GB326865A - Process for the manufacture of mixed ethers of carbohydrates - Google Patents
Process for the manufacture of mixed ethers of carbohydratesInfo
- Publication number
- GB326865A GB326865A GB3751228A GB3751228A GB326865A GB 326865 A GB326865 A GB 326865A GB 3751228 A GB3751228 A GB 3751228A GB 3751228 A GB3751228 A GB 3751228A GB 326865 A GB326865 A GB 326865A
- Authority
- GB
- United Kingdom
- Prior art keywords
- per cent
- propyl
- content
- cellulose
- chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/193—Mixed ethers, i.e. ethers with two or more different etherifying groups
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
326,865. Carpmael, A., (I. G. Farbenindustrie Akt.-Ges.). Dec. 19, 1928. Right to Patent relinquished. Carbohydrate ethers are obtained by the action of a mixture of alkylating agents, comprising a methyl or ethyl compound and an alkyl compound of which the alkyl group contains three or more carbon atoms, upon a cellulose, starch or other colloidal carbohydrate in the presence of caustic alkali. The mixed ethers have a marked strength and insensitivity to water and are suitable for making artificial silk, films, and plastic masses. In examples, cotton linters or purified pine wood cellulose are mixed with excess of 50 per cent caustic soda solution and heated with a mixture of ethyl chloride and propyl or butyl chloride at about 120‹ C. When the reaction is complete the excess of alkyl chlorides is distilled off and the crude product is washed with water. The mixed ethers are soluble in alcohol-benzene mixtures, and possess high tearing strength and low water expansion. The proportions of ethyl chloride and propyl or butyl chloride may be varied and products having ethoxy content of 33 per cent, propyl-oxy content 12 per cent, or ethoxy content 32 per cent, butyl-oxy content 14 per cent may be obtained. Specifications 6035/13, 164,374, [both in Class 2 (ii), Cellulose &c.], and 184,825 are referred to.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB3751228A GB326865A (en) | 1928-12-19 | 1928-12-19 | Process for the manufacture of mixed ethers of carbohydrates |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB3751228A GB326865A (en) | 1928-12-19 | 1928-12-19 | Process for the manufacture of mixed ethers of carbohydrates |
Publications (1)
Publication Number | Publication Date |
---|---|
GB326865A true GB326865A (en) | 1930-03-19 |
Family
ID=10397015
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3751228A Expired GB326865A (en) | 1928-12-19 | 1928-12-19 | Process for the manufacture of mixed ethers of carbohydrates |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB326865A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106939052A (en) * | 2017-03-24 | 2017-07-11 | 山东滕新材料股份有限公司 | A kind of preparation method of cellulose ether |
-
1928
- 1928-12-19 GB GB3751228A patent/GB326865A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106939052A (en) * | 2017-03-24 | 2017-07-11 | 山东滕新材料股份有限公司 | A kind of preparation method of cellulose ether |
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