GB977477A - The preparation of mono sulfonic acid anhydrides of halogen substituted aromatic hydrocarbons - Google Patents
The preparation of mono sulfonic acid anhydrides of halogen substituted aromatic hydrocarbonsInfo
- Publication number
- GB977477A GB977477A GB328862A GB328862A GB977477A GB 977477 A GB977477 A GB 977477A GB 328862 A GB328862 A GB 328862A GB 328862 A GB328862 A GB 328862A GB 977477 A GB977477 A GB 977477A
- Authority
- GB
- United Kingdom
- Prior art keywords
- chlorotoluene
- halogenated
- reaction mixture
- sulphonating
- sulphonating agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000004945 aromatic hydrocarbons Chemical class 0.000 title abstract 3
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 title 1
- 229910052736 halogen Inorganic materials 0.000 title 1
- 125000005843 halogen group Chemical group 0.000 title 1
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 abstract 10
- 239000003795 chemical substances by application Substances 0.000 abstract 3
- 150000008282 halocarbons Chemical class 0.000 abstract 3
- 125000004971 nitroalkyl group Chemical group 0.000 abstract 3
- 239000011541 reaction mixture Substances 0.000 abstract 3
- QARVLSVVCXYDNA-UHFFFAOYSA-N bromobenzene Chemical compound BrC1=CC=CC=C1 QARVLSVVCXYDNA-UHFFFAOYSA-N 0.000 abstract 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 abstract 2
- INANHCYXMBSHDN-UHFFFAOYSA-N (4-iodophenyl)sulfonyl 4-iodobenzenesulfonate Chemical compound C1=CC(I)=CC=C1S(=O)(=O)OS(=O)(=O)C1=CC=C(I)C=C1 INANHCYXMBSHDN-UHFFFAOYSA-N 0.000 abstract 1
- RELMFMZEBKVZJC-UHFFFAOYSA-N 1,2,3-trichlorobenzene Chemical compound ClC1=CC=CC(Cl)=C1Cl RELMFMZEBKVZJC-UHFFFAOYSA-N 0.000 abstract 1
- WJIFKOVZNJTSGO-UHFFFAOYSA-N 1-bromo-3-methylbenzene Chemical compound CC1=CC=CC(Br)=C1 WJIFKOVZNJTSGO-UHFFFAOYSA-N 0.000 abstract 1
- DLKQHBOKULLWDQ-UHFFFAOYSA-N 1-bromonaphthalene Chemical compound C1=CC=C2C(Br)=CC=CC2=C1 DLKQHBOKULLWDQ-UHFFFAOYSA-N 0.000 abstract 1
- IBSQPLPBRSHTTG-UHFFFAOYSA-N 1-chloro-2-methylbenzene Chemical compound CC1=CC=CC=C1Cl IBSQPLPBRSHTTG-UHFFFAOYSA-N 0.000 abstract 1
- OSOUNOBYRMOXQQ-UHFFFAOYSA-N 1-chloro-3-methylbenzene Chemical compound CC1=CC=CC(Cl)=C1 OSOUNOBYRMOXQQ-UHFFFAOYSA-N 0.000 abstract 1
- JTPNRXUCIXHOKM-UHFFFAOYSA-N 1-chloronaphthalene Chemical compound C1=CC=C2C(Cl)=CC=CC2=C1 JTPNRXUCIXHOKM-UHFFFAOYSA-N 0.000 abstract 1
- APSMUYYLXZULMS-UHFFFAOYSA-N 2-bromonaphthalene Chemical compound C1=CC=CC2=CC(Br)=CC=C21 APSMUYYLXZULMS-UHFFFAOYSA-N 0.000 abstract 1
- NPDACUSDTOMAMK-UHFFFAOYSA-N 4-Chlorotoluene Chemical compound CC1=CC=C(Cl)C=C1 NPDACUSDTOMAMK-UHFFFAOYSA-N 0.000 abstract 1
- 150000008064 anhydrides Chemical class 0.000 abstract 1
- YCOXTKKNXUZSKD-UHFFFAOYSA-N as-o-xylenol Natural products CC1=CC=C(O)C=C1C YCOXTKKNXUZSKD-UHFFFAOYSA-N 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- SNHMUERNLJLMHN-UHFFFAOYSA-N iodobenzene Chemical compound IC1=CC=CC=C1 SNHMUERNLJLMHN-UHFFFAOYSA-N 0.000 abstract 1
- LYGJENNIWJXYER-UHFFFAOYSA-N nitromethane Chemical compound C[N+]([O-])=O LYGJENNIWJXYER-UHFFFAOYSA-N 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DK35061A DK100996C (da) | 1961-01-26 | 1961-01-26 | Fremgangsmåde til fremstilling af monosulfonsyreanhydrider af halogensubstituerede aromatiske carbonhydrider ved sulfonering af carbonhydriderne med svovltrioxid eller svovltrioxidholdige sulfoneringsmidler. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB977477A true GB977477A (en) | 1964-12-09 |
Family
ID=8092531
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB328862A Expired GB977477A (en) | 1961-01-26 | 1962-01-29 | The preparation of mono sulfonic acid anhydrides of halogen substituted aromatic hydrocarbons |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE612941A (en)) |
| CH (1) | CH431500A (en)) |
| DE (1) | DE1205963B (en)) |
| DK (1) | DK100996C (en)) |
| GB (1) | GB977477A (en)) |
| NL (2) | NL273797A (en)) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018192954A1 (en) * | 2017-04-18 | 2018-10-25 | Basf Se | Process for purifying alkanesulfonic anhydride and process for producing alkanesulfonic acid using the purified alkanesulfonic anhydride |
-
0
- BE BE612941D patent/BE612941A/xx unknown
- NL NL133969D patent/NL133969C/xx active
- NL NL273797D patent/NL273797A/xx unknown
-
1961
- 1961-01-26 DK DK35061A patent/DK100996C/da active
-
1962
- 1962-01-17 DE DEA39251A patent/DE1205963B/de active Pending
- 1962-01-25 CH CH89962A patent/CH431500A/de unknown
- 1962-01-29 GB GB328862A patent/GB977477A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018192954A1 (en) * | 2017-04-18 | 2018-10-25 | Basf Se | Process for purifying alkanesulfonic anhydride and process for producing alkanesulfonic acid using the purified alkanesulfonic anhydride |
| CN110770207A (zh) * | 2017-04-18 | 2020-02-07 | 巴斯夫欧洲公司 | 提纯链烷磺酸酐的方法和使用纯化的链烷磺酸酐生产链烷磺酸的方法 |
| US10730827B2 (en) | 2017-04-18 | 2020-08-04 | Basf Se | Process for purifying alkanesulfonic anhydride and process for producing alkanesulfonic acid using the purified alkanesulfonic anhydride |
| CN110770207B (zh) * | 2017-04-18 | 2022-06-24 | 巴斯夫欧洲公司 | 提纯链烷磺酸酐的方法和使用纯化的链烷磺酸酐生产链烷磺酸的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| NL133969C (en)) | |
| DE1205963B (de) | 1965-12-02 |
| BE612941A (en)) | |
| CH431500A (de) | 1967-03-15 |
| NL273797A (en)) | |
| DK100996C (da) | 1965-02-15 |
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