GB637025A - Improvements in or relating to a method of insolubilising continuously travelling tows of artificial filamentary products - Google Patents

Improvements in or relating to a method of insolubilising continuously travelling tows of artificial filamentary products

Info

Publication number
GB637025A
GB637025A GB26790/47A GB2679047A GB637025A GB 637025 A GB637025 A GB 637025A GB 26790/47 A GB26790/47 A GB 26790/47A GB 2679047 A GB2679047 A GB 2679047A GB 637025 A GB637025 A GB 637025A
Authority
GB
United Kingdom
Prior art keywords
tow
saturated
solution
acidified
passed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB26790/47A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Publication of GB637025A publication Critical patent/GB637025A/en
Expired legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F4/00Monocomponent artificial filaments or the like of proteins; Manufacture thereof
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D10/00Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
    • D01D10/04Supporting filaments or the like during their treatment
    • D01D10/0436Supporting filaments or the like during their treatment while in continuous movement
    • D01D10/0481Supporting filaments or the like during their treatment while in continuous movement the filaments passing through a tube

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Artificial Filaments (AREA)
  • Peptides Or Proteins (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

Continuously travelling tows of artificial filamentary products obtained by spinning solutions of vegetable seed globulins or phospho-proteins in aqueous alkaline or other aqueous solvent media into acidified saline coagulating baths, are insolubilized by advancing the tow through a tubular passage by means of a turbulent stream of an aqueous formaldehyde solution saturated with sodium chloride and containing sodium sulphate or magnesium sulphate and having a pH of 4 to 6, and then advancing the treated tow through <PICT:0637025/IV (a)/1> another tubular passage by means of a turbulent stream of an aqueous formaldehyde solution strongly acidified with sulphuric acid and saturated with sodium sulphate or magnesium sulphate, this second solution being at a higher temperature than the first. The vegetable seed globulins may be peanut proteins, and the phospho-protein may be casein. The tubular passage is preferably of narrow diameter and may be either straight or arranged in helical form, but in both cases the liquid is passed through under such conditions as to be in turbulent flow. In the example, a matured caustic soda solution of groundnut globulin prepared from a solution containing peanut globulin, caustic soda and sodium sulphite is extruded through a spinneret 1 into a coagulating bath 2 containing sodium sulphate and sulphuric acid. The resulting tow 3 is then stretched between godets 4 and 5 and led over godet 6 through a device 8 having a reciprocating motion radial to the centre of the ring trough 7 and into the trough, which contains a saturated acidified solution of sodium chloride. The tow is taken up and stretched between godets 1 and 12, passed over godet 13 and then through a vertical helical coil 15 through which a formaldehyde solution saturated with sodium chloride and containing sodium sulphate is passed at 70 DEG C. After stretching between godets 17 and 18 the tow is passed through another helical coil 20 containing a formaldehyde solution acidified with sulphuric acid and saturated with sodium sulphate at 95 DEG C., and is finally washed and dried. Specifications 513,910, 597,497 and 623,460 are referred to.
GB26790/47A 1947-10-06 1947-10-06 Improvements in or relating to a method of insolubilising continuously travelling tows of artificial filamentary products Expired GB637025A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB276372X 1947-10-06

Publications (1)

Publication Number Publication Date
GB637025A true GB637025A (en) 1950-05-10

Family

ID=10262835

Family Applications (1)

Application Number Title Priority Date Filing Date
GB26790/47A Expired GB637025A (en) 1947-10-06 1947-10-06 Improvements in or relating to a method of insolubilising continuously travelling tows of artificial filamentary products

Country Status (7)

Country Link
US (1) US2565908A (en)
BE (1) BE485166A (en)
CH (1) CH276372A (en)
DE (1) DE848847C (en)
FR (1) FR970037A (en)
GB (1) GB637025A (en)
NL (1) NL68974C (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE505443A (en) * 1950-08-28
JPS5452749A (en) * 1977-09-30 1979-04-25 Kuraray Co Production of fibrous high protein food

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE458719A (en) * 1940-08-29
US2428603A (en) * 1941-10-29 1947-10-07 Nat Dairy Prod Corp Process for hardening protein fibre
GB564591A (en) * 1943-01-28 1944-10-04 Courtaulds Ltd Improvements in the manufacture and production of artificial threads, filaments and the like
US2429214A (en) * 1944-01-11 1947-10-21 Du Pont Shaped protein structures and their preparation
US2409475A (en) * 1944-01-11 1946-10-15 Du Pont Shaped protein structures and their preparation

Also Published As

Publication number Publication date
DE848847C (en) 1952-09-08
CH276372A (en) 1951-07-15
FR970037A (en) 1950-12-28
NL68974C (en)
US2565908A (en) 1951-08-28
BE485166A (en)

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