GB468627A - Manufacture of vat-dyestuffs - Google Patents

Manufacture of vat-dyestuffs

Info

Publication number
GB468627A
GB468627A GB290/36A GB29036A GB468627A GB 468627 A GB468627 A GB 468627A GB 290/36 A GB290/36 A GB 290/36A GB 29036 A GB29036 A GB 29036A GB 468627 A GB468627 A GB 468627A
Authority
GB
United Kingdom
Prior art keywords
dyestuff
decacyclene
chlorsulphonic acid
sodium sulphide
treated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB290/36A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IG Farbenindustrie AG
Original Assignee
IG Farbenindustrie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IG Farbenindustrie AG filed Critical IG Farbenindustrie AG
Publication of GB468627A publication Critical patent/GB468627A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B57/00Other synthetic dyes of known constitution
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B49/00Sulfur dyes
    • C09B49/12Sulfur dyes from other compounds, e.g. other heterocyclic compounds
    • C09B49/124Sulfur dyes from other compounds, e.g. other heterocyclic compounds from polycarbocyclic compounds

Abstract

Vat dyestuffs are prepared by subjecting decacyclene, in the presence of chlorsulphonic acid to sulphurization and halogenation, either simultaneously or successively. In examples: (1) decacyclene is treated in chlorsulphonic acid with sulphur chloride which effects both sulphurization and chlorination; the product is refluxed with sodium sulphide to obtain a dyestuff soluble in sodium sulphide which dyes cotton copper brown tints, and a dyestuff insoluble in sodium sulphide which dyes cotton orange tints from a hydrosulphite vat; (2) the crude dyestuff of example 1 of Specification 468,416 is treated with chlorine in chlorsulphonic acid to give a dyestuff insoluble in sodium sulphide; (3) decacyclene is treated in chlorsulphonic acid with sulphur and then with chlorine. Samples have been furnished under Sect. 2 (5) of the products of the examples and also of a product obtained by brominating the crude dyestuff prepared by treating decacyclene in chlorsulphonic acid with sulphur.
GB290/36A 1935-01-12 1936-01-03 Manufacture of vat-dyestuffs Expired GB468627A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE468627X 1935-01-12

Publications (1)

Publication Number Publication Date
GB468627A true GB468627A (en) 1937-07-05

Family

ID=6540883

Family Applications (1)

Application Number Title Priority Date Filing Date
GB290/36A Expired GB468627A (en) 1935-01-12 1936-01-03 Manufacture of vat-dyestuffs

Country Status (1)

Country Link
GB (1) GB468627A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2539188A (en) * 1948-05-25 1951-01-23 Great Lakes Carbon Corp Sulfochlorohydrocarbons and method for making them
US2560462A (en) * 1946-06-12 1951-07-10 Francolor Sa Water-soluble tetracene dyestuffs and method of dyeing employing them

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2560462A (en) * 1946-06-12 1951-07-10 Francolor Sa Water-soluble tetracene dyestuffs and method of dyeing employing them
US2539188A (en) * 1948-05-25 1951-01-23 Great Lakes Carbon Corp Sulfochlorohydrocarbons and method for making them

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