GB485549A - Improved process of distillation of natural glycerides and preparation of vitamin compositions - Google Patents

Improved process of distillation of natural glycerides and preparation of vitamin compositions

Info

Publication number
GB485549A
GB485549A GB22675/36A GB2267536A GB485549A GB 485549 A GB485549 A GB 485549A GB 22675/36 A GB22675/36 A GB 22675/36A GB 2267536 A GB2267536 A GB 2267536A GB 485549 A GB485549 A GB 485549A
Authority
GB
United Kingdom
Prior art keywords
oil
high vacuum
vacuum distillation
fraction
oils
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB22675/36A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eastman Kodak Co
Original Assignee
Eastman Kodak Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eastman Kodak Co filed Critical Eastman Kodak Co
Publication of GB485549A publication Critical patent/GB485549A/en
Expired legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/59Compounds containing 9, 10- seco- cyclopenta[a]hydrophenanthrene ring systems

Abstract

Animal or vegetable oils are subjected to high vacuum distillation to obtain a fraction free of proteins and rancid products, and having an iodine value greater than 100, the fraction then being blended with vitamin concentrates. Drying oils and semi-dryers such as perilla, linseed, n'gart, walnut, poppy seed, soya bean, sunflower, candle nut, corn, cottonseed and fish oils, rich in unsaturates, such as salmon, sardine, menhaden and cod liver are specified. Short path high vacuum distillation is preferred. Prior to distillation, hydrogen may be bubbled through the oil, which latter is then de-gassed in an apparatus heated to 100 DEG C. and evacuated to a pressure of 100 mm. of mercury. In an example linseed oil is subjected to short path high vacuum distillation. The fraction collected at 190 DEG C. and under a pressure of 5 x 10-2 millimetres of mercury comprises a mixture of free fatty acids and sterols. Fractions p collected between 225-250 DEG C. and at pressures between 0,5 to 3 x 10-2 millimetres of mercury comprise the desired fractions for blending with vitamin concentrates, and contain glycerides corresponding to over 88 per cent of unsaturated fatty acid. For medicinal uses, lecithin may be added to the mixture; the oil may be emulsified, or flavouring materials may be admixed. The vitamin concentrates may be obtained from the source of oil, such as fish oils. British Specification 485,614, and U.S.A. Specifications 1,925,559 and 1,942,858 are referred to.ALSO:In the short-path high vacuum distillation of crude linseed oil the first distillate taken off at a temperature of 190 DEG C. and pressure of 5 x 10-2 millimetres of mercury comprises a mixture of free fatty acids and sterols. British Specification 485,614, [Group III], and U.S.A. Specifications 1,925,559 and 1,942,858 are referred to.ALSO:In the preparation of a medicinal composition, animal or vegetable oils are subjected to high vacuum distillation to obtain a fraction free of proteins and rancid products and having an iodine value greater than 100, the fraction then being blended with vitamin concentrates. Drying oils and semi-dryers such as perilla, linseed, N'Gart, walnut, poppy seed, soya bean, sunflower, candle nut, corn, cottonseed and fish oils, rich in unsaturates, such as salmon, sardine, menhaden and cod liver are specified. Short path high vacuum distillation is preferred. Applied to linseed oil, fractions collected between 225-250 DEG C. and at pressures between 0,5 to 3 x 10-2 mms. of mercury comprise the desired fractions and contain glycerides corresponding to over 88 per cent of unsaturated fatty acid. Lecithin may be added to the mixture. The vitamin concentrates may be obtained from the source of oil, such as fish oils. British Specification 485,614. [Group III], and U.S.A. Specifications 1,925,559, and 1,942,858 are referred to.ALSO:In the preparation of a food fat, animal or vegetable oils are subjected to high vacuum distillation to obtain a fraction free of proteins and rancid products and having an iodine value greater than 100, the fraction then being blended with vitamin concentrates. Drying oils and semi-dryers such as perilla, linseed, N'Gart, walnut, poppy seed, soya bean, sunflower, candle nut, corn, cottonseed and fish oils, rich in unsaturates such as salmon, sardine, menhaden and cod liver are specified. Shortpath high vacuum distillation is preferred. Applied to linseed oil, fractions collected between 225-250 DEG C. and at pressures between 0,5 to 3 x 10-2 mms. of mercury comprise the desired fractions and contain glycerides corresponding to over 88 per cent of unsaturated fatty acid. The oil may be emulsified and flavouring materials may be admixed. The vitamin concentrates may be obtained from the source of oil, such as fish oils. British Specification 485,614, [Group III], and U.S.A. Specifications 1,925,559 and 1,942,858 are referred to.
GB22675/36A 1935-08-24 1936-08-18 Improved process of distillation of natural glycerides and preparation of vitamin compositions Expired GB485549A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US485549XA 1935-08-24 1935-08-24

Publications (1)

Publication Number Publication Date
GB485549A true GB485549A (en) 1938-05-18

Family

ID=21955215

Family Applications (1)

Application Number Title Priority Date Filing Date
GB22675/36A Expired GB485549A (en) 1935-08-24 1936-08-18 Improved process of distillation of natural glycerides and preparation of vitamin compositions

Country Status (2)

Country Link
DE (1) DE664745C (en)
GB (1) GB485549A (en)

Also Published As

Publication number Publication date
DE664745C (en) 1938-09-05

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