HRP20200063T1 - Mikroinkapsulirani pripravak inhibitora nitrifikacije - Google Patents
Mikroinkapsulirani pripravak inhibitora nitrifikacije Download PDFInfo
- Publication number
- HRP20200063T1 HRP20200063T1 HRP20200063TT HRP20200063T HRP20200063T1 HR P20200063 T1 HRP20200063 T1 HR P20200063T1 HR P20200063T T HRP20200063T T HR P20200063TT HR P20200063 T HRP20200063 T HR P20200063T HR P20200063 T1 HRP20200063 T1 HR P20200063T1
- Authority
- HR
- Croatia
- Prior art keywords
- microcapsules
- weight
- suspension formulation
- aqueous phase
- aromatics
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims 17
- 239000003112 inhibitor Substances 0.000 title 1
- 239000003094 microcapsule Substances 0.000 claims 19
- 238000009472 formulation Methods 0.000 claims 16
- 239000000725 suspension Substances 0.000 claims 13
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 claims 8
- 239000008346 aqueous phase Substances 0.000 claims 8
- 239000003849 aromatic solvent Substances 0.000 claims 4
- 239000001963 growth medium Substances 0.000 claims 4
- 239000007788 liquid Substances 0.000 claims 4
- 238000000034 method Methods 0.000 claims 4
- 239000000618 nitrogen fertilizer Substances 0.000 claims 4
- 239000012071 phase Substances 0.000 claims 4
- 229920002396 Polyurea Polymers 0.000 claims 2
- 239000003337 fertilizer Substances 0.000 claims 2
- 239000012948 isocyanate Substances 0.000 claims 2
- 150000002513 isocyanates Chemical class 0.000 claims 2
- DCUJJWWUNKIJPH-UHFFFAOYSA-N nitrapyrin Chemical compound ClC1=CC=CC(C(Cl)(Cl)Cl)=N1 DCUJJWWUNKIJPH-UHFFFAOYSA-N 0.000 claims 2
- 239000002245 particle Substances 0.000 claims 2
- 239000000575 pesticide Substances 0.000 claims 2
- 229920000538 Poly[(phenyl isocyanate)-co-formaldehyde] Polymers 0.000 claims 1
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 230000008635 plant growth Effects 0.000 claims 1
- 229920000768 polyamine Polymers 0.000 claims 1
- 238000006068 polycondensation reaction Methods 0.000 claims 1
- 229920000642 polymer Polymers 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000003381 stabilizer Substances 0.000 claims 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/10—Dispersions; Emulsions
- A61K9/107—Emulsions ; Emulsion preconcentrates; Micelles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/10—Dispersions; Emulsions
- A61K9/107—Emulsions ; Emulsion preconcentrates; Micelles
- A61K9/1075—Microemulsions or submicron emulsions; Preconcentrates or solids thereof; Micelles, e.g. made of phospholipids or block copolymers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
- C05G5/35—Capsules, e.g. core-shell
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/20—Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
- Y02P60/21—Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Health & Medical Sciences (AREA)
- Soil Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Epidemiology (AREA)
- Pharmacology & Pharmacy (AREA)
- Medicinal Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Plant Pathology (AREA)
- Biophysics (AREA)
- Molecular Biology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fertilizers (AREA)
- Pyridine Compounds (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Soil Conditioners And Soil-Stabilizing Materials (AREA)
- Peptides Or Proteins (AREA)
Claims (15)
1. Suspenzijska formulacija mikrokapsula, naznačena time što sadrži:
(a) suspendiranu fazu, gdje suspendirana faza sadrži više mikrokapsula, gdje mikrokapsule imaju srednjui volumnu veličinu čestica od 1 do 10 mikrometara, gdje mikrokapsule imaju:
(1) stijenku mikrokapsule proizvedenu reakcijom polikondenzacije na granici faza između polimernog izocijanata i poliamina kako bi se dobilo ljusku od poliuree težinskog postotka od 0,2 do 40 posto od ukupne težine suspenzijske formulacije mikrokapsula, i
(2) uglavnom tekuću jezgru, gdje je uglavnom tekuća jezgra inkapsulirana u ljusci od poliuree, gdje uglavnom tekuća jezgra sadrži 2-klor-6-(triklormetil)piridin, no najviše 60 težinskih postotaka od cijele mikrokapsule, te gdje na temperaturi od najmanje 15 °C uglavnom tekuća jezgra sadrži najviše 1,0 težinskih postotaka čvrstog 2-klor-6-(triklormetil)piridina; i
(b) vodenu fazu, gdje vodena faza sadrži najmanje 1,0 težinskih postotaka aromatskog otapala od ukupne težine suspenzijske formulacije mikrokapsula.
2. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 1, naznačena time što dodatno sadrži:
najmanje jedan ionski stabilizator prisutan u vodenoj fazi.
3. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 1, naznačena time što je aromatsko otapalo prisutno u vodenoj fazi najmnje jedan spoj kojeg se bira iz skupine koju čine: laki aromati, laki aromati osiromašeni naftalenom, teški aromati, te teški aromati osiromašeni naftalenom.
4. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 3, naznačena time što je aromatsko otapalo prisutno u vodenoj fazi teški C10-13 aromati ili teški C10-13 aromati osiromašeni naftalenom.
5. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 4, naznačena time što aromatsko otapalo prisutno u vodenoj fazi sadrži između otprilike 1%, težinski, i otprilike 10%, težinski, po mogućnosti između otprilike 2%, težinski, i otprilike 5%, težinski, i poželjnije između otprilike 2,5%, težinski, i otprilike 3,0%, težinski, teški C10-13 aromati odnosno teški C10-13 aromati osiromašeni naftalenom.
6. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 1, naznačena time što mikrokapsule imaju srednju volumnu veličinu čestica od 1 do otprilike 5 mikrometara.
7. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 1, naznačena time što se omjer između suspendirane faze a) i vodene faze b) kreće od 1:0,75 do 1:100.
8. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 1, naznačena time što se omjer između suspendirane faze a) i vodene faze b) kreće od otprilike 1:1 do otprilike 1:7, po mogućnosti od otprilike 1:1 do otprilike 1:4.
9. Suspenzijska formulacija mikrokapsula u skladu s patentnim zahtjevom 1, naznačena time što je polimerni izocijanat polimetilen-polifenilizocijanat.
10. Gnojivni pripravak, naznačen time što sadrži: dušično gnojivo i suspenzijsku formulaciju mikrokapsula u skladu s patentnim zahtjevom 1.
11. Gnojivni pripravak u skladu s patentnim zahtjevom 10, naznačen time što je dušično gnojivo urea–amonijev nitrat.
12. Postupak suprimiranja nitrifikacije amonijskog dušika u mediju za rast, naznačen time što se sastoji u koracima primjene suspenzijske formulacije mikrokapsula u skladu s patentnim zahtjevom 1 u medij za rast biljaka.
13. Postupak u skladu s patentnim zahtjevom 12, naznačen time što se formulaciju uključuje u medij za rast, ili primjenjuje na površinu medija za rast.
14. Postupak u skladu s patentnim zahtjevom 12, naznačen time što se formulaciju primjenjuje u kombinaciji s pesticidom ili nakon pesticida.
15. Postupak u skladu s patentnim zahtjevom 12, naznačen time što se formulaciju primjenjuje s dušičnim gnojivom, gdje je dušično gnojivo po mogućnosti urea–amonijev nitrat.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201461988056P | 2014-05-02 | 2014-05-02 | |
| PCT/US2015/028843 WO2015168593A1 (en) | 2014-05-02 | 2015-05-01 | Microencapsulated nitrification inhibitor composition |
| EP15785632.9A EP3137437B1 (en) | 2014-05-02 | 2015-05-01 | Microencapsulated nitrification inhibitor composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| HRP20200063T1 true HRP20200063T1 (hr) | 2020-04-03 |
Family
ID=54354723
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HRP20200063TT HRP20200063T1 (hr) | 2014-05-02 | 2020-01-16 | Mikroinkapsulirani pripravak inhibitora nitrifikacije |
Country Status (24)
| Country | Link |
|---|---|
| US (1) | US9862652B2 (hr) |
| EP (1) | EP3137437B1 (hr) |
| JP (1) | JP6572239B2 (hr) |
| KR (1) | KR102407375B1 (hr) |
| CN (1) | CN106458783B (hr) |
| AR (1) | AR100269A1 (hr) |
| AU (1) | AU2015252899B2 (hr) |
| BR (1) | BR112016025065B8 (hr) |
| CA (1) | CA2947161C (hr) |
| DK (1) | DK3137437T3 (hr) |
| ES (1) | ES2767524T3 (hr) |
| HR (1) | HRP20200063T1 (hr) |
| HU (1) | HUE047271T2 (hr) |
| IL (1) | IL248509B (hr) |
| LT (1) | LT3137437T (hr) |
| MX (1) | MX2016014020A (hr) |
| PL (1) | PL3137437T3 (hr) |
| PT (1) | PT3137437T (hr) |
| RS (1) | RS59849B1 (hr) |
| RU (1) | RU2689542C2 (hr) |
| SI (1) | SI3137437T1 (hr) |
| TW (1) | TWI654162B (hr) |
| UY (1) | UY36107A (hr) |
| WO (1) | WO2015168593A1 (hr) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX2017008450A (es) | 2014-12-31 | 2017-10-12 | Dow Agrosciences Llc | Composiciones inhibidoras de nitrificacion microencapsuladas. |
| EA201992200A1 (ru) * | 2017-03-17 | 2020-03-12 | ДАУ АГРОСАЙЕНСИЗ ЭлЭлСи | Микроинкапсулированные композиции ингибиторов нитрификации |
| CN107285968A (zh) * | 2017-07-25 | 2017-10-24 | 张忠庆 | 具有氮肥缓控释功能的微胶囊悬浮制剂及其制备方法和应用 |
| WO2019027634A1 (en) * | 2017-07-31 | 2019-02-07 | Dow Global Technologies Llc | ADDITIVE COMPOSITION AND METHOD |
| CN109665927B (zh) * | 2019-02-15 | 2021-11-19 | 金正大生态工程集团股份有限公司 | 一种稳定的硝化抑制剂及其制备方法与应用 |
| CN114423518A (zh) * | 2019-09-30 | 2022-04-29 | 富士胶片株式会社 | 微胶囊、微胶囊的制造方法 |
| CN112919981A (zh) * | 2021-04-13 | 2021-06-08 | 福建恒生态建筑工程有限公司 | 一种树枝与粪便堆肥的工艺 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3135594A (en) | 1961-09-01 | 1964-06-02 | Dow Chemical Co | Method and product for treating soil to suppress the nitrification of ammonium nitrogen therein |
| US4285720A (en) | 1972-03-15 | 1981-08-25 | Stauffer Chemical Company | Encapsulation process and capsules produced thereby |
| DE3147821A1 (de) * | 1981-12-03 | 1983-06-16 | Skw Trostberg Ag, 8223 Trostberg | Stabilisierte duengerloesungen |
| GB8325061D0 (en) | 1983-09-20 | 1983-10-19 | Dow Chemical Co | Microcapsules |
| US4563212A (en) * | 1983-12-27 | 1986-01-07 | Monsanto Company | High concentration encapsulation by interfacial polycondensation |
| US4640709A (en) * | 1984-06-12 | 1987-02-03 | Monsanto Company | High concentration encapsulation by interfacial polycondensation |
| US4677003A (en) | 1985-04-30 | 1987-06-30 | Rohm And Haas Company | Microsuspension process for preparing solvent core sequential polymer dispersion |
| US4936901A (en) * | 1986-07-09 | 1990-06-26 | Monsanto Company | Formulations of water-dispersible granules and process for preparation thereof |
| HU201869B (en) | 1988-12-30 | 1991-01-28 | Egyt Gyogyszervegyeszeti Gyar | Process for producing microcapsules of quick dissolving active component |
| CN1103540C (zh) * | 1993-11-15 | 2003-03-26 | 泽尼卡有限公司 | 含生物活性化合物悬浮液的微囊 |
| US5925464A (en) * | 1995-01-19 | 1999-07-20 | Dow Agrosciences Llc | Microencapsulation process and product |
| US6303552B1 (en) * | 1999-08-04 | 2001-10-16 | Napier International Technologies, Inc. | Aerosol paint stripper compositions |
| US6992047B2 (en) | 2001-04-11 | 2006-01-31 | Monsanto Technology Llc | Method of microencapsulating an agricultural active having a high melting point and uses for such materials |
| DE10223916A1 (de) | 2002-05-29 | 2003-12-11 | Bayer Cropscience Ag | Mikrokapsel-Formulierungen |
| GB0319071D0 (en) * | 2003-08-14 | 2003-09-17 | Avecia Ltd | Catalyst and process |
| US20050277549A1 (en) | 2004-06-14 | 2005-12-15 | Monsanto Technology Llc | Microcapsules having activated release of core material therein |
| WO2006006035A2 (en) * | 2004-06-30 | 2006-01-19 | United Phosphorus, Ltd. | A safe delivery system for agriculturally active material |
| WO2008091538A1 (en) * | 2007-01-22 | 2008-07-31 | Dow Agrosciences Llc | Enhanced nitrification inhibitor composition |
| US8741805B2 (en) * | 2007-01-22 | 2014-06-03 | Dow Agrosciences, Llc. | Enhanced nitrification inhibitor composition |
| BR112012031300A2 (pt) * | 2010-06-07 | 2015-09-22 | Dow Agrosciences Llc | "suspensões de microcápsulas incluindo altos níveis de ingredientes agricolamente ativos" |
| AU2012206618A1 (en) * | 2011-01-11 | 2013-07-25 | Basf Se | Agrochemical formulation comprising encapsulated pesticide |
| TWI556737B (zh) | 2011-02-11 | 2016-11-11 | 陶氏農業科學公司 | 改良的殺蟲劑配方 |
| CN102249817B (zh) * | 2011-04-21 | 2013-08-28 | 浙江奥复托化工有限公司 | 一种抑制土壤氮流失的制剂、制备方法及其应用 |
| BR102012027933A2 (pt) * | 2011-11-01 | 2015-11-17 | Dow Agrosciences Llc | composições pesticidas estáveis |
| CN103044137B (zh) * | 2012-12-26 | 2014-11-12 | 南通联农农药制剂研究开发有限公司 | 一种氮肥稳定剂组合物及其制备方法 |
| CN103202298A (zh) * | 2013-03-21 | 2013-07-17 | 江苏三迪化学有限公司 | 一种2-氯-6-三氯甲基吡啶微胶囊悬浮剂的制作方法 |
| MX2017008450A (es) * | 2014-12-31 | 2017-10-12 | Dow Agrosciences Llc | Composiciones inhibidoras de nitrificacion microencapsuladas. |
-
2015
- 2015-05-01 BR BR112016025065A patent/BR112016025065B8/pt active IP Right Grant
- 2015-05-01 JP JP2016565072A patent/JP6572239B2/ja active Active
- 2015-05-01 ES ES15785632T patent/ES2767524T3/es active Active
- 2015-05-01 DK DK15785632.9T patent/DK3137437T3/da active
- 2015-05-01 CN CN201580026973.5A patent/CN106458783B/zh active Active
- 2015-05-01 RU RU2016145913A patent/RU2689542C2/ru active
- 2015-05-01 AU AU2015252899A patent/AU2015252899B2/en active Active
- 2015-05-01 WO PCT/US2015/028843 patent/WO2015168593A1/en active Application Filing
- 2015-05-01 LT LTEP15785632.9T patent/LT3137437T/lt unknown
- 2015-05-01 CA CA2947161A patent/CA2947161C/en active Active
- 2015-05-01 MX MX2016014020A patent/MX2016014020A/es unknown
- 2015-05-01 EP EP15785632.9A patent/EP3137437B1/en active Active
- 2015-05-01 RS RS20200062A patent/RS59849B1/sr unknown
- 2015-05-01 SI SI201531073T patent/SI3137437T1/sl unknown
- 2015-05-01 PT PT157856329T patent/PT3137437T/pt unknown
- 2015-05-01 KR KR1020167032691A patent/KR102407375B1/ko active IP Right Grant
- 2015-05-01 US US14/702,126 patent/US9862652B2/en active Active
- 2015-05-01 PL PL15785632T patent/PL3137437T3/pl unknown
- 2015-05-01 HU HUE15785632A patent/HUE047271T2/hu unknown
- 2015-05-04 UY UY0001036107A patent/UY36107A/es not_active Application Discontinuation
- 2015-05-04 TW TW104114159A patent/TWI654162B/zh active
- 2015-05-04 AR ARP150101337A patent/AR100269A1/es active IP Right Grant
-
2016
- 2016-10-26 IL IL248509A patent/IL248509B/en active IP Right Grant
-
2020
- 2020-01-16 HR HRP20200063TT patent/HRP20200063T1/hr unknown
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