GB761430A - Process of preparing silica-alumina catalysts - Google Patents

Process of preparing silica-alumina catalysts

Info

Publication number
GB761430A
GB761430A GB36486/54A GB3648654A GB761430A GB 761430 A GB761430 A GB 761430A GB 36486/54 A GB36486/54 A GB 36486/54A GB 3648654 A GB3648654 A GB 3648654A GB 761430 A GB761430 A GB 761430A
Authority
GB
United Kingdom
Prior art keywords
alumina
silica
hydrosol
drying
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB36486/54A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WR Grace and Co
Original Assignee
WR Grace and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WR Grace and Co filed Critical WR Grace and Co
Publication of GB761430A publication Critical patent/GB761430A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/12Silica and alumina

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Silicon Compounds (AREA)

Abstract

A silica/alumina catalyst is produced by forming an alkaline silica hydrosol, preferably formed at pH between 9.5 and 10.5; allowing the hydrosol to gel, preferably in aqueous slurry; co-mingling with resultant alkaline hydrogel sufficient aluminium sulphate solution, preferably of pH 1, to provide the desired alumina concentration in the final product; adding sufficient ammonia to effect precipitation of alumina; if desired ageing the mixture which usually has a pH of about 7.5 for about 15 minutes when the pH is about 7.0; finally washing and drying the product. The hydrosol may be formed from sodium silicate and a mineral acid, preferably sulphuric acid. The composition of the catalyst is preferably 87/13 silica/ alumina. Drying before the final washing and drying is a preferred feature. Comparison of the catalytic properties is made with the similar product produced according to Specification 753,695.
GB36486/54A 1953-12-29 1954-12-16 Process of preparing silica-alumina catalysts Expired GB761430A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US761430XA 1953-12-29 1953-12-29

Publications (1)

Publication Number Publication Date
GB761430A true GB761430A (en) 1956-11-14

Family

ID=22130176

Family Applications (1)

Application Number Title Priority Date Filing Date
GB36486/54A Expired GB761430A (en) 1953-12-29 1954-12-16 Process of preparing silica-alumina catalysts

Country Status (1)

Country Link
GB (1) GB761430A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111672494A (en) * 2020-06-10 2020-09-18 江苏扬农化工集团有限公司 Preparation method of composite catalyst for synthesizing hexamethylene diamine intermediate and application of composite catalyst

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111672494A (en) * 2020-06-10 2020-09-18 江苏扬农化工集团有限公司 Preparation method of composite catalyst for synthesizing hexamethylene diamine intermediate and application of composite catalyst
CN111672494B (en) * 2020-06-10 2023-06-02 江苏扬农化工集团有限公司 Preparation method of composite catalyst for synthesizing hexamethylenediamine intermediate and application of composite catalyst

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