GB895119A - Process for purifying impure cresols, particularly those with a strong odour - Google Patents

Process for purifying impure cresols, particularly those with a strong odour

Info

Publication number
GB895119A
GB895119A GB26916/58A GB2691658A GB895119A GB 895119 A GB895119 A GB 895119A GB 26916/58 A GB26916/58 A GB 26916/58A GB 2691658 A GB2691658 A GB 2691658A GB 895119 A GB895119 A GB 895119A
Authority
GB
United Kingdom
Prior art keywords
cresol
cresolate
solution
cresols
aqueous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB26916/58A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Leuna Werke GmbH
Leuna Werke Walter Ulbright Germany VEB
Original Assignee
Leuna Werke GmbH
Leuna Werke Walter Ulbright Germany VEB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Leuna Werke GmbH, Leuna Werke Walter Ulbright Germany VEB filed Critical Leuna Werke GmbH
Publication of GB895119A publication Critical patent/GB895119A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/86Purification; separation; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A process for the purification of impure cresols, particularly those with a strong odour, consists in first converting the impure cresol into an aqueous cresolate solution, then extracting the aqueous cresolate solution with cresol or one of its homologues in which the cresolate is insoluble or difficulty soluble to remove the impurities and separating the purified aqueous cresolate from the cresol or homologue thereof containing the impurities and treating said purified aqueous cresolate by known means to regenerate cresol and then recovering same from the aqueous solution. The term "cresols" is intended to include mixtures of isomeric cresols with homologous alkyl phenols and homogenous cresols such as o-, m- or p-cresol. The process may be carried out by converting the cresol or cresol mixture with, e.g. lime in the presence of water into an aqueous calcium cresolate solution diluting such solution with water so that part of the cresol separates and contains the impurities, the polluted cresol is separated and the remaining pure cresolate solution is treated to liberate and separate cresol, e.g. by acidification with hydrochloric acid and distillation.
GB26916/58A 1958-01-10 1958-08-21 Process for purifying impure cresols, particularly those with a strong odour Expired GB895119A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AT895119X 1958-01-10

Publications (1)

Publication Number Publication Date
GB895119A true GB895119A (en) 1962-05-02

Family

ID=3682854

Family Applications (1)

Application Number Title Priority Date Filing Date
GB26916/58A Expired GB895119A (en) 1958-01-10 1958-08-21 Process for purifying impure cresols, particularly those with a strong odour

Country Status (1)

Country Link
GB (1) GB895119A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5750009A (en) * 1994-08-31 1998-05-12 Dakota Gasification Company Method for purifying natural cresylic acid mixtures

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5750009A (en) * 1994-08-31 1998-05-12 Dakota Gasification Company Method for purifying natural cresylic acid mixtures

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