GB478386A - Improvements in or relating to the manufacture and use of catalysts for hydrogenation and like processes - Google Patents

Improvements in or relating to the manufacture and use of catalysts for hydrogenation and like processes

Info

Publication number
GB478386A
GB478386A GB27366/36A GB2736636A GB478386A GB 478386 A GB478386 A GB 478386A GB 27366/36 A GB27366/36 A GB 27366/36A GB 2736636 A GB2736636 A GB 2736636A GB 478386 A GB478386 A GB 478386A
Authority
GB
United Kingdom
Prior art keywords
nickel
catalysts
reduction
precipitated
nickel compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB27366/36A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR822222D priority Critical patent/FR822222A/fr
Application filed by Individual filed Critical Individual
Priority to GB27366/36A priority patent/GB478386A/en
Priority to GB16933/37A priority patent/GB478487A/en
Publication of GB478386A publication Critical patent/GB478386A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/94—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the iron group metals or copper
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B31/00—Reduction in general
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C27/00—Processes involving the simultaneous production of more than one class of oxygen-containing compounds
    • C07C27/04—Processes involving the simultaneous production of more than one class of oxygen-containing compounds by reduction of oxygen-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • C07C29/175—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds with simultaneous reduction of an oxo group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

In the preparation of catalysts comprising finely divided metallic nickel suspended in an inert liquid such as mineral oil, a reducible nickel compound precipitated in an aqueous medium is ground in a colloid mill with an excess of precipitating agent. The mass is repeated filtered, diluted with water, and repassed through the colloid mill until free from all traces of water-soluble salt. The reduction to the metallic state is preferably effected after the precipitate has been dried and dispersed in the inert medium. The nickel is preferably precipitated from an aqueous solution of a soluble salt by means of alkaline carbonate. Additional substances may be mixed with the nickel compound, e.g. copper hydroxide or basic carbonate for facilitating the reduction of the nickel, or aluminium or magnesium hydroxide for retarding the growth of crystals of the precipitated nickel compound. After reduction, the product may be re-ground in a paint mill. The catalysts are particularly useful for the hydrogenation of crotonaldehyde to butyraldehyde and butyl alcohol.
GB27366/36A 1936-10-08 1936-10-08 Improvements in or relating to the manufacture and use of catalysts for hydrogenation and like processes Expired GB478386A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
FR822222D FR822222A (en) 1936-10-08
GB27366/36A GB478386A (en) 1936-10-08 1936-10-08 Improvements in or relating to the manufacture and use of catalysts for hydrogenation and like processes
GB16933/37A GB478487A (en) 1936-10-08 1936-10-08 Improvements in or relating to the reactivation of catalysts used in hydrogenation and like processes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB27366/36A GB478386A (en) 1936-10-08 1936-10-08 Improvements in or relating to the manufacture and use of catalysts for hydrogenation and like processes

Publications (1)

Publication Number Publication Date
GB478386A true GB478386A (en) 1938-01-18

Family

ID=10258435

Family Applications (2)

Application Number Title Priority Date Filing Date
GB27366/36A Expired GB478386A (en) 1936-10-08 1936-10-08 Improvements in or relating to the manufacture and use of catalysts for hydrogenation and like processes
GB16933/37A Expired GB478487A (en) 1936-10-08 1936-10-08 Improvements in or relating to the reactivation of catalysts used in hydrogenation and like processes

Family Applications After (1)

Application Number Title Priority Date Filing Date
GB16933/37A Expired GB478487A (en) 1936-10-08 1936-10-08 Improvements in or relating to the reactivation of catalysts used in hydrogenation and like processes

Country Status (2)

Country Link
FR (1) FR822222A (en)
GB (2) GB478386A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2971984A (en) * 1957-07-16 1961-02-14 Hoechst Ag Process for preparing butyraldehyde

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19933348B4 (en) * 1999-07-16 2005-11-17 Oxeno Olefinchemie Gmbh Process for reducing oxidic hydrogenation contacts

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2971984A (en) * 1957-07-16 1961-02-14 Hoechst Ag Process for preparing butyraldehyde

Also Published As

Publication number Publication date
FR822222A (en) 1937-12-23
GB478487A (en) 1938-01-19

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