GB970363A - Improvements in vitamin preparations and process for producing them - Google Patents
Improvements in vitamin preparations and process for producing themInfo
- Publication number
- GB970363A GB970363A GB4065/60A GB406560A GB970363A GB 970363 A GB970363 A GB 970363A GB 4065/60 A GB4065/60 A GB 4065/60A GB 406560 A GB406560 A GB 406560A GB 970363 A GB970363 A GB 970363A
- Authority
- GB
- United Kingdom
- Prior art keywords
- vitamin
- zein
- esters
- menadione
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Animal Husbandry (AREA)
- Zoology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Fodder In General (AREA)
- Medicinal Preparation (AREA)
Abstract
A vitamin-containing additive for feeding stuffs, particularly for poultry, consists of or comprises particles of zein throughout which one or more of the following vitamin-active substances is or are distributed in soluble or dispersed form: Vitamin A, b -carotin, Vitamin D2 or D3 or their esters, Vitamin K, menadione and its bisulphite compounds, and 2-methyl, 1,4-naphtho-hydroquinone e.g. in the form of the salts of its phosphoric acid and sulphuric acid esters and the like synthetic K-vitamin-active substances. The additive preferably includes: (i) substances capable of modifying the properties of the zein such as carbohydrates e.g. glucose or maltose, higher glycols or free fatty acids or esters of these, esters of phthalic acid or similar acids, compounds of high molecular weight containing hydrophilic groups as polyethylene glycol, higher fatty acid esters of sorbitol, especially the monoester, and fatty acids containing 7 to 9 carbon atoms in the carbon chain and (ii) antioxidants such as p-aminophenol, butylhydroxytoluene or 6-ethoxy-1,2-dihydro-2,2,4-trimethylquinoline. In preparations containing menadione or menadione bisulphite, aninorganic acid such as sulphuric, hydrochloric or phosphoric acid is included to reduce the loss in K-Vitamin activity during storage. A chelating agent such as the sodium salt of ethylene diaminetetra-acetic acid also may be included. In the production of the vitamin-containing additive there is produced a homogeneous solution or a dispersion of one or more of the vitamin-active substances in a solution of zein, the solution or dispersion is dried and the dried product obtained, if it has not already before or during the drying been formed and crushed into separate particles containing the vitamin-active substance enclosed in a zein-containing mass, is formed and crushed into such particles. The zein may be dissolved in ethanol, propanol or butanol in the presence or absence of various nonsolvents such as water, ketones and chlorinated hydrocarbons. According to an example, 30 grams of a commercial Vitamin A concentrate having a Vitamin A content of one million International Units per gram and 1 milligram of 2,6-ditertiary-butyl p-cresol per gram were mixed with a solution of 300 grams of zein and 30 grams of diethyl phthalate in a mixture of 180 grams ethanol and 60 grams water at 60 DEG C. The emulsion formed by vigorous stirring was poured out in 1mm. thick layers on trays and dried at 40 DEG C. in a current of air. The dried product was ground in a hammer mill to an average size of between 30 and 60 mesh. This product was mixed with such a quantity of wheat bran, containing 17% moisture, that the mixture contained 1000 I.U. Vitamin A per gram; this mixture was then compressed with chicken-feed ingredients into pellets with a diameter of about 5-6mm. containing 10 I.U. Vitamin A per gram; the chicken feed ingredients included in specified proportions: wheat flour, wheat bran, oats, oats polishing flour, ground barley, alfalfa flour, linseed meal, meat and bone meal, herring meal, buttermilk powder, whey powder, dried yeast, calcium carbonate and sodium chloride. In a further example the emulsion was spray dried and then admixed with lactose. According to certain other examples there were employed (a) Vitamin A acetate dissolved in soya oil and mixed with 6-ethoxy-1,2-di-hydro-2,2,4-trimethylquinoline, (b) menadione sodium bisulphite and (c) a mixture of Vitamin D3 and menadione sodium bisulphite.ALSO:A vitamin composition consists of or comprises particles of zein throughout which one or more of the following vitamin-active substances is or are distributed in soluble or dispersed form: Vitamin A, b -carotin, Vitamin D2 or D3 or their esters, Vitamin K, menadione and its bisulphite compounds, and 2-methyl-1,4-naphtho-hydroquinone, eig. in the form of the salts of its phosphoric acid and sulphuric acid esters and the like synthetic K-vitamin-active substances. The composition preferably includes substances capable of modifying the properties of the zein such as carbohydrates, e.g. glucose or maltose, higher glycols or free fatty acids or esters of these, esters of phthalic acid or similar acids, compounds of high molecular weight containing hydrophilic groups such as polyethylene glycol, higher fatty acid esters of sorbitol, especially the monoester, and fatty acids containing 7 to 9 carbon atoms in the carbon chain and antioxidants. In preparations containing menadione or menadione bisulphite, an inorganic acid such as sulphuric, hydrochloric or phosphoric acid is included to reduce the loss in K-vitamin activity during storage. A chelating agent such as the sodium salt of ethylene diaminetetra-acetic acid also may be included. In the production of the composition there is produced a homogeneous solution or a dispersion of one or more of the vitamin-active substances in a solution of zein, the solution or dispersion is dried and the dried product obtained, if it has not already before or during the drying been formed and crushed into separate particles containing the vitamin-active substance enclosed in a zein-containing mass, is formed and crushed into such particles. The zein may be dissolved in ethanol, propanol or butanol in the presence or absence of various non-solvents such as water, ketones and chlorinated hydrocarbons.
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB4065/60A GB970363A (en) | 1960-02-04 | 1960-02-04 | Improvements in vitamin preparations and process for producing them |
DEL38090A DE1165392B (en) | 1960-02-04 | 1961-02-01 | Substances containing vitamins as admixture to animal feed |
BE599795A BE599795A (en) | 1960-02-04 | 1961-02-02 | Process for the preparation of compositions containing substances endowed with vitamin activity and products obtained |
CH123761A CH418106A (en) | 1960-02-04 | 1961-02-02 | Process for the production of feed additives |
ES0264643A ES264643A1 (en) | 1960-02-04 | 1961-02-03 | Procedure to produce a preparation of vitamin activity (Machine-translation by Google Translate, not legally binding) |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB4065/60A GB970363A (en) | 1960-02-04 | 1960-02-04 | Improvements in vitamin preparations and process for producing them |
Publications (1)
Publication Number | Publication Date |
---|---|
GB970363A true GB970363A (en) | 1964-09-23 |
Family
ID=9770068
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB4065/60A Expired GB970363A (en) | 1960-02-04 | 1960-02-04 | Improvements in vitamin preparations and process for producing them |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE1165392B (en) |
GB (1) | GB970363A (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2204776B (en) * | 1987-04-03 | 1991-02-20 | Nisshin Flour Milling Co | Process for producing vitamin k2-enriched fowl egg |
CN103548764A (en) * | 2013-09-22 | 2014-02-05 | 安徽兴牧畜禽有限公司 | Countryside hill field chicken free-ranging method |
CN103548765A (en) * | 2013-09-22 | 2014-02-05 | 安徽兴牧畜禽有限公司 | Method of feeding chickens scattered in jujubes |
US8809398B2 (en) | 2007-01-16 | 2014-08-19 | Basf Se | Liquid formulations containing a carotinoid |
US9375387B2 (en) | 2008-10-07 | 2016-06-28 | Basf Se | Ready-to-use, stable emulsion |
US11185093B2 (en) | 2007-11-29 | 2021-11-30 | Christian Köpsel | Pulverulent carotenoid preparation for colouring drinks |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2508477A (en) * | 1946-10-16 | 1950-05-23 | Merck & Co Inc | Enriched foodstuffs |
GB704064A (en) * | 1949-09-08 | 1954-02-17 | Vitamins Ltd | Improvements in or relating to vitamin preparations |
FR1056114A (en) * | 1950-12-06 | 1954-02-24 | Philips Nv | Dry vitamin product suitable for dusting, obtained by spray drying, and method of preparation thereof |
US2775521A (en) * | 1953-09-29 | 1956-12-25 | Hoffmann La Roche | Method of fortifying grain products and the resulting product |
US2831770A (en) * | 1954-06-22 | 1958-04-22 | Hoffmann La Roche | Enrichment of cereal grains |
US2895880A (en) * | 1955-05-13 | 1959-07-21 | Smith Kline French Lab | Sustained release pharmaceutical product |
-
1960
- 1960-02-04 GB GB4065/60A patent/GB970363A/en not_active Expired
-
1961
- 1961-02-01 DE DEL38090A patent/DE1165392B/en active Pending
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2204776B (en) * | 1987-04-03 | 1991-02-20 | Nisshin Flour Milling Co | Process for producing vitamin k2-enriched fowl egg |
US8809398B2 (en) | 2007-01-16 | 2014-08-19 | Basf Se | Liquid formulations containing a carotinoid |
US11185093B2 (en) | 2007-11-29 | 2021-11-30 | Christian Köpsel | Pulverulent carotenoid preparation for colouring drinks |
US9375387B2 (en) | 2008-10-07 | 2016-06-28 | Basf Se | Ready-to-use, stable emulsion |
US10004670B2 (en) | 2008-10-07 | 2018-06-26 | Basf Se | Ready-to-use, stable emulsion |
CN103548764A (en) * | 2013-09-22 | 2014-02-05 | 安徽兴牧畜禽有限公司 | Countryside hill field chicken free-ranging method |
CN103548765A (en) * | 2013-09-22 | 2014-02-05 | 安徽兴牧畜禽有限公司 | Method of feeding chickens scattered in jujubes |
CN103548764B (en) * | 2013-09-22 | 2016-05-11 | 安徽兴牧畜禽有限公司 | A kind of rural area hill is raised native chicken method scattered |
CN103548765B (en) * | 2013-09-22 | 2016-09-28 | 安徽兴牧畜禽有限公司 | The feeding method of chicken is raised scattered in a kind of Fructus Jujubae woods |
Also Published As
Publication number | Publication date |
---|---|
DE1165392B (en) | 1964-03-12 |
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