GB878101A - Process for the manufacture of titanium disulphide - Google Patents

Process for the manufacture of titanium disulphide

Info

Publication number
GB878101A
GB878101A GB2889558A GB2889558A GB878101A GB 878101 A GB878101 A GB 878101A GB 2889558 A GB2889558 A GB 2889558A GB 2889558 A GB2889558 A GB 2889558A GB 878101 A GB878101 A GB 878101A
Authority
GB
United Kingdom
Prior art keywords
chamber
hydrogen sulphide
titanium tetrachloride
vapour
titanium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2889558A
Inventor
Howard Arthur Stanley Bristow
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Laporte Titanium Ltd
Original Assignee
Laporte Titanium Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Laporte Titanium Ltd filed Critical Laporte Titanium Ltd
Priority to GB2889558A priority Critical patent/GB878101A/en
Publication of GB878101A publication Critical patent/GB878101A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/007—Titanium sulfides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Titanium disulphide is prepared by reacting titanium tetrachloride vapour and hydrogen sulphide in a chamber at 450 DEG C. to 600 DEG C. in the presence of water vapour present in a proportion of 1 to 50 milligrams of water per litre of hydrogen sulphide (measured at 15 DEG C. and 760 mm. pressure). The titanium tetrachloride vapour may be mixed with an inert gas, e.g. nitrogen, and the water vapour may be introduced into the chamber mixed with the hydrogen sulphide. The titanium tetrachloride and hydrogen sulphide may be introduced by jets close together and remote from the walls of the chamber, or they may be introduced into and reacted in a bed of fluidized particles. The reactants may be wholly or partially preheated before entering the chamber. An example is given. Specification 866,363 is referred to.
GB2889558A 1958-09-09 1958-09-09 Process for the manufacture of titanium disulphide Expired GB878101A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2889558A GB878101A (en) 1958-09-09 1958-09-09 Process for the manufacture of titanium disulphide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2889558A GB878101A (en) 1958-09-09 1958-09-09 Process for the manufacture of titanium disulphide

Publications (1)

Publication Number Publication Date
GB878101A true GB878101A (en) 1961-09-27

Family

ID=10282921

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2889558A Expired GB878101A (en) 1958-09-09 1958-09-09 Process for the manufacture of titanium disulphide

Country Status (1)

Country Link
GB (1) GB878101A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4137297A (en) * 1977-12-01 1979-01-30 Laporte Industries Limited Process for the production of titanium disulphide
US4259310A (en) * 1980-01-28 1981-03-31 Kerr-Mcgee Chemical Corporation Process for the manufacture of titanium disulfide
DE2945306A1 (en) * 1979-11-09 1981-05-21 Degussa Ag, 6000 Frankfurt METHOD FOR PRODUCING HIGH PURE PURITY TITANE DISULFIDE AND STOECHIOMETRIC COMPOSITION

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4137297A (en) * 1977-12-01 1979-01-30 Laporte Industries Limited Process for the production of titanium disulphide
DE2945306A1 (en) * 1979-11-09 1981-05-21 Degussa Ag, 6000 Frankfurt METHOD FOR PRODUCING HIGH PURE PURITY TITANE DISULFIDE AND STOECHIOMETRIC COMPOSITION
US4337239A (en) * 1979-11-09 1982-06-29 Degussa Aktiengesellschaft Process for the production of titanium disulfide of high purity and stoichiometric composition
US4259310A (en) * 1980-01-28 1981-03-31 Kerr-Mcgee Chemical Corporation Process for the manufacture of titanium disulfide

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