GB819302A - Improvements in or relating to method of decomposing double salts by heat and apparatus therefor - Google Patents
Improvements in or relating to method of decomposing double salts by heat and apparatus thereforInfo
- Publication number
- GB819302A GB819302A GB364055A GB364055A GB819302A GB 819302 A GB819302 A GB 819302A GB 364055 A GB364055 A GB 364055A GB 364055 A GB364055 A GB 364055A GB 819302 A GB819302 A GB 819302A
- Authority
- GB
- United Kingdom
- Prior art keywords
- retort
- ammonium
- stainless steel
- fluoride
- decomposition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003839 salts Chemical class 0.000 title abstract 4
- XWSCPZIYKQVRKD-UHFFFAOYSA-N azanium;beryllium;fluoride Chemical compound [Be].[NH4+].[F-] XWSCPZIYKQVRKD-UHFFFAOYSA-N 0.000 abstract 3
- 229910001220 stainless steel Inorganic materials 0.000 abstract 3
- 239000010935 stainless steel Substances 0.000 abstract 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- LWBPNIJBHRISSS-UHFFFAOYSA-L beryllium dichloride Chemical compound Cl[Be]Cl LWBPNIJBHRISSS-UHFFFAOYSA-L 0.000 abstract 2
- 238000000354 decomposition reaction Methods 0.000 abstract 2
- 239000007789 gas Substances 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- DDFHBQSCUXNBSA-UHFFFAOYSA-N 5-(5-carboxythiophen-2-yl)thiophene-2-carboxylic acid Chemical compound S1C(C(=O)O)=CC=C1C1=CC=C(C(O)=O)S1 DDFHBQSCUXNBSA-UHFFFAOYSA-N 0.000 abstract 1
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- 229910052786 argon Inorganic materials 0.000 abstract 1
- 229910001627 beryllium chloride Inorganic materials 0.000 abstract 1
- JZKFIPKXQBZXMW-UHFFFAOYSA-L beryllium difluoride Chemical compound F[Be]F JZKFIPKXQBZXMW-UHFFFAOYSA-L 0.000 abstract 1
- 229910001633 beryllium fluoride Inorganic materials 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 229910002804 graphite Inorganic materials 0.000 abstract 1
- 239000010439 graphite Substances 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 238000005470 impregnation Methods 0.000 abstract 1
- 230000006698 induction Effects 0.000 abstract 1
- 206010022000 influenza Diseases 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 230000005855 radiation Effects 0.000 abstract 1
- 229910010271 silicon carbide Inorganic materials 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 238000004227 thermal cracking Methods 0.000 abstract 1
- 238000005979 thermal decomposition reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B35/00—Obtaining beryllium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J6/00—Heat treatments such as Calcining; Fusing ; Pyrolysis
- B01J6/005—Fusing
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F3/00—Compounds of beryllium
- C01F3/005—Fluorides or double fluorides of beryllium with alkali metals or ammonium; Preparation of beryllium compounds therefrom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Vertical, Hearth, Or Arc Furnaces (AREA)
Abstract
819,302. Retorts ; decomposing double salts ; beryllium fluoride. UNITED KINGDOM ATOMIC ENERGY AUTHORITY. Feb. 27, 1956 [Feb. 8, 1955], No. 3640/55. Classes 1 (1) and 1 (3). [Also in Group XII] A double salt, such as ammonium beryllium fluoride, which is liable to froth on thermal decomposition is scattered over the hearth of a retort heated at the bottom sufficiently to melt the solid formed by decomposition and at the roof to a higher temperature such that radiation from the roof will bring about decomposition of the double salt. In the described embodiment (see Fig. 1), a stainless steel ram 8 operating in a carbon-lined water-jacketed stainless steel tube 6 connected to a source of argon, is used to scatter ammonium beryllium fluoride after the hearth of a retort 1 lined with graphite rendered impervious by impregnation with a hydrocarbon followed by thermal cracking thereof. The retort is heated from below to 800-850 ‹ C. by means of gases passing through a lower heating chamber 3 and from above to 1200-1250‹ C. by means of burner gases in chamber 13 having a baffle 14. Alternatively, electrical resistance or induction heating may be employed. Molten beryllium chloride is tapped off into preheated moulds through stainless steel orifice 9a closed by carbon valve 9 whilst ammonium fluoride vapour is recovered in a condenser or scrubber for reuse in the production of further ammonium beryllium fluoride. The parts of the supporting structure 2 adjacent to the chambers and flues are made of molochite and the sheath 1a of the retort is protected where exposed by means of carborundum.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB364055A GB819302A (en) | 1955-02-08 | 1955-02-08 | Improvements in or relating to method of decomposing double salts by heat and apparatus therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB364055A GB819302A (en) | 1955-02-08 | 1955-02-08 | Improvements in or relating to method of decomposing double salts by heat and apparatus therefor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB819302A true GB819302A (en) | 1959-09-02 |
Family
ID=9762137
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB364055A Expired GB819302A (en) | 1955-02-08 | 1955-02-08 | Improvements in or relating to method of decomposing double salts by heat and apparatus therefor |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB819302A (en) |
-
1955
- 1955-02-08 GB GB364055A patent/GB819302A/en not_active Expired
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