GB728947A - Reagent for the quantitative determination of very small amounts of water in gases, liquids and solid substances, and method of preparing the reagent - Google Patents
Reagent for the quantitative determination of very small amounts of water in gases, liquids and solid substances, and method of preparing the reagentInfo
- Publication number
- GB728947A GB728947A GB998953A GB998953A GB728947A GB 728947 A GB728947 A GB 728947A GB 998953 A GB998953 A GB 998953A GB 998953 A GB998953 A GB 998953A GB 728947 A GB728947 A GB 728947A
- Authority
- GB
- United Kingdom
- Prior art keywords
- reagent
- sodium
- water
- liquids
- gases
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/16—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using titration
- G01N31/168—Determining water content by using Karl Fischer reagent
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
A reagent for use in the quantitative determination of water in gases, liquids, or solids, comprises a solution in methyl alcohol of iodine and sulphur dioxide, to which has been added an alcoholate, phenolate, or salt of an organic acid, which serves to bind the hydrogen ions produced during the water determination. Sodium, potassium, calcium, strontium, barium, magnesium, or zinc salts may be used. In examples, sodium methylate, sodium phenolate, sodium acetate, or a mixture of sodium acetate and zinc acetate are added. The reagent may also contain sodium iodide.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BE519298D BE519298A (en) | 1953-04-13 | ||
GB998953A GB728947A (en) | 1953-04-13 | 1953-04-13 | Reagent for the quantitative determination of very small amounts of water in gases, liquids and solid substances, and method of preparing the reagent |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB998953A GB728947A (en) | 1953-04-13 | 1953-04-13 | Reagent for the quantitative determination of very small amounts of water in gases, liquids and solid substances, and method of preparing the reagent |
Publications (1)
Publication Number | Publication Date |
---|---|
GB728947A true GB728947A (en) | 1955-04-27 |
Family
ID=9882493
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB998953A Expired GB728947A (en) | 1953-04-13 | 1953-04-13 | Reagent for the quantitative determination of very small amounts of water in gases, liquids and solid substances, and method of preparing the reagent |
Country Status (2)
Country | Link |
---|---|
BE (1) | BE519298A (en) |
GB (1) | GB728947A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4550083A (en) * | 1982-02-12 | 1985-10-29 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Karl-Fischer reagent and procedure for the determination of water using it |
EP0159518A1 (en) * | 1984-03-27 | 1985-10-30 | MERCK PATENT GmbH | Karl Fischer reagent and method for the determination of water using this reagent |
US4703014A (en) * | 1984-02-27 | 1987-10-27 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Karl-Fischer reagent and process for the determination of water |
FR2737921A1 (en) * | 1995-08-15 | 1997-02-21 | Israel State | REAGENT FOR THE DETERMINATION OF WATER AND ENE DIOLS OR THIOLS |
-
0
- BE BE519298D patent/BE519298A/xx unknown
-
1953
- 1953-04-13 GB GB998953A patent/GB728947A/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4550083A (en) * | 1982-02-12 | 1985-10-29 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Karl-Fischer reagent and procedure for the determination of water using it |
US4703014A (en) * | 1984-02-27 | 1987-10-27 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Karl-Fischer reagent and process for the determination of water |
EP0159518A1 (en) * | 1984-03-27 | 1985-10-30 | MERCK PATENT GmbH | Karl Fischer reagent and method for the determination of water using this reagent |
US4647542A (en) * | 1984-03-27 | 1987-03-03 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Karl Fischer reagent and method for determining water by means of this reagent |
FR2737921A1 (en) * | 1995-08-15 | 1997-02-21 | Israel State | REAGENT FOR THE DETERMINATION OF WATER AND ENE DIOLS OR THIOLS |
Also Published As
Publication number | Publication date |
---|---|
BE519298A (en) |
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