GB829439A - New phenol ethers of vitamin bí¬factor iii - Google Patents
New phenol ethers of vitamin bí¬factor iiiInfo
- Publication number
- GB829439A GB829439A GB219757A GB219757A GB829439A GB 829439 A GB829439 A GB 829439A GB 219757 A GB219757 A GB 219757A GB 219757 A GB219757 A GB 219757A GB 829439 A GB829439 A GB 829439A
- Authority
- GB
- United Kingdom
- Prior art keywords
- ether
- factor iii
- vitamin
- hydroxy
- dinitro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon, or a metal, e.g. chelates, vitamin B12
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03B—APPARATUS OR ARRANGEMENTS FOR TAKING PHOTOGRAPHS OR FOR PROJECTING OR VIEWING THEM; APPARATUS OR ARRANGEMENTS EMPLOYING ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ACCESSORIES THEREFOR
- G03B15/00—Special procedures for taking photographs; Apparatus therefor
- G03B15/02—Illuminating scene
- G03B15/03—Combinations of cameras with lighting apparatus; Flash units
- G03B15/04—Combinations of cameras with non-electronic flash apparatus; Non-electronic flash units
- G03B15/041—Separatable flash apparatus; Means for mounting the flash apparatus on the photographic apparatus
- G03B15/0431—Rotatable mounting means
Abstract
The invention comprises Vitamin B12 Factor III in which the phenolic hydroxy group in the basic part of Factor III has been converted into the methyl ether, the ethyl ether, the allyl ether, the b -hydroxyethyl ether, the benzyl ether, the 2,4-dinitrophenyl-(1) ether, 2,4-dinitro - 5 - hydroxy - phenyl - (1) ether, 2,4 - dinitro - 5 - benzoxyphenyl - (1) ether and 2,4,21,41 - tetranitro - 51 - hydroxy - diphenyl (5) ether, and a process for the production of new derivatives of Vitamin B12 Factor III in which the phenolic hydroxyl group in the basic part of Factor III is etherified characterized in that an etherifying agent is allowed to react with the Factor III in a weakly alkaline medium, and the ether obtained thereby isolated. The etherification may be effected with an alkylating or arylating agent in the temperature range 20-60 DEG C. and subsequently traces of etherification agent removed by adding an aqueous phenol solution. As weakly alkaline medium there may be used an alkali carbonate or bicarbonate. Further purification may be effected by means of chromatography or electrophoresis.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEA0025353 | 1956-07-21 | ||
DEA25664A DE1017325B (en) | 1956-07-21 | 1956-09-13 | Method for separating vitamin B factor III from other B species |
DEA25843A DE1055539B (en) | 1956-07-21 | 1956-10-11 | Process for the production of ethers of the vitamin B group |
DEA26307A DE1054461B (en) | 1956-07-21 | 1957-01-02 | Process for the production of ethers of the vitamin B group |
Publications (1)
Publication Number | Publication Date |
---|---|
GB829439A true GB829439A (en) | 1960-03-02 |
Family
ID=41059885
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB219757A Expired GB829439A (en) | 1956-07-21 | 1957-01-21 | New phenol ethers of vitamin bí¬factor iii |
Country Status (3)
Country | Link |
---|---|
DE (4) | DE1020440B (en) |
FR (1) | FR1326303A (en) |
GB (1) | GB829439A (en) |
-
1956
- 1956-07-21 DE DEA25352A patent/DE1020440B/en active Pending
- 1956-09-13 DE DEA25664A patent/DE1017325B/en active Pending
- 1956-10-11 DE DEA25843A patent/DE1055539B/en active Pending
-
1957
- 1957-01-02 DE DEA26307A patent/DE1054461B/en active Pending
- 1957-01-21 GB GB219757A patent/GB829439A/en not_active Expired
- 1957-01-23 FR FR13017583A patent/FR1326303A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE1055539B (en) | 1959-04-23 |
DE1020440B (en) | 1957-12-05 |
FR1326303A (en) | 1963-05-10 |
DE1054461B (en) | 1959-04-09 |
DE1017325B (en) | 1957-10-10 |
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