GB630644A - Improvements in and relating to the preparation of tetramethyl silicate - Google Patents
Improvements in and relating to the preparation of tetramethyl silicateInfo
- Publication number
- GB630644A GB630644A GB16793/47A GB1679347A GB630644A GB 630644 A GB630644 A GB 630644A GB 16793/47 A GB16793/47 A GB 16793/47A GB 1679347 A GB1679347 A GB 1679347A GB 630644 A GB630644 A GB 630644A
- Authority
- GB
- United Kingdom
- Prior art keywords
- copper
- silicon
- silicate
- compound
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 title abstract 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 6
- 229910052802 copper Inorganic materials 0.000 abstract 6
- 239000010949 copper Substances 0.000 abstract 6
- 239000010703 silicon Substances 0.000 abstract 4
- 239000005749 Copper compound Substances 0.000 abstract 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 3
- 150000001880 copper compounds Chemical class 0.000 abstract 3
- 229910052710 silicon Inorganic materials 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 229910000676 Si alloy Inorganic materials 0.000 abstract 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 abstract 1
- 150000001242 acetic acid derivatives Chemical class 0.000 abstract 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- WCCJDBZJUYKDBF-UHFFFAOYSA-N copper silicon Chemical compound [Si].[Cu] WCCJDBZJUYKDBF-UHFFFAOYSA-N 0.000 abstract 1
- BERDEBHAJNAUOM-UHFFFAOYSA-N copper(I) oxide Inorganic materials [Cu]O[Cu] BERDEBHAJNAUOM-UHFFFAOYSA-N 0.000 abstract 1
- KRFJLUBVMFXRPN-UHFFFAOYSA-N cuprous oxide Chemical compound [O-2].[Cu+].[Cu+] KRFJLUBVMFXRPN-UHFFFAOYSA-N 0.000 abstract 1
- 229940112669 cuprous oxide Drugs 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 abstract 1
- 150000004675 formic acid derivatives Chemical class 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
- 150000004679 hydroxides Chemical class 0.000 abstract 1
- 238000007689 inspection Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000002823 nitrates Chemical class 0.000 abstract 1
- 150000002825 nitriles Chemical class 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 229910052814 silicon oxide Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/04—Esters of silicic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
Tetramethyl silicate is prepared by passing methyl alcohol through the interstices of a mass consisting of silicon with copper or with a compound yielding copper under the conditions of the reaction, the temperature of said mass being within the range 150 DEG to 450 DEG C. Suitable copper compounds are oxides, hydroxides, halides, nitrates, acetates, formates, carbonates or cyanides of copper. By weight, from about 2 to 50 per cent of copper or copper compound may be used based on the total weight of the silicon and copper or copper compound. In examples, methyl silicate is prepared by passing methyl alcohol over heated powdered copper and silicon, copper-silicon alloy, and a mixture of silicon and cuprous oxide powders. The Specification as open to inspection under Sect. 91 refers to the preparation of tetraethyl silicate from ethyl alcohol by the above method. This subject-matter does not appear in the Specification as accepted.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US630644XA | 1946-06-26 | 1946-06-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB630644A true GB630644A (en) | 1949-10-18 |
Family
ID=22046677
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB16793/47A Expired GB630644A (en) | 1946-06-26 | 1947-06-25 | Improvements in and relating to the preparation of tetramethyl silicate |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB630644A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4447632A (en) * | 1983-04-18 | 1984-05-08 | Union Carbide Corporation | Process for production of alkyl silicates from silicon metal |
-
1947
- 1947-06-25 GB GB16793/47A patent/GB630644A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4447632A (en) * | 1983-04-18 | 1984-05-08 | Union Carbide Corporation | Process for production of alkyl silicates from silicon metal |
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