GB472623A - Improvements in rendering micro-organisms innocuous - Google Patents

Improvements in rendering micro-organisms innocuous

Info

Publication number
GB472623A
GB472623A GB35759/35A GB3575935A GB472623A GB 472623 A GB472623 A GB 472623A GB 35759/35 A GB35759/35 A GB 35759/35A GB 3575935 A GB3575935 A GB 3575935A GB 472623 A GB472623 A GB 472623A
Authority
GB
United Kingdom
Prior art keywords
acid
oil
ether
disinfectants
hydroxy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB35759/35A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of GB472623A publication Critical patent/GB472623A/en
Expired legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions

Landscapes

  • Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Chlorinated thymotic or carracrotic acid is prepared by passing chlorine to saturation into an aqueous solution of the mono-potassium salt of the acid, dissolving the precipitate in caustic potash, filtering, acidifying the filtrate with hydrochloric acid, extracting the solution with ether, and evaporating off the ether.ALSO:Carboxyl groups are introduced into oil of thyme or other essential oil by heating with continuous passage of carbon dioxide and gradual introduction of metallic sodium. The product may be separated out by pouring the mixture into dilute hydrochloric acid, or the mixture may be poured into water saturated with carbon dioxide and extracted with ether to obtain a "soda-insoluble fraction" leaving an aqueous residue which is precipitated with strong hydrochloric acid to yield a "soda-soluble fraction." A CH2OH group may be added to oil of cloves or other essential oil by heating a caustic soda solution of the oil with formaldehyde, neutralizing the product with dilute acetic acid and filtering off the mass which separates. Fennel oil may be treated with potassium permanganate solution, acidified with sulphuric acid and extracted with ether. The various products are dispersed into the atmosphere to act as disinfectants. The disinfecting action of these and various other disinfectants, mainly consisting of essential oils or their constituents or of hydroxy carboxylic cyclic acids and their derivatives, is increased by treatment of the substances with ultra violet light, with or without the simultaneous supply of oxygen or ozone, or the air in which the disinfectants have been dispersed may be so treated.ALSO:Germs and other micro-organisms in the air are destroyed by finely dispersing in the air one or more of the following classes of substances of low vapour tension, viz. hydroxy carboxylic acids of iso- or heterocyclic, mono- or poly-cyclic character and with or without side chains on the nucleus; ethers and esters of such acids; substances obtained by chemical treatment of essential oils so as to add hydroxyl and/or carboxyl groups thereto; ethers and esters of such compounds; halogen derivatives of any of the foregoing substances; also terpinols, eugenol methyl ether, cinnamic aldehyde, cinnamic acid, geraniol, safrol, isosafrol, and citral. Active substances specified are salicylic, p-hydroxy benzoic, cresotic, hydroxydimethyl-benzene carboxylic, o- and p-thymotic, o- and p-carvacrotic, and hydroxyisoamyl-benzene carboxylic acids, chlorination products of these acids, methyl and propyl esters of p-hydroxy-benzene carboxylic acids, 8-hydroxy-quinoline-7-carboxylic acid and its methyl, propyl, isopropyl and isobutyl esters, b -naphthol-o-carboxylic acid, the methyl ester of hydroxy-naphthol-o-carboxylic acid, and chloro-hydroxy-methyl-isopropyl-benzene-carboxylic acid. The substances may be dispersed, in liquid or solid form or in solution, by spraying, volatilizing or smouldering. Solvents, when used, may be of high or low vapour tension and may be themselves disinfectants, the use of alcohol and acetone being referred to. The active substance may be dispersed in separate small portions, or a solvent may first be dispersed alone and then in admixture with the active disinfectant. The efficiency of the active disinfectants may be increased by treating them before or during dispersion with ultraviolet light, with or without the simultaneous supply of air, oxygen or ozone, or the air in which the disinfectants are dispersed may be so treated. The use, as disinfectants of substances of high vapour tension is also referred to, alcohol, n-propyl alcohol, benzene and ethyl acetate being specified. Chlorinated thymotic, or carvacrotic, acid is prepared by passing chlorine to saturation into an aqueous solution of the p mono-potassium salt of the non-chlorinated acid, dissolving the precipitate in caustic potash, filtering, acidifying the filtrate with hydrochloric acid, extracting the solution with ether and evaporating off the ether. Carboxyl groups are introduced into oil of thyme or other essential oil by heating with continuous passage of carbon dioxide and gradual introduction of metallic sodium. The product may be separated out by pouring the mixture into dilute hydrochloric acid, or the mixture may be poured into water saturated with carbon dioxide and extracted with ether to obtain a " soda insoluble fraction " leaving an aqueous residue which is precipitated with strong hydrochloric acid to yield a " soda-soluble fraction. " A CH2OH group may be added to oil of cloves or other essential oil by heating a caustic soda solution of the oil with formaldehyde, pouring the product into dilute acetic acid to neutralize it, and filtering off the mass which separates. Fennel oil may also be treated with potassium permanganate solution, acidified with sulphuric acid and extracted with ether.
GB35759/35A 1934-12-28 1935-12-24 Improvements in rendering micro-organisms innocuous Expired GB472623A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE472623X 1934-12-28

Publications (1)

Publication Number Publication Date
GB472623A true GB472623A (en) 1937-09-27

Family

ID=6541456

Family Applications (1)

Application Number Title Priority Date Filing Date
GB35759/35A Expired GB472623A (en) 1934-12-28 1935-12-24 Improvements in rendering micro-organisms innocuous

Country Status (1)

Country Link
GB (1) GB472623A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996039826A1 (en) * 1995-06-07 1996-12-19 Proguard, Inc. Disinfection of a contaminated environment

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996039826A1 (en) * 1995-06-07 1996-12-19 Proguard, Inc. Disinfection of a contaminated environment
US5738861A (en) * 1995-06-07 1998-04-14 Proguard, Inc. Method and composition for disinfection of a contaminated environment

Similar Documents

Publication Publication Date Title
CN105797189B (en) Plant extraction liquid air purifying preparation preparation method
CN104434669A (en) Traditional Chinese medicine disinfectant and preparation method thereof
GB472623A (en) Improvements in rendering micro-organisms innocuous
Harada Olive oil ozonide and its fungicidal quality
US2079772A (en) Aqueous germicidal composition containing alkyl phenols
Nelson The flavor of maple sirup
Wheeler et al. PARA-CYMENE STUDIES. XI. PARA-CYMYL-2-CARBITHIOIC ACID
Clark Deguelin. IV. The Structure of Deguelin and Tephrosin
DE504646C (en) Process for the preparation of anthraquinone and its offshoots
Brunnstrom The Alkaline Oxidation of 2-Naphthol
US1854764A (en) Bleaching methods and agent
JPS6152184B2 (en)
Krauss et al. DICHLOROAMINE T. AND CHLORINATED EUCALYPTOL 1.2.
DE2722346A1 (en) WATER-SOLUBLE HALOGEN COMPLEXES, PROCESS FOR THEIR PRODUCTION AND THEIR USE IN HYGIENE AND DERMATOLOGY AND FOR MAKING FLUIDS ASEPTIC
CN104490650A (en) Disinfectant and preparation method thereof
DE509379C (en) Seed dressing
DE517539C (en) Process for the preparation of aromatic oxyaldehydes
US1858551A (en) Manufacture of glycidic acids
DE866486C (en) Process for the production of organic sulfur compounds
US717016A (en) Organic peroxid.
US1947315A (en) Separation of vitamins from saponifiable oils
AT146915B (en) Process for the preparation of durable solutions of dioxydiaminoarsenobenzene and its derivatives.
DE331887C (en) Process for the production of soluble, discolored, odorless and tasteless proteins from blood
DE565900C (en) Process for separating antirachitic highly effective radiation products from the antirachitic ineffective radiation products of ergosterol
DE327050C (en) Process for the production of sulfur preparations of the thiophene series