GB751045A - Improvements in the production of low density metal powders - Google Patents

Improvements in the production of low density metal powders

Info

Publication number
GB751045A
GB751045A GB11760/54A GB1176054A GB751045A GB 751045 A GB751045 A GB 751045A GB 11760/54 A GB11760/54 A GB 11760/54A GB 1176054 A GB1176054 A GB 1176054A GB 751045 A GB751045 A GB 751045A
Authority
GB
United Kingdom
Prior art keywords
carbonyl
temperature
powder
low density
free space
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB11760/54A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Badische Anilin and Sodafabrik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE, Badische Anilin and Sodafabrik AG filed Critical BASF SE
Publication of GB751045A publication Critical patent/GB751045A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/16Making metallic powder or suspensions thereof using chemical processes
    • B22F9/30Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis
    • B22F9/305Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis of metal carbonyls

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

Low density metal powder, e.g. having a bulk density of less than 0,9 Kg per litre, is produced by the thermal decomposition of metal carbonyls in the free space of a heated vessel by keeping the temperature of the wall of the vessel, particularly at the point of entry of the carbonyl, at least 270 DEG C. higher than the temperature at the middle of the free space. The temperature difference may be achieved by (a) increasing the rate of carbonyl feed, (b) increasing the supply of heat to the walls or (c) the supply of cold gases or vapours. To produce very low density powders, the temperature at the middle of the free space is kept below 300 DEG C., e.g. at 230 DEG C., by supplying carbonyl to the decomposition chamber in such an amount that the effluent carbon monoxide contains undecomposed carbonyl which has, however, a partial pressure considerably below the saturation pressure of the carbonyl at room temperature. An example of the production of Ni powder is given. Ni powder and Fe-Ni powder produced by the process may be used for the manufacture of electrode frameworks, for alkaline accumulators and for porous plates and tubes. Specification 679,439 is referred to.
GB11760/54A 1953-04-24 1954-04-23 Improvements in the production of low density metal powders Expired GB751045A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE751045X 1953-04-24

Publications (1)

Publication Number Publication Date
GB751045A true GB751045A (en) 1956-06-27

Family

ID=6651290

Family Applications (1)

Application Number Title Priority Date Filing Date
GB11760/54A Expired GB751045A (en) 1953-04-24 1954-04-23 Improvements in the production of low density metal powders

Country Status (1)

Country Link
GB (1) GB751045A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2900245A (en) * 1957-01-24 1959-08-18 Gen Aniline & Film Corp Production of finely divided metals

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2900245A (en) * 1957-01-24 1959-08-18 Gen Aniline & Film Corp Production of finely divided metals

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