HK1151281A1 - Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime - Google Patents

Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime

Info

Publication number
HK1151281A1
HK1151281A1 HK11105377.9A HK11105377A HK1151281A1 HK 1151281 A1 HK1151281 A1 HK 1151281A1 HK 11105377 A HK11105377 A HK 11105377A HK 1151281 A1 HK1151281 A1 HK 1151281A1
Authority
HK
Hong Kong
Prior art keywords
compound
formula
millireactors
microreactors
formation
Prior art date
Application number
HK11105377.9A
Other languages
English (en)
Inventor
Sascha Braune
Stefan Steinhofer
Peter Poechlauer
Rafael Wilhelmus Elisabeth Ghislain Reintjens
Nicole Theodora Wilhelmina Linssen
Mehul Thathagar
Original Assignee
Dsm Fine Chem Austria Gmbh
Dsm Nfg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dsm Fine Chem Austria Gmbh, Dsm Nfg filed Critical Dsm Fine Chem Austria Gmbh
Publication of HK1151281A1 publication Critical patent/HK1151281A1/xx

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/02—Preparation of esters of nitric acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/0086—Dimensions of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00889—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/0095—Control aspects
    • B01J2219/00952—Sensing operations
    • B01J2219/00954—Measured properties
    • B01J2219/00966—Measured properties pH
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/0095—Control aspects
    • B01J2219/00984—Residence time

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
HK11105377.9A 2007-12-20 2011-05-31 Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime HK1151281A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP07024754 2007-12-20
PCT/EP2008/068034 WO2009080755A1 (en) 2007-12-20 2008-12-19 Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime

Publications (1)

Publication Number Publication Date
HK1151281A1 true HK1151281A1 (en) 2012-01-27

Family

ID=39313631

Family Applications (1)

Application Number Title Priority Date Filing Date
HK11105377.9A HK1151281A1 (en) 2007-12-20 2011-05-31 Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime

Country Status (8)

Country Link
US (1) US8536366B2 (zh)
EP (1) EP2222628B1 (zh)
KR (1) KR101579989B1 (zh)
CN (1) CN101903328B (zh)
ES (1) ES2391601T3 (zh)
HK (1) HK1151281A1 (zh)
PL (1) PL2222628T3 (zh)
WO (1) WO2009080755A1 (zh)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201139337A (en) 2010-03-31 2011-11-16 Lonza Ag Process for the production of esters of nitric acid
KR101433422B1 (ko) * 2010-11-23 2014-08-27 주식회사 엘지화학 니트로화 반응 장치 및 니트로화 방법
EP2535105A1 (en) 2011-06-14 2012-12-19 Corning Incorporated Systems and methods for scale-up of microreactors
CN105330549A (zh) * 2015-11-20 2016-02-17 南京理工大学 一种在微通道反应器中制备硝酸异辛酯的方法
CN105566117A (zh) * 2015-12-25 2016-05-11 江西西林科股份有限公司 一种硝酸异辛酯粗品的脱酸方法
US11369938B2 (en) 2017-03-05 2022-06-28 Corning Incorporated Flow reactor for photochemical reactions
CN108359811A (zh) * 2018-03-07 2018-08-03 昆明理工大学 一种利用微流体技术反萃钴的方法
EP3539943A1 (de) * 2018-03-15 2019-09-18 Nitrochemie Aschau GmbH Verfahren zur herstellung von n-alkyl-nitratoethylnitraminen
US10703707B2 (en) 2018-11-07 2020-07-07 Industrial Technology Research Institute Method for preparing nitrate ester
US10562873B1 (en) * 2018-12-07 2020-02-18 Northrop Grumman Innovation Systems, Inc. Methods of producing glycidyl nitrate
CN110433682B (zh) * 2019-08-30 2024-04-12 欧志安 一种承压流体混合装置

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5089652A (en) * 1990-01-17 1992-02-18 Atlas Powder Company Nitrate ester preparation
WO2001029111A1 (en) * 1999-10-19 2001-04-26 Alliant Techsystems Inc. Polymerization of poly(glycidyl nitrate) from high purity glycidyl nitrate synthesized from glycerol
DE10014296A1 (de) * 2000-03-23 2001-09-27 Merck Patent Gmbh Verfahren zur Dehydratisierung organischer Verbindungen zu ungesättigten Verbindungen
WO2002014854A1 (en) * 2000-08-14 2002-02-21 Chevron U.S.A. Inc. Use of microchannel reactors in combinatorial chemistry
CA2465697C (en) * 2001-11-27 2010-05-11 Astrazeneca Ab Process for the preparation of (s)-naproxen 4-nitrooxybutyl ester
WO2004004328A1 (ja) 2002-06-26 2004-01-08 Matsushita Electric Industrial Co., Ltd. 特性補正装置
ITMI20022410A1 (it) 2002-11-14 2004-05-15 Dinamite Dipharma S P A Procedimento per la nitrazione di alcandioli.
ITMI20022409A1 (it) * 2002-11-14 2004-05-15 Dinamite Dipharma S P A Procedimento per la purificazione di 1, 4-butandiolo mononitrato.
US6995549B2 (en) 2003-10-14 2006-02-07 Intersil Americas Inc. DC-to-DC power regulator having non-linear load line and automatic leakage current offset adjustment
DE102004007706A1 (de) * 2004-02-16 2005-08-25 Dynamit Nobel Gmbh Explosivstoff- Und Systemtechnik Verfahren zur Herstellung von flüssigen Nitratestern
US7874432B2 (en) * 2004-03-23 2011-01-25 Velocys Protected alloy surfaces in microchannel apparatus and catalysts, alumina supported catalysts, catalyst intermediates, and methods of forming catalysts and microchannel apparatus
EP1604733A1 (en) 2004-06-11 2005-12-14 Corning Incorporated Microstructure designs for optimizing mixing and pressure drop
EP1838431A4 (en) * 2004-12-03 2012-08-22 California Inst Of Techn MICROFLUIDIC DEVICES WITH CIRCUITRY OF CHEMICAL REACTIONS

Also Published As

Publication number Publication date
CN101903328B (zh) 2013-05-15
WO2009080755A1 (en) 2009-07-02
KR101579989B1 (ko) 2015-12-23
CN101903328A (zh) 2010-12-01
EP2222628B1 (en) 2012-07-18
KR20100117569A (ko) 2010-11-03
US8536366B2 (en) 2013-09-17
US20110034720A1 (en) 2011-02-10
PL2222628T3 (pl) 2012-12-31
ES2391601T3 (es) 2012-11-28
EP2222628A1 (en) 2010-09-01

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