-07-07 |
CL2017000861A1 (es) | 2017-11-10 |
KR102654043B1 (ko) | 2024-04-02 |
PT3240774T (pt) | 2020-03-10 |
AU2015374094A1 (en) | 2017-04-27 |
RS60620B1 (sr) | 2020-09-30 |
AU2015374094B2 (en) | 2020-07-16 |
CN107108484B (zh) | 2021-04-13 |
ECSP17035769A (es) | 2017-06-30 |
CA2962148C (en) | 2023-04-25 |
ZA201704904B (en) | 2018-12-19 |
PH12017501227B1 (en) | 2018-01-15 |
CN107108484A (zh) | 2017-08-29 |
LT3240774T (lt) | 2020-03-25 |
CR20170295A (es) | 2017-11-24 |
PL3240774T3 (pl) | 2020-06-29 |
MX2017008810A (es) | 2017-10-19 |
KR20170104143A (ko) | 2017-09-14 |
AR103335A1 (es) | 2017-05-03 |
ES2776426T3 (es) | 2020-07-30 |
EP3240774A4 (en) | 2018-08-15 |
NI201700084A (es) | 2017-07-18 |
CA2962148A1 (en) | 2016-07-07 |
PH12017501227A1 (en) | 2018-01-15 |
EP3240774B1 (en) | 2019-12-11 |
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