GB611417A - Preparation of guanidine - Google Patents

Preparation of guanidine

Info

Publication number
GB611417A
GB611417A GB33555/45A GB3355545A GB611417A GB 611417 A GB611417 A GB 611417A GB 33555/45 A GB33555/45 A GB 33555/45A GB 3355545 A GB3355545 A GB 3355545A GB 611417 A GB611417 A GB 611417A
Authority
GB
United Kingdom
Prior art keywords
ammonium
sulphamate
reaction
guanidine
imidodisulphonate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB33555/45A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beazer East Inc
Original Assignee
Koppers Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Koppers Co Inc filed Critical Koppers Co Inc
Publication of GB611417A publication Critical patent/GB611417A/en
Expired legal-status Critical Current

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Abstract

A guanidine salt is obtained by heating ammonium thiocyanate, thiurea, or a mixture thereof to a temperature of 80-250 DEG C. in contact with an inorganic non-acidic compound having in its structure a sulphonamido (SONH2-) or sulphonimido (SO2NH-) grouping. Compounds specified are sulphamide, sulphimide, ammonium sulphamate, sodium or potassium sulphamate, ammonium imidodisulphonate. Products other than guanidine salts which may be obtained by altered conditions are biguanide, melamine, melam, melem, melon, ammeline, ammelide, thioammeline and thioammelide. The reaction product contains elemental sulphur, and may be used directly as a fertilizer, or worked up for the guanidine salt by leaching with water and treatment with alkali earth oxides or hydroxides. Examples describe (1) the reaction of ammonium sulphamate with ammonium thiocyanate or with thiourea and the reaction of ammonium thiocyanate with (2) sodium sulphamate, (3) ammonium imidodisulphonate and sulphamide.
GB33555/45A 1944-08-08 1945-12-11 Preparation of guanidine Expired GB611417A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US611417XA 1944-08-08 1944-08-08

Publications (1)

Publication Number Publication Date
GB611417A true GB611417A (en) 1948-10-29

Family

ID=22033878

Family Applications (1)

Application Number Title Priority Date Filing Date
GB33555/45A Expired GB611417A (en) 1944-08-08 1945-12-11 Preparation of guanidine

Country Status (1)

Country Link
GB (1) GB611417A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2567677A (en) * 1949-11-12 1951-09-11 American Cyanamid Co Preparation of guanidine sulfate
US2567676A (en) * 1949-03-15 1951-09-11 American Cyanamid Co Production of guanidine sulfate

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2567676A (en) * 1949-03-15 1951-09-11 American Cyanamid Co Production of guanidine sulfate
US2567677A (en) * 1949-11-12 1951-09-11 American Cyanamid Co Preparation of guanidine sulfate

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