GB909245A - Improvements in or relating to the manufacture of metal halides - Google Patents
Improvements in or relating to the manufacture of metal halidesInfo
- Publication number
- GB909245A GB909245A GB13913/60A GB1391360A GB909245A GB 909245 A GB909245 A GB 909245A GB 13913/60 A GB13913/60 A GB 13913/60A GB 1391360 A GB1391360 A GB 1391360A GB 909245 A GB909245 A GB 909245A
- Authority
- GB
- United Kingdom
- Prior art keywords
- oxide particles
- cracking
- particles
- via line
- chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
- C22B34/1222—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes using a halogen containing agent
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F3/00—Compounds of beryllium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/26—Magnesium halides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/48—Halides, with or without other cations besides aluminium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/48—Halides, with or without other cations besides aluminium
- C01F7/56—Chlorides
- C01F7/58—Preparation of anhydrous aluminium chloride
- C01F7/60—Preparation of anhydrous aluminium chloride from oxygen-containing aluminium compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G1/00—Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
- C01G1/06—Halides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G33/00—Compounds of niobium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G35/00—Compounds of tantalum
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
<PICT:0909245/III/1> Metal halides, especially of magnesium, vanadium, tantalum, titanium, aluminium, zirconium, niobium, or beryllium, are prepared by cracking one or more gaseous hydrocarbons in contact with metal oxide particles at a temperature above 900 DEG C., and thereafter reacting the resultant carbon coated particles with at least one halogen at a temperature below 1400 DEG C. The cracking is preferably effected at 1100 DEG -1400 DEG C. The hydrocarbon preferably does not contain more than 4 carbon atoms, for example methane, and oxygen or an oxygen-containing gas may also be present. The gases resulting from the cracking may be burnt to heat the oxide particles. The oxide particles may be treated in stationary or fluidized beds, or in moving masses. In Fig. 1, metal oxide particles are preheated in combustion chamber 1 by the burning of cracked gases from chamber 2, and the particles then pass to chamber 2, where they are contacted with hydrocarbon gases entering via line 8, thereby coating the particles with carbon, which then pass to halogenation chamber 3 and contacted with halogen entering via line 13. The halide product is either withdrawn via line 7, or if in the vapour from either via line 15 or via heat exchanger 16 and line 18. The oxide particles are preferably below 20 mm. in diameter. The halogenation and cracking may be effected in the same zone.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR792933A FR1232489A (en) | 1959-04-23 | 1959-04-23 | Process for the preparation of metal halides or the like |
| FR819006A FR91101E (en) | 1959-04-23 | 1960-02-19 | Process for the preparation of metal halides or the like |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB909245A true GB909245A (en) | 1962-10-31 |
Family
ID=26183965
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB13913/60A Expired GB909245A (en) | 1959-04-23 | 1960-04-20 | Improvements in or relating to the manufacture of metal halides |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE590043A (en) |
| ES (1) | ES257515A1 (en) |
| FR (1) | FR91101E (en) |
| GB (1) | GB909245A (en) |
-
1960
- 1960-02-19 FR FR819006A patent/FR91101E/en not_active Expired
- 1960-04-20 GB GB13913/60A patent/GB909245A/en not_active Expired
- 1960-04-21 ES ES0257515A patent/ES257515A1/en not_active Expired
- 1960-04-22 BE BE590043A patent/BE590043A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES257515A1 (en) | 1960-12-01 |
| FR91101E (en) | 1968-04-19 |
| BE590043A (en) | 1960-10-24 |
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