GB963265A - Process for purifying l(+)-lysine - Google Patents

Process for purifying l(+)-lysine

Info

Publication number
GB963265A
GB963265A GB11534/61A GB1153461A GB963265A GB 963265 A GB963265 A GB 963265A GB 11534/61 A GB11534/61 A GB 11534/61A GB 1153461 A GB1153461 A GB 1153461A GB 963265 A GB963265 A GB 963265A
Authority
GB
United Kingdom
Prior art keywords
lysine
monohydrochloride
compound
solution
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB11534/61A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Inventa AG fuer Forschung und Patentverwertung
Original Assignee
Inventa AG fuer Forschung und Patentverwertung
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inventa AG fuer Forschung und Patentverwertung filed Critical Inventa AG fuer Forschung und Patentverwertung
Publication of GB963265A publication Critical patent/GB963265A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00—Preparation of nitrogen-containing organic compounds
    • C12P13/04—Alpha- or beta- amino acids
    • C12P13/08—Lysine; Diaminopimelic acid; Threonine; Valine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/26—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one amino group bound to the carbon skeleton, e.g. lysine

Landscapes

  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L(+)-Lysine-monohydrochloride of optical purity better than 99% is prepared by evaporating an unsaturated aqueous solution of L(+)- and DL-lysine monohydrochlorides of optical purity 80-99%.L(+)-lysine to a concentration of the L compound such that at a temperature lower than the evaporation temperature the solution would be saturated with L compound, cooling the solution to the lower temperature while seeding with DL-lysine-monohydrochloride, separating the precipitate of DL and some L compound, and recovering L(+)-lysine monohydrochloride from the mother liquor.
GB11534/61A 1960-04-07 1961-03-29 Process for purifying l(+)-lysine Expired GB963265A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH394160A CH377368A (en) 1960-04-07 1960-04-07 Process for the purification of 1 (+) - lysine

Publications (1)

Publication Number Publication Date
GB963265A true GB963265A (en) 1964-07-08

Family

ID=4266770

Family Applications (1)

Application Number Title Priority Date Filing Date
GB11534/61A Expired GB963265A (en) 1960-04-07 1961-03-29 Process for purifying l(+)-lysine

Country Status (3)

Country Link
BE (1) BE602174A (en)
CH (1) CH377368A (en)
GB (1) GB963265A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5118414B1 (en) * 1967-01-11 1976-06-09
EP0424028A2 (en) * 1989-10-17 1991-04-24 Merck & Co. Inc. S(+)-ibuprofen-L-amino acid and S(+)-ibuprofen-D-amino acid as onset hastened enhanced analgesics

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5118414B1 (en) * 1967-01-11 1976-06-09
EP0424028A2 (en) * 1989-10-17 1991-04-24 Merck & Co. Inc. S(+)-ibuprofen-L-amino acid and S(+)-ibuprofen-D-amino acid as onset hastened enhanced analgesics
EP0424028A3 (en) * 1989-10-17 1992-06-10 Merck & Co. Inc. S(+)-ibuprofen-l-amino acid and s(+)-ibuprofen-d-amino acid as onset hastened enhanced analgesics

Also Published As

Publication number Publication date
BE602174A (en) 1961-07-31
CH377368A (en) 1964-05-15

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