GB997335A - Process for preparing inorganic dispersions - Google Patents
Process for preparing inorganic dispersionsInfo
- Publication number
- GB997335A GB997335A GB22117/62A GB2211762A GB997335A GB 997335 A GB997335 A GB 997335A GB 22117/62 A GB22117/62 A GB 22117/62A GB 2211762 A GB2211762 A GB 2211762A GB 997335 A GB997335 A GB 997335A
- Authority
- GB
- United Kingdom
- Prior art keywords
- metal
- alkoxide
- soluble
- oil
- alkali metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000006185 dispersion Substances 0.000 title abstract 7
- 238000004519 manufacturing process Methods 0.000 title 1
- 229910052751 metal Inorganic materials 0.000 abstract 20
- 239000002184 metal Substances 0.000 abstract 20
- 150000004703 alkoxides Chemical class 0.000 abstract 12
- -1 alkali metal alkoxide Chemical class 0.000 abstract 11
- 150000003839 salts Chemical class 0.000 abstract 10
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 9
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 abstract 9
- 229910052783 alkali metal Inorganic materials 0.000 abstract 8
- 125000004432 carbon atom Chemical group C* 0.000 abstract 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 6
- 230000001476 alcoholic effect Effects 0.000 abstract 6
- 239000002270 dispersing agent Substances 0.000 abstract 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 4
- 239000000969 carrier Substances 0.000 abstract 4
- 239000003208 petroleum Substances 0.000 abstract 4
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 abstract 4
- 229910052720 vanadium Inorganic materials 0.000 abstract 4
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 abstract 4
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 abstract 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 3
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 abstract 3
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract 3
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 3
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 abstract 3
- 229910052787 antimony Inorganic materials 0.000 abstract 3
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 abstract 3
- 229910052785 arsenic Inorganic materials 0.000 abstract 3
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 abstract 3
- 229910052797 bismuth Inorganic materials 0.000 abstract 3
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 abstract 3
- 229910052793 cadmium Inorganic materials 0.000 abstract 3
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 abstract 3
- 150000001735 carboxylic acids Chemical class 0.000 abstract 3
- 229910052804 chromium Inorganic materials 0.000 abstract 3
- 239000011651 chromium Substances 0.000 abstract 3
- 229910017052 cobalt Inorganic materials 0.000 abstract 3
- 239000010941 cobalt Substances 0.000 abstract 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 3
- 229910052802 copper Inorganic materials 0.000 abstract 3
- 239000010949 copper Substances 0.000 abstract 3
- 239000000446 fuel Substances 0.000 abstract 3
- 229910052742 iron Inorganic materials 0.000 abstract 3
- 239000011133 lead Substances 0.000 abstract 3
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 abstract 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 abstract 3
- 229910052753 mercury Inorganic materials 0.000 abstract 3
- 150000002736 metal compounds Chemical class 0.000 abstract 3
- 150000002739 metals Chemical class 0.000 abstract 3
- 239000010688 mineral lubricating oil Substances 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 229910052750 molybdenum Inorganic materials 0.000 abstract 3
- 239000011733 molybdenum Substances 0.000 abstract 3
- 229910052759 nickel Inorganic materials 0.000 abstract 3
- 239000003921 oil Substances 0.000 abstract 3
- 235000019198 oils Nutrition 0.000 abstract 3
- 230000000737 periodic effect Effects 0.000 abstract 3
- 229910052709 silver Inorganic materials 0.000 abstract 3
- 239000004332 silver Substances 0.000 abstract 3
- 229910052718 tin Inorganic materials 0.000 abstract 3
- 229910052725 zinc Inorganic materials 0.000 abstract 3
- 239000011701 zinc Substances 0.000 abstract 3
- 229910052726 zirconium Inorganic materials 0.000 abstract 3
- 241000158728 Meliaceae Species 0.000 abstract 2
- VKCLPVFDVVKEKU-UHFFFAOYSA-N S=[P] Chemical compound S=[P] VKCLPVFDVVKEKU-UHFFFAOYSA-N 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- 239000000654 additive Substances 0.000 abstract 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 2
- 150000001340 alkali metals Chemical class 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- 239000001569 carbon dioxide Substances 0.000 abstract 2
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 230000003301 hydrolyzing effect Effects 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 125000005608 naphthenic acid group Chemical group 0.000 abstract 2
- FBUKVWPVBMHYJY-UHFFFAOYSA-N nonanoic acid Chemical compound CCCCCCCCC(O)=O FBUKVWPVBMHYJY-UHFFFAOYSA-N 0.000 abstract 2
- 239000000344 soap Substances 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 2
- 235000015112 vegetable and seed oil Nutrition 0.000 abstract 2
- 239000008158 vegetable oil Substances 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- OBETXYAYXDNJHR-SSDOTTSWSA-M (2r)-2-ethylhexanoate Chemical compound CCCC[C@@H](CC)C([O-])=O OBETXYAYXDNJHR-SSDOTTSWSA-M 0.000 abstract 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 abstract 1
- ZNVKBJFZIOOWKR-UHFFFAOYSA-N 1,2-dioctylcyclopentane-1-carboxylic acid Chemical class CCCCCCCCC1CCCC1(CCCCCCCC)C(O)=O ZNVKBJFZIOOWKR-UHFFFAOYSA-N 0.000 abstract 1
- GBZUYUQGHANCOJ-UHFFFAOYSA-N 1-hexadecylcyclohexane-1-carboxylic acid Chemical class CCCCCCCCCCCCCCCCC1(C(O)=O)CCCCC1 GBZUYUQGHANCOJ-UHFFFAOYSA-N 0.000 abstract 1
- VIZFUFHTPYGKSY-UHFFFAOYSA-N 1-octadecyl-2,3,3a,4,5,6,7,7a-octahydroindene-1-carboxylic acid Chemical class C1CCCC2C(CCCCCCCCCCCCCCCCCC)(C(O)=O)CCC21 VIZFUFHTPYGKSY-UHFFFAOYSA-N 0.000 abstract 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 abstract 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 abstract 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 abstract 1
- 239000004254 Ammonium phosphate Substances 0.000 abstract 1
- DJHGAFSJWGLOIV-UHFFFAOYSA-K Arsenate3- Chemical compound [O-][As]([O-])([O-])=O DJHGAFSJWGLOIV-UHFFFAOYSA-K 0.000 abstract 1
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 abstract 1
- XEBPBIBXVBMCHQ-UHFFFAOYSA-N C(CCCCCCCCCCC)C12CCCCC2(CCCC1)CCCCCCCCCCCC Chemical compound C(CCCCCCCCCCC)C12CCCCC2(CCCC1)CCCCCCCCCCCC XEBPBIBXVBMCHQ-UHFFFAOYSA-N 0.000 abstract 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 abstract 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 abstract 1
- BDAGIHXWWSANSR-UHFFFAOYSA-M Formate Chemical compound [O-]C=O BDAGIHXWWSANSR-UHFFFAOYSA-M 0.000 abstract 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 abstract 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract 1
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 1
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 abstract 1
- 239000005642 Oleic acid Substances 0.000 abstract 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 abstract 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- 239000005643 Pelargonic acid Substances 0.000 abstract 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 abstract 1
- 150000004645 aluminates Chemical class 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 abstract 1
- 235000019289 ammonium phosphates Nutrition 0.000 abstract 1
- 229940000489 arsenate Drugs 0.000 abstract 1
- 229910052788 barium Inorganic materials 0.000 abstract 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 abstract 1
- SXDBWCPKPHAZSM-UHFFFAOYSA-M bromate Inorganic materials [O-]Br(=O)=O SXDBWCPKPHAZSM-UHFFFAOYSA-M 0.000 abstract 1
- SXDBWCPKPHAZSM-UHFFFAOYSA-N bromic acid Chemical compound OBr(=O)=O SXDBWCPKPHAZSM-UHFFFAOYSA-N 0.000 abstract 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 239000011575 calcium Substances 0.000 abstract 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical compound [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 abstract 1
- 238000002485 combustion reaction Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- 238000005260 corrosion Methods 0.000 abstract 1
- 230000007797 corrosion Effects 0.000 abstract 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 abstract 1
- 150000001991 dicarboxylic acids Chemical class 0.000 abstract 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 1
- 229940075933 dithionate Drugs 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 229930195729 fatty acid Natural products 0.000 abstract 1
- 239000000194 fatty acid Substances 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
- 239000003112 inhibitor Substances 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- ICIWUVCWSCSTAQ-UHFFFAOYSA-M iodate Chemical compound [O-]I(=O)=O ICIWUVCWSCSTAQ-UHFFFAOYSA-M 0.000 abstract 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 abstract 1
- 235000020778 linoleic acid Nutrition 0.000 abstract 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 abstract 1
- 230000001050 lubricating effect Effects 0.000 abstract 1
- 239000010687 lubricating oil Substances 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 239000011777 magnesium Substances 0.000 abstract 1
- LBSANEJBGMCTBH-UHFFFAOYSA-N manganate Chemical compound [O-][Mn]([O-])(=O)=O LBSANEJBGMCTBH-UHFFFAOYSA-N 0.000 abstract 1
- MEFBJEMVZONFCJ-UHFFFAOYSA-N molybdate Chemical compound [O-][Mo]([O-])(=O)=O MEFBJEMVZONFCJ-UHFFFAOYSA-N 0.000 abstract 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 150000003017 phosphorus Chemical class 0.000 abstract 1
- 229920001155 polypropylene Polymers 0.000 abstract 1
- WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 abstract 1
- 229960003656 ricinoleic acid Drugs 0.000 abstract 1
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 229910052712 strontium Inorganic materials 0.000 abstract 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 abstract 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 abstract 1
- 239000010689 synthetic lubricating oil Substances 0.000 abstract 1
- 229940095064 tartrate Drugs 0.000 abstract 1
- PBYZMCDFOULPGH-UHFFFAOYSA-N tungstate Chemical compound [O-][W]([O-])(=O)=O PBYZMCDFOULPGH-UHFFFAOYSA-N 0.000 abstract 1
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical compound [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/68—Preparation of metal alcoholates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/68—Preparation of metal alcoholates
- C07C29/685—Preparation of metal alcoholates by converting O-metal groups to other O-metal groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic Table
- C07F1/005—Compounds containing elements of Groups 1 or 11 of the Periodic Table without C-Metal linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F13/00—Compounds containing elements of Groups 7 or 17 of the Periodic Table
- C07F13/005—Compounds without a metal-carbon linkage
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
- C07F15/04—Nickel compounds
- C07F15/045—Nickel compounds without a metal-carbon linkage
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
- C07F15/06—Cobalt compounds
- C07F15/065—Cobalt compounds without a metal-carbon linkage
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/003—Compounds containing elements of Groups 2 or 12 of the Periodic Table without C-Metal linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/003—Compounds containing elements of Groups 3 or 13 of the Periodic Table without C-Metal linkages
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/143—Organic compounds mixtures of organic macromolecular compounds with organic non-macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
- C10M159/12—Reaction products
- C10M159/20—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/192—Macromolecular compounds
- C10L1/195—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C10L1/196—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds derived from monomers containing a carbon-to-carbon unsaturated bond and a carboxyl group or salts, anhydrides or esters thereof homo- or copolymers of compounds having one or more unsaturated aliphatic radicals each having one carbon bond to carbon double bond, and at least one being terminated by a carboxyl radical or of salts, anhydrides or esters thereof
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Abstract
A stable dispersion of a metal compound in a non-volatile carrier is prepared by:-(a) mixing an alkoxide and/or alcohol-soluble carbonate of the alkoxide of a metal from Group Ib, IIa, IIb, IIIa, IIIb, IVa, IVb, Va, Vb, VIb, VIIb, and VIII of the Periodic Table according to Deming, an oil-soluble dispersing agent, a nonvolatile carrier, and water; (b) hydrolysing the metal alkoxide to an oil-insoluble metal compound and (c) removing the volatile materials from the mixture; the said metal alkoxide having been prepared by reacting an alkali metal or alkali metal hydroxide with an alcohol to form an alkali metal alkoxide, and then reacting a salt of the said metal with the alkali metal alkoxide in an alcoholic solution to form a metal alkoxide, the resulting alkali metal salt being less soluble in the alcoholic solution than the metal salt. The alcoholic solution of the metal salt may be stabilized by carbonating the solution by passing in carbon dioxide. The process is particularly suitable for preparing dispersions of compounds of chromium, molybdenum, manganese, iron, cobalt, nickel, copper, zinc, cadmium, tin, lead, vanadium, zirconium, silver, mercury, arsenic, antimony and bismuth. Suitable alcohols for use in the process are alkanols having 1-6 carbon atoms, monoethers of ethylene glycol containing not more than 8 carbon atoms, and monoethers of diethylene glycol containing not more than 8 carbon atoms. The non-volatile carriers used in the dispersion include mineral lubricating oils, vegetable oils and synthetic oils such as propylene polymers, polyoxyalkylenes, and esters of dicarboxylic acids or phosphorus acids, the preferred ones being mineral or synthetic lubricating oils. The non-volatile carriers may be diluted with a solvent, e.g. petroleum naphtha or hydrocarbons, to reduce the viscosity. Suitable oil-soluble dispersing agents include oil-soluble sulphonic acids, carboxylic acids, phosphorus sulphide-treated olefines, phenolic organic compounds and metal salts thereof. The preferred dispersing agents are sulphonates, e.g. alkyl and aryl sulphonates, mahogany soaps and wax sulphonates the wax being obtained from crude petroleum oil, and carboxylic acids, e.g. naphthenic acids such as cetyl cyclohexane carboxylic acids, dioctyl cyclopentane carboxylic acids, dilauryl decahydronaphthalene and stearyl-octahydroindene carboxylic acids and oil-soluble salts thereof, and fatty acids such as 2-ethyl hexanoic acid, pelargonic acid, oleic acid linoleic acid and ricinoleic acid. Specification 906,208 is referred to.ALSO:Alkoxides of metals of Group Ib, IIa, IIb, IIIa, IIIb, IVa, IVb, Va, Vb, VIb, VIIb and VIII of the Periodic Table (according to Deming) are prepared by reacting an alkali metal or alkali metal hydroxide with an alcohol to form an alkali metal alkoxide and then reacting a salt of one of the above specified metals with the alkali metal alkoxide in an alcoholic solution to form the metal alkoxide, the resulting alkali metal salt being less soluble in the alcoholic solution than the starting metal salt. Preferably the alcohol is an aliphatic monohydric alcohol having 1-6 carbon atoms, a monoether of ethylene glycol having not more than 8 carbon atoms or a monoether of diethylene glycol having not more than 8 carbon atoms. The metal salts used as starting materials may be, for example, a halide, nitrate, sulphate, acetate, ammonium phosphate, bromate, carbonate, citrate, cyamide, dithionate, formate, iodate, nitrite, oxalate, phosphate, silicate, sulphate, sulphite, tartrate, aluminate, antimonate, arsenate, bismuthate, borate, chromate, manganate, molybdate, selenate, tungstate, uranate or vanadate and the metal salts are preferably those of aluminium, silver, arsenic, barium, bismuth, calcium, cadmium, cobalt, chromium, copper, iron, mercury, magnesium, manganese, molybdenum, nickel, lead, antimony, strontium, tin, vanadium, zinc and zirconium. In some cases it may be necessary to carbonate the metal alkoxide in order to stabilize the alcoholic solution. The carbonating is effected by passing carbon dioxide through the system and the product is a metal alkoxide carbonate complex. Specification 906,208 is referred to.ALSO:A stable dispersion for use as an additive for fuels or lubricating oils is prepared by: (a) mixing an alkoxide and/or alcohol-soluble carbonate of the alkoxide of a metal from Groups Ib, IIa, IIb, IIIa, IIIb, IVa, IVb, Va, Vb, VIb, VIIb and VIII of the Periodic Table according to Denning, an oil-soluble dispersing agent, a non-volatile carrier and water; (b) hydrolysing the metal alkoxide to an oil-insoluble metal compound, and (c) removing the volatile materials from the mixture. The preferred metals are chromium, molybdenum, manganese, iron, cobalt, nickel, copper, zinc, cadmium, tin, lead, vanadium, zirconium, silver, mercury, arsenic, antimony and bismuth. Suitable alcohol constituents of the alkoxide are C1-C6 alkanols and monoethers of ethylene glycol and diethylene glycol having not more than 8 carbon atoms. The non-volatile carriers used in the dispersion include mineral lubricating oils, vegetable oils and synthetic oils. The non-volatile carriers may be diluted with a solvent, for example petroleum naphtha or hydrocarbons, to reduce the viscosity. Suitable oil-soluble dispersing agents include oil-soluble sulphonic acids, carboxylic acids, phosphorus sulphide-treated olefines, phenolic organic compounds and metal salts thereof. The preferred dispersing agents are sulphonates, e.g. alkyl and aryl sulphonates, mahogany soaps and wax sulphonates, the wax being obtained from crude petroleum oils, and naphthenic acids. The dispersions may be added to internal-combustion engine lubricating compositions and may be used as corrosion inhibitors in vanadium-containing fuels and as additives to fuels in general. Specification 906,208 is referred to.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US124315A US3277002A (en) | 1961-07-17 | 1961-07-17 | Process for stably dispersing metal compounds |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB997335A true GB997335A (en) | 1965-07-07 |
Family
ID=22414130
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB22117/62A Expired GB997335A (en) | 1961-07-17 | 1962-06-07 | Process for preparing inorganic dispersions |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US3277002A (en) |
| FR (1) | FR1337804A (en) |
| GB (1) | GB997335A (en) |
| NL (1) | NL281035A (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4200544A (en) * | 1976-04-29 | 1980-04-29 | The Lubrizol Corporation | Magnesium-containing greases and method for their preparation |
| WO1980001807A1 (en) * | 1979-02-21 | 1980-09-04 | Lubrizol Corp | Magnesium oxide-carboxylate complexes,method for their preparation,and compositions containing the same |
| WO1980001806A1 (en) * | 1979-02-21 | 1980-09-04 | Lubrizol Corp | Magnesium-containing complexes,method for their preparation,and compositions containing the same |
| USRE32235E (en) * | 1976-04-29 | 1986-08-26 | The Lubrizol Corporation | Magnesium-containing complexes, method for their preparation, and compositions containing the same |
| WO1987004454A3 (en) * | 1986-01-21 | 1987-09-11 | Lubrizol Corp | Lubricant composition containing transition metals for viscosity control |
| FR2648473A1 (en) * | 1989-06-19 | 1990-12-21 | Elf Aquitaine | LOWERING ADDITIVES FOR LUBRICATING OILS COMPRISING A MOLYBDENUM COMPLEX, PROCESS FOR THEIR PREPARATION AND COMPOSITIONS COMPRISING SAID ADDITIVES |
| FR2716891A1 (en) * | 1994-03-03 | 1995-09-08 | Inst Francais Du Petrole | New colloidal prods. useful as anti-wear and extreme pressure additives in oil and grease lubricants |
| FR2810341A1 (en) * | 2000-06-19 | 2001-12-21 | Ge Energy Products France Snc | Nickel compounds for inhibiting vanadium corrosion of thermal equipment burning vanadium-containing fuels are used in the form of aqueous or liposoluble solutions |
| EP1947162A3 (en) * | 2007-01-16 | 2010-01-06 | Afton Chemical Corporation | Safe combustion additives and methods of formulation |
| US7682526B2 (en) | 2005-12-22 | 2010-03-23 | Afton Chemical Corporation | Stable imidazoline solutions |
| US7709423B2 (en) | 2005-11-16 | 2010-05-04 | Afton Chemical Corporation | Additives and lubricant formulations for providing friction modification |
| US7767632B2 (en) | 2005-12-22 | 2010-08-03 | Afton Chemical Corporation | Additives and lubricant formulations having improved antiwear properties |
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|---|---|---|---|---|
| US3907906A (en) * | 1972-03-29 | 1975-09-23 | Continental Oil Co | Process of recovering alcohols and oil from waste mixtures |
| US3915727A (en) * | 1973-03-05 | 1975-10-28 | Continental Oil Co | Method for selectively modifying the permeability of subterranean formation |
| US3907691A (en) * | 1974-07-15 | 1975-09-23 | Chevron Res | Extreme-pressure mixed metal borate lubricant |
| US4104180A (en) * | 1975-05-23 | 1978-08-01 | Exxon Research & Engineering Co. | Production of overbased metal phenates |
| GB2055885B (en) * | 1979-07-27 | 1983-06-22 | Exxon Research Engineering Co | Overbased magnesium detergent additives |
| US4837190A (en) * | 1986-05-09 | 1989-06-06 | Akzo America Inc. | Organic solvent soluble polyvalent metal alkoxy alkoxides |
| US4847239A (en) * | 1987-12-07 | 1989-07-11 | Texas Alkyls, Inc. | Hydrocarbon soluble copper alkoxide compositions |
| US5059703A (en) * | 1987-12-07 | 1991-10-22 | Texas Alkyls, Inc. | Hydrocarbon soluble copper alkoxide compositions |
| US5104997A (en) * | 1988-09-30 | 1992-04-14 | Fmc Corporation | Mass treatment of cellulosic materials |
| US5006508A (en) * | 1989-02-03 | 1991-04-09 | General Atomics | Preparation of copper alkoxides and sol/gel precursors of superconducting ceramics |
| DE4207883A1 (en) * | 1992-03-12 | 1993-09-16 | Hoechst Ag | METHOD FOR STABILIZING ETHANOLIC ETHYL MAGNESIUM CARBONATE SOLUTIONS |
| DE4237701A1 (en) * | 1992-11-07 | 1994-05-11 | Huels Chemische Werke Ag | Storage-stable solutions of carbonized magnesium ethylate in ethanol as well as their production and use |
| US7615520B2 (en) | 2005-03-14 | 2009-11-10 | Afton Chemical Corporation | Additives and lubricant formulations for improved antioxidant properties |
| US7615519B2 (en) | 2004-07-19 | 2009-11-10 | Afton Chemical Corporation | Additives and lubricant formulations for improved antiwear properties |
| US7776800B2 (en) | 2005-12-09 | 2010-08-17 | Afton Chemical Corporation | Titanium-containing lubricating oil composition |
| CN114369482A (en) * | 2021-12-29 | 2022-04-19 | 烟台大学 | Preparation and use method of nanoscale super-smooth powder antifriction additive |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1689356A (en) * | 1925-11-12 | 1928-10-30 | Chem Fab Auf Actien | Method of producing complex metal alcoholates |
| US2125961A (en) * | 1937-08-16 | 1938-08-09 | Standard Oil Co | Color stable viscous hydrocarbon oil |
| US2229528A (en) * | 1938-03-23 | 1941-01-21 | Standard Oil Co | Stabilized hydrocarbon oil |
| US2252664A (en) * | 1938-07-16 | 1941-08-12 | Socony Vacuum Oil Co Inc | Alkyl substituted metal aryl hydroxylate-metal carboxylate salts and a method of making them |
| US2585520A (en) * | 1948-12-03 | 1952-02-12 | Shell Dev | Lubricating compositions containing highly basic metal sulfonates |
| US2671758A (en) * | 1949-09-27 | 1954-03-09 | Shell Dev | Colloidal compositions and derivatives thereof |
| NL82973C (en) * | 1950-12-30 | |||
| GB774683A (en) * | 1952-11-03 | 1957-05-15 | Anglamol Ltd | Improvements in or relating to lubricating compositions |
| US2794828A (en) * | 1953-04-10 | 1957-06-04 | Sonneborn Sons Inc L | Petroleum mahogany sulfonates with high alkaline earth metal content |
| NL228145A (en) * | 1957-05-28 | |||
| US2920105A (en) * | 1957-12-13 | 1960-01-05 | Texaco Inc | Preparation of hyperbasic sulfonates |
| BE602059A (en) * | 1959-05-07 |
-
0
- NL NL281035D patent/NL281035A/xx unknown
-
1961
- 1961-07-17 US US124315A patent/US3277002A/en not_active Expired - Lifetime
-
1962
- 1962-06-07 GB GB22117/62A patent/GB997335A/en not_active Expired
- 1962-07-06 FR FR903272A patent/FR1337804A/en not_active Expired
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4200544A (en) * | 1976-04-29 | 1980-04-29 | The Lubrizol Corporation | Magnesium-containing greases and method for their preparation |
| USRE32235E (en) * | 1976-04-29 | 1986-08-26 | The Lubrizol Corporation | Magnesium-containing complexes, method for their preparation, and compositions containing the same |
| WO1980001807A1 (en) * | 1979-02-21 | 1980-09-04 | Lubrizol Corp | Magnesium oxide-carboxylate complexes,method for their preparation,and compositions containing the same |
| WO1980001806A1 (en) * | 1979-02-21 | 1980-09-04 | Lubrizol Corp | Magnesium-containing complexes,method for their preparation,and compositions containing the same |
| WO1987004454A3 (en) * | 1986-01-21 | 1987-09-11 | Lubrizol Corp | Lubricant composition containing transition metals for viscosity control |
| AU604678B2 (en) * | 1986-01-21 | 1991-01-03 | Lubrizol Corporation, The | Lubricant composition containing transition metals for viscosity control |
| FR2648473A1 (en) * | 1989-06-19 | 1990-12-21 | Elf Aquitaine | LOWERING ADDITIVES FOR LUBRICATING OILS COMPRISING A MOLYBDENUM COMPLEX, PROCESS FOR THEIR PREPARATION AND COMPOSITIONS COMPRISING SAID ADDITIVES |
| EP0404650A1 (en) * | 1989-06-19 | 1990-12-27 | Societe Nationale Elf Aquitaine | Overbased lubricating oil additives containing a molybdenun complex, process of preparation and compositions containing the same |
| FR2716891A1 (en) * | 1994-03-03 | 1995-09-08 | Inst Francais Du Petrole | New colloidal prods. useful as anti-wear and extreme pressure additives in oil and grease lubricants |
| WO1996030467A1 (en) * | 1994-03-03 | 1996-10-03 | Institut Français Du Petrole | Colloidal products containing calcium, barium and/or magnesium as well as bismuth, and being modified by sulphur- and optionally nitrogen-containing carboxylic acid activity |
| US5696062A (en) * | 1994-03-03 | 1997-12-09 | Institut Francais Du Petrole | Colloidal products containing calcium barium and/or magnesium also bismuth modified by the action of carboxylic acids containing sulphur and optionally nitrogen |
| FR2810341A1 (en) * | 2000-06-19 | 2001-12-21 | Ge Energy Products France Snc | Nickel compounds for inhibiting vanadium corrosion of thermal equipment burning vanadium-containing fuels are used in the form of aqueous or liposoluble solutions |
| WO2001098437A1 (en) * | 2000-06-19 | 2001-12-27 | Ge Energy Products France Snc | Use of nickel compounds as vanadium corrosion inhibitors |
| US7709423B2 (en) | 2005-11-16 | 2010-05-04 | Afton Chemical Corporation | Additives and lubricant formulations for providing friction modification |
| US7682526B2 (en) | 2005-12-22 | 2010-03-23 | Afton Chemical Corporation | Stable imidazoline solutions |
| US7767632B2 (en) | 2005-12-22 | 2010-08-03 | Afton Chemical Corporation | Additives and lubricant formulations having improved antiwear properties |
| EP1947162A3 (en) * | 2007-01-16 | 2010-01-06 | Afton Chemical Corporation | Safe combustion additives and methods of formulation |
Also Published As
| Publication number | Publication date |
|---|---|
| NL281035A (en) | |
| FR1337804A (en) | 1963-08-12 |
| US3277002A (en) | 1966-10-04 |
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