GB350735A - Improvements in or relating to the manufacture of compounds of manganese and rosin - Google Patents
Improvements in or relating to the manufacture of compounds of manganese and rosinInfo
- Publication number
- GB350735A GB350735A GB18885/30A GB1888530A GB350735A GB 350735 A GB350735 A GB 350735A GB 18885/30 A GB18885/30 A GB 18885/30A GB 1888530 A GB1888530 A GB 1888530A GB 350735 A GB350735 A GB 350735A
- Authority
- GB
- United Kingdom
- Prior art keywords
- manganese
- rosin
- mineral oil
- per cent
- fused
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 title abstract 4
- 229910052748 manganese Inorganic materials 0.000 title abstract 4
- 239000011572 manganese Substances 0.000 title abstract 4
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 title abstract 3
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 title abstract 3
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 title abstract 3
- 150000001875 compounds Chemical class 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 abstract 4
- 239000002480 mineral oil Substances 0.000 abstract 3
- 235000010446 mineral oil Nutrition 0.000 abstract 3
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 abstract 2
- 235000021314 Palmitic acid Nutrition 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 abstract 1
- 239000000155 melt Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 abstract 1
- 239000003921 oil Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 239000002966 varnish Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
- C09F9/00—Compounds to be used as driers, i.e. siccatives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
A manganese resinate containing at least 4,5 per cent manganese is obtained by heating rosin with the requisite quantity of manganese dioxide at 300-315 DEG C. until reaction is complete, and then rapidly cooling. In operation the rosin is fused and raised to 250 DEG C., and the manganese dioxide slowly sifted in without stirring. The temperature is then raised slowly to 300 DEG C., the melt stirred, and the reaction completed at 310-315 DEG C. The product is soluble in mineral oil and may be used as a drier for varnish compositions, or be added to mineral oil together with palmitic acid an be used in the purification of used mineral oil, for instance by the process described in Specification 242,272 [Class 91, Oils &c.]. A statement of the art refers to a "fused" resinate containing up to 3\ba1/2\be per cent of manganese, and a "precipitated" resinate containing up to 7\ba1/2\be-8 per cent of manganese.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US350735XA | 1929-06-20 | 1929-06-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB350735A true GB350735A (en) | 1931-06-18 |
Family
ID=21880465
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB18885/30A Expired GB350735A (en) | 1929-06-20 | 1930-06-20 | Improvements in or relating to the manufacture of compounds of manganese and rosin |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB350735A (en) |
-
1930
- 1930-06-20 GB GB18885/30A patent/GB350735A/en not_active Expired
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