HRP20191415T1 - Pretvaranje ulja koja sadržavaju triacilglicerid u ugljikovodike - Google Patents

Pretvaranje ulja koja sadržavaju triacilglicerid u ugljikovodike Download PDF

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HRP20191415T1
HRP20191415T1 HRP20191415T HRP20191415T1 HR P20191415 T1 HRP20191415 T1 HR P20191415T1 HR P20191415 T HRP20191415 T HR P20191415T HR P20191415 T1 HRP20191415 T1 HR P20191415T1
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Croatia
Prior art keywords
triacylglycerides
water
reaction
waste liquid
molecular hydrogen
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Ujjal K Mukherjee
Arun Arora
Marvin I Greene
Edward Coppola
Charles Red Jr
J Steven Baxley
Sanjay Nana
Jeffrey Rine
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Chevron Lummus Global Llc
Applied Res Associates Inc
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Application filed by Chevron Lummus Global Llc, Applied Res Associates Inc filed Critical Chevron Lummus Global Llc
Publication of HRP20191415T1 publication Critical patent/HRP20191415T1/hr

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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/50—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids in the presence of hydrogen, hydrogen donors or hydrogen generating compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • C07C1/22—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms by reduction
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    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/50—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids in the presence of hydrogen, hydrogen donors or hydrogen generating compounds
    • C10G3/52—Hydrogen in a special composition or from a special source
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    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
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    • C10G45/08—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof in combination with chromium, molybdenum, or tungsten metals, or compounds thereof
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    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C10G45/10—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing platinum group metals or compounds thereof
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    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/32—Selective hydrogenation of the diolefin or acetylene compounds
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    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
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    • C10G65/00—Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C10G65/02—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only
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  • Chemical & Material Sciences (AREA)
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Claims (15)

1. Postupak za pretvaranje ulja koja sadržavaju triacilgliceride u prekursore sirove nafte i / ili destilat ugljikovodičnih goriva, naznačen time, da postupak uključuje: reakcija smjese ulja, vode i molekularnog vodika koja sadržava triacilgliceride (16) pri temperaturi u rasponu od 250 °C do 560 °C i tlaku većem od 7,5 MPa (75 bara) radi pretvaranja barem dijela triacilglicerida i dobivanje reakcijske otpadne tekućine (28) koja sadržava vodu i jedan ili više izoolefina, izoparafina, cikloolefina, cikloparafina i aromatika; i katalitička hidroobrada reakcijske otpadne tekućine (28), bez ikakvih međufaznih odvajanja, da se dobije hidroobrađena otpadna tekućina (34; 84), pri čemu smjesa triacilglicerida, vode i molekularnog vodika (16) ima omjer vode i triacilglicerida u rasponu od 0,001 : 1 do 1 : 1 i pri čemu smjesa triacilglicerida, vode i molekularnog vodika (16) ima udio molekularnog vodika u odnosu na triacilgliceride u rasponu od 0,005 : 1 do 0,5 : 1.
2. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da nadalje obuhvaća miješanje ulja (2) koje sadržava triacilgliceride s vodom (10) i molekularnim vodikom (14) radi dobivanja smjese triacilglicerida, vode i molekularnog vodika (16).
3. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da nadalje obuhvaća miješanje ulja (2) koje sadržava triacilgliceride i vode (10) radi dobivanja smjese triacilglicerida i vode (12).
4. Postupak u skladu s patentnim zahtjevom 3, naznačen time, da nadalje obuhvaća miješanje smjese triacilglicerida i vode (12) s molekularnim vodikom (14) radi dobivanja smjese triacilglicerida, vode i molekularnog vodika (16).
5. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da nadalje obuhvaća odvajanje najmanje jednog od molekularnog vodika (36; 64) i vode (32) iz hidroobrađene otpadne tekućine (34; 84).
6. Postupak u skladu s patentnim zahtjevom 5, naznačen time, da nadalje obuhvaća ponovnu upotrebu u reakcijskom koraku barem jednog od odvojenog molekularnog vodika i odvojene vode.
7. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da nadalje obuhvaća ko-obradu neobnovljive ugljikovodične sirovine (25) s reakcijskom otpadnom tekućinom (28) u koraku hidroobrade .
8. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da ulje koje sadržava triacilgliceride (2) sadržava obnovljivo ulje iz barem jednog od sljedećeg: kamelija, karinat, pamuk, jatrofa, karanja, moringa, palma, ricinus, kukuruz, laneno sjeme, kikiriki, soja, suncokretovo, volframovo, babassu ili barem jedno ulje koje sadržava triacilgliceride iz barem jednog od sljedećeg: uljane repice, shea maslaca, visokog ulja, loja, otpadnog biljnog ulja, alginog ulja i pongomije.
9. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da nadalje uključuje frakcioniranje hidroobrađene otpadne tekućine (34; 84) da bi se dobila jedna ili više frakcija ugljikovodika koje imaju vrelište u području nafte (38), dizela (41) ili mlaznog goriva (40).
10. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da se reakcija izvodi u odsutnosti heterogenog ili topljivog metalnog katalizatora.
11. Postupak u skladu s patentnim zahtjevom 1, naznačen time, da se reakcija provodi u reaktoru za hidrotermolizu (82), a postupak nadalje uključuje ubrizgavanje vode u reaktor za hidrotermolizu (82) radi održavanja temperature ili temperaturnog profila unutar reaktora za hidrotermolizu (82).
12. Postupak u skladu s patentnim zahtjevom 9, naznačen time, da se frakcija mlaznog goriva (40) koristi izravno kao mlazno gorivo bez miješanja; ili se dizelska frakcija koristi izravno kao dizelsko gorivo bez miješanja.
13. Postupak u skladu s patentnim zahtjevom 4, naznačen time, da: reakcija se provodi u reakcijskoj zoni hidrotermolize (18); postupak nadalje uključuje: dobivanje reakcijske otpadne tekućine (28) iz reakcijske zone hidrotermolize (18); punjenje reakcijske otpadne tekućine (28) iz reakcijske zone hidrotermolize (18), bez ikakvih međufaznih odvajanja, u zonu katalitičke hidroobrade (29) radi hidroobrade reakcijske otpadne tekućine (28); i dobivanje hidroobrađenog otpada (34; 84).
14. Postupak u skladu s patentnim zahtjevom 13, naznačen time, da se hidrotermoliza provodi bez dodanog anorganskog heterogenog katalizatora.
15. Postupak u skladu s patentnim zahtjevom 13, naznačen time, da reakcijska otpadna tekućina (28) nadalje sadržava organske kiseline i pri čemu se u zoni katalitičke hidroobrade dodatno provodi hidrodeoksigenacija i / ili dekarboksilacija otpadne tekućine hidrotermolize.
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