GB2490393A - Monitoring microstructure of a metal target - Google Patents

Monitoring microstructure of a metal target Download PDF

Info

Publication number
GB2490393A
GB2490393A GB1205896.2A GB201205896A GB2490393A GB 2490393 A GB2490393 A GB 2490393A GB 201205896 A GB201205896 A GB 201205896A GB 2490393 A GB2490393 A GB 2490393A
Authority
GB
United Kingdom
Prior art keywords
metal target
magnetic field
electromagnetic sensors
microstructure
response
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB1205896.2A
Other versions
GB2490393B (en
GB201205896D0 (en
Inventor
Anthony Peyton
Wuliang Yin
Stephen John Dickinson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
University of Manchester
Original Assignee
University of Manchester
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by University of Manchester filed Critical University of Manchester
Priority to GB1205896.2A priority Critical patent/GB2490393B/en
Publication of GB201205896D0 publication Critical patent/GB201205896D0/en
Publication of GB2490393A publication Critical patent/GB2490393A/en
Application granted granted Critical
Publication of GB2490393B publication Critical patent/GB2490393B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/12Measuring magnetic properties of articles or specimens of solids or fluids
    • G01R33/1223Measuring permeability, i.e. permeameters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B38/00Methods or devices for measuring, detecting or monitoring specially adapted for metal-rolling mills, e.g. position detection, inspection of the product
    • B21B38/04Methods or devices for measuring, detecting or monitoring specially adapted for metal-rolling mills, e.g. position detection, inspection of the product for measuring thickness, width, diameter or other transverse dimensions of the product
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/72Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/0023Electronic aspects, e.g. circuits for stimulation, evaluation, control; Treating the measured signals; calibration
    • G01R33/0035Calibration of single magnetic sensors, e.g. integrated calibration
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/12Measuring magnetic properties of articles or specimens of solids or fluids
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R35/00Testing or calibrating of apparatus covered by the other groups of this subclass
    • G01R35/005Calibrating; Standards or reference devices, e.g. voltage or resistance standards, "golden" references
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/72Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
    • G01N27/80Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables for investigating mechanical hardness, e.g. by investigating saturation or remanence of ferromagnetic material
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/72Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
    • G01N27/82Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables for investigating the presence of flaws

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Analytical Chemistry (AREA)
  • Electrochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Investigating Or Analyzing Materials By The Use Of Magnetic Means (AREA)

Abstract

A system for monitoring a microstructure of a metal target comprises a plurality of electromagnetic sensors 911-91n for outputting a magnetic field, wherein an excitation signal output by each of the electromagnetic sensors is a multi-frequency waveform, detecting a resultant magnetic field and outputting a detection signal in response thereto, and a control unit 920 arranged to receive the detection signals from the plurality of sensors, to determine a phase change between the output magnetic field and the resultant magnetic field at each of a plurality of frequencies forming the multi-frequency waveform for each of the sensors, and to determine a microstructure of a metal target at the plurality of electromagnetic sensors based on the phase changes. The system can be used on a hot steel production line.

Description

Improvements in Sensors Embodiments of the present invention relate to apparatus and methods for monitoring the microstructure of a metal target. In particular, although not exclusively, some embodiments of the present invention relate to apparatus and methods for calibrating electromagnetic sensors. In particular, although not exclusively, some embodiments of the invention relate to monitoring the microstructural formation of a metal target.
Background
During production processing of metals, such as steel, rolling of the metal is followed by controlled cooling. During the production processing, particularly the cooling process, a microstructure of the metal evolves and results in a final microstrueture of the processed metal. The microstrueture of the processed metal has an impact on many aspects of the metal's character, such as tensile strength.
Conventional microstructural analysis techniques are destructive and involve removing samples for analysis from, for example, the end of a coil of the processed material. This is time-consuming, costly, does not allow continuous monitoring, and assesses only a small fraction of the material processed.
When the processed material is steel, it is known that electromagnetic techniques can monitor steel phase transformations by detecting the ferromagnetic phase change due to the changes in electrical conductivity and magnetic permeability within the steel. Furthermore, if a coil is placed in the vicinity of the steel being processed, this results in a change in impedance measurements for the coil because conductivity and permeability are influenced by the steel's mierostructure. For example austenite, the stable phase of iron at elevated temperatures, is paramagnetie whereas the stable low temperature phases ferrite, pearlite, bainite and martensite are ferromagnetic below the Curie temperature of about 760°C. Steel properties vary strongly with the volume fractions of these phases, which are controlled largely by the cooling rate and alloy content of the steel.
I
However, problems exist in monitoring in real-time the electromagnetic properties of metals during processing. Many problems result from the environmental conditions associated with metal processing, such as heat, moisture, humidity, etc. It is an object of embodiments of the invention to at least mitigate one or more of the
problems of the prior art.
Brief Description of the Drawings
Embodiments of the invention will now be described by way of example only, with reference to the accompanying figures, in which: Figure 1 is a schematic of a metal production process or "hot mill"; Figure 2 is an illustration of a prior art electromagnetic sensor; Figure 3 is an example graph of normalised sensor output against ferrite fraction; Figure 4 is an illustration of an example electromagnetic sensor; Figure 5 is an illustration of an example electromagnetic sensor according; Figure 6 is a schematic of an example system; Figure 7 is an illustration of phasors determined at a plurality of signal frequencies; Figure 8 is an example of a sensor output; Figure 9 is an apparatus according to an embodiment of the invention; and Figure 10 is an illustration of phasors determined from a plurality of sensors according to embodiments of the invention.
Detailed Description of Embodiments of the Invention Embodiments of the present invention are intended to reduce problems associated with the monitoring of an evolution of a microstructure of a metal target during production processing of the metal target. An example of such processing may be in the case of steel production where hot rolling of the steel is followed by controlled cooling. However, it will be realised that embodiments of the present invention are not limited to use with steel targets and may be utilised with a range of metals, including ferrous and non-ferrous metal targets. Changes to the microstrueture of the steel during the controlled cooling may be deduced by measurements of the accompanying electromagnetic properties of the material.
Embodiments of the invention will be described with reference to the processing of steel.
However, it is realised that embodiments of the invention may also be useful in monitoring other metals, particularly ferrous metals.
An overview of a metal processing stage, sometimes known as a "hot mill" is shown in Figure. 1.
Steel 10! being processed is rolled to a required shape and initial size with one or more successive passes through one or more rolling stands 110. The production process is typically instrumented with one or more sensors 120 to measure thickness, width, shape etc and temperature of the steel. When the steel product leaves the last rolling stand 110, the structure of the steel is usually a high-temperature face-centred cubic austenite phase.
As the steel cools, often in an accelerated cooling process with air, water or oil coolants which may be applied to the steel via one or a plurality of outlets 125 located in a controlled cooling zone, the steel transforms to a structure consisting of the body centred cubic ferrite phase and carbide, usually eementite (Fe3C), the morphology of the latter depending on cooling rate and composition. Increasing the cooling rate or alloy content causes transformation to occur at lower temperatures, giving a finer carbide dispersion and, hence, a stronger product. By altering the final mierostruetures, a wide range of strengths can be produced in the metal product from very low carbon, essentially, ferritic structures with tensile strengths of about 200 N/mm2 to high strength steels with tensile strengths in excess of 1000 N/mm2. These have higher carbon contents with microstructures consisting of mixtures of ferrite, pearlite, bainite, martensite and, in some cases, known as TRIP steels, austenite which by suitable alloying has been stabilized at temperatures down to ambient. The cooling process is often monitored and controlled by one or more temperature sensors 140, such as optical pyrometers, which may be positioned before and/or after and occasionally in special zones in the middle of the outlets 125.
It would be useftil to monitor the structure of the steel during the cooling process, such as by sensors within the controlled cooling zone.
A number of techniques have been proposed for monitoring the steel microstructure on-line i.e. in real time, each with their limitations. Optical temperature sensors are used to implement feedback control of cooling but are adversely affected by water spray variations and surface emissivity irregularities. In addition, temperature is only an assumed indicator of mierostructure and only the surface of the steel is measured. Other possible approaches such as X-ray diffraction and laser ultrasound have been demonstrated in the laboratory, but cannot easily be deployed in the water cooling zone due to the effects of water spray and mist.
Past attempts to use electromagnetic sensors to monitor microstructure have been limited by: 1) interference from other process parameters, such as the effects of nearby steelwork and variations in lift-off (i.e. the distance between the sensor head and the material) 2) a limited detection range, with the sensor response levelling off for ferritie phase fractions above typically 30% ferrite content. This is a serious limitation as the industry is interested in controlling transformation at much higher fractions 3) the difficulty of getting a sensor to work long-term in the hostile conditions encountered in a steel hot rolling mill especially with the effects of thermal drift because of the elevated temperatures that such sensors would have to endure.
Fig. 2 shows a prior art sensor unit, denoted generally with reference numeral 200, for detecting electromagnetic properties of a metal target 260.
Typically the metal target 260 may be moving quickly over a series of rollers and therefore close access to the metal target is restricted to one side only, with for instance a sensor unit positioned between a pair of rollers.
The scnsor unit 200 may contain a magnetic core 210, a magnetic excitation source 220 and one or more magnetic detectors 230, 240. The magnetic core 210 is configured to apply as much of an interrogating magnetic field 250 to the metal target 260 as possible and consequently designs based on U-shaped cores 210 are preferred. The excitation source 220 may be a permanent magnet or an electromagnet. The detection components 230, 240 are magnetometers and both induction detector coils and Hall probe sensor have been reported. The magnetic detectors 230, 240 are fitted to the poles of the magnetic core 210.
Also shown in Fig. 2 are two variations on the basic U-core design of sensor 200. The first variation shows an extra pole 270 and magnetometer, which may be added to provide an extra measurement of the magnetic field 250. The measurements provided by the extra magnetic detector 270 may be used to cancel potential sources of error, such as changes caused by the variation in the distance between the sensor unit 200 and the metal target 260.
This distance is often referred to as lift-off. The second variation is the combination of two extra poles 280, 290 in a back-to-back configuration to realise an H-shaped sensor.
EN 77626A entitled "System for Online-Detecting Transformation value and/or Flatness of Steel or Magnetic Material" discloses a system for detecting the transformation and/or a flatness of a steel or a magnetic material on-line. The system consists of an exciting coil on one side of the plate shaped metal target with an excitation coil generating an alternating magnetic field. Two or more detection coils are arranged at positions different in distance from the exciting coil but mutually induced with the exciting coil in an arrangement similar to that shown in Fig. 2. The magnetic measurements from the detection coils are fed to an arithmetic unit for obtaining the transformation value and the flatness of the metal target.
JP03262957A entitled "Transformation Ratio Measuring Instrument for Steel Material" discloses a system using separate magnetic cores of different sizes.
EPOI 308721 entitled "Device and Method for Detecting Magnetic Properties of a Metal Object" discloses a similar system to EP1 77626A, but in this ease a device is disclosed for detecting the magnetic properties of a metal target object. The system comprises a means of generating a magnetic field and a detecting means for measuring the effect on a portion of the magnetic field produced by the metal target. In this case however, EP01308721 discloses that the generated magnetic field is a continuous DC magnetic field and the detecting means are means suitable for detecting at least a continuous component of the magnetic field. The detecting means may be positioned on the poles of the sensor unit as shown in Fig. 2. In addition the reported system has a non-magnetic metallic shield located between the generating and detection means and the metal target. The non-magnetic metallic shield does not affect the DC magnetic field, which is a key feature of using continuous DC rather than alternating AC magnetic fields.
To overcome problems associated with interference from the magnetisation of the rollers carrying the metal target when the metal target is in the form of a plate or strip, JP07325067A entitled "Transformation Factor Measuring Device" discloses a transformation factor measuring device in which the excitation source is provided in one side of a metal target plate and the detection components are provided in the other side of the metal target plate. This approach helps to reduce the effects of the magnetisation of the roller carrying the metal target plate, but has the disadvantages that different parts of the system are located in different positions making the system more difficult to deploy and making the system components more difficult to protect from the fast moving metal target plate.
A disadvantage of using a sensor unit which employs only a continuous DC excitation or a single frequency excitation is that the measurement system is sensitive a limited detection range of the transformed fraction of a steel target, with the sensor unit response levelling off for ferritic phase fractions above typically 30% ferrite content, as reported in (Yin et al, Journal of Material Science (2007), Vol. 42, pp. 6854-6861, "Exploring the relationship between ferrite fraction and morphology and the electromagnetic properties of steel") and as shown in Fig. 3. This is a serious limitation as the steel industry is interested in controlling transformation at much higher fractions. The paper by Yin et a! discusses that a sensor unit can be used to identify the transformed fraction in steel targets across the ftll range (0-100%) of ferrite transformed fraction using multiple frequency measurements.
JP60017350A discloses a system to quantitatively measure the transformation rate of a steel target using an exciting coil and a detecting coil at the same side of the steel target to be measured, passing a current of variable frequency to the exciting coil, and obtaining a magnetic permeability of the measuring material for the thickness direction from both coils in each frequency.
The use of different frequencies has also been reported by (Dickinson et al, IEEE Transactions on Instrumentation and Measurement (2007), Vol. 5 6(3), pp. 879-886, "The development of a multi-frequency electromagnetic instrument for monitoring the phase transformation of hot strip steel"). This paper describes an instrument arranged to analyze the phase transformations of hot strip steel using an electromagnetic sensor. The sensor exploits variations in the electrical conductivity and magnetic permeability of the steel to monitor microstructure evolution during processing. The sensor is an inductive device based on an H-shaped ferrite core, which is interrogated with a multi-frequency impedance analyzer containing a digital signal processor. Online fast Fourier transform was performed to abstract the multi-frequency inductance changes due to the microstructural evolution of the sample. An overview of the instrument and measurements from a range of carbon steel samples are presented. The results verify the ability of the instrument both to monitor the mierostructural changes and to reject variations in lift-off distance between the sensor and the hot strip.
JP 2000-3 04725 entitled "Method for Measuring Thickness of Transformation Layer of Steel Material" also discloses a multi-frequency method for monitoring the progress of transformation through a metal target. In this case the metal target is thick and the system measures the thickness of the outer transformed layer by analysing the spectra measured by the sensor unit.
However, significant problems exist with using such electromagnetic sensors in a metal processing environment. Some embodiments of the invention aim to reduce one or more of such problems so that electromagnetic sensors may be more reliably and accurately used in such environments. There are challenges for the design of an electromagnetic sensor unit.
An ideal sensor unit should be able to (i) reject or reduce interference from other process parameters, such as the effects of nearby steelwork and variations in lift-off, (ii) measure a wide range of transformed fractions, such as a full range 0 to 100% of transformed fractions, and (iii) to have a low sensitivity to variations caused by the high temperature environment with hot metal at temperatures of 1000 °C only a short distance, such as a few cm from the active side of the sensor unit. Some embodiments of the invention may aim to address or reduce some of these problems.
Some embodiments of the invention relate to an apparatus and method for calibrating an electromagnetic sensor unit. In particular, some embodiments relate to an apparatus and method for achieving regular calibration during operation of the sensor unit. Frequent calibration of the sensor unit is desirable because of the very high temperature environment encountered in operation with very high radiant heat loads, typically exerted at least in part from the metal target undergoing measurement.
These embodiments of the invention provide an electronic means of applying one or more reference calibration levels to an electromagnetic sensor unit.
Figure 4 illustrates an apparatus 400 according to a first embodiment of the invention. The apparatus is an electromagnetic sensor unit 400 for sensing a microstructure of a metal target.
The sensor unit 400 comprises a magnetic core 410, one or more a magnetic excitation sources 420 and one or more magnetic detectors 430. The magnetic core 410 is configured to apply an interrogating magnetic field 440 generated by the excitation source(s) 420 to a metal target (not shown). The metal core 410 may be U-shaped, as shown in Figure 4, or may be configured as a different shape, such as H-shaped. The excitation source 420 may be a permanent magnet, an electromagnet or a combination thereof The magnetic detector 430 is arranged for detecting a magnetic field 440 and may include one or more induction detector coils and/or Hall probe sensors. Other magnetometers are also envisaged. In some embodiments, the sensor unit 400 comprises two magnetic detectors 430, each fitted to a corresponding pole of the magnetic core 410. The core 410 may be U-shaped or H-shaped (H-shaped includes two U-shaped cores arranged back-to-back). In some embodiments, the core may be H-shaped and comprises one or more background detector coils 445. The sensor unit 400 further comprises a calibration unit 450 for calibrating the sensor unit 400.
S
The calibration unit 450 comprises one or more calibration circuits for generating a calibration magnetic field which interacts with the magnetic field 440 generated by the one or more excitation sources 420 to simulate the effect of a metal target being present proximal to the sensor 400. In some embodiments of the invention, the calibration magnetic field is generated by currents induced in the calibration circuit by the interrogating magnetic field 440. The calibration circuit may comprise a calibration coil 451 for increasing the sensitivity of the calibration circuit to the magnetic field 440. Whilst one calibration coil 451 is shown in Figure 4, it will be realised that the calibration unit 450 may comprise a plurality of calibration coils 451.
The calibration unit 450 may further comprise a control or switching means 452 for controlling an operation of the calibration coil 451. The control means 452 is shown in Figure 4 as a switch for selectively activating the calibration coil 451 by selectively applying the induced electrical eddy current to the calibration coil 451. The control means may be operated responsive to a received calibration control signal, as will be discussed. in other embodiments, the control means 452 may be implemented in other ways, such as by a controllable power source or signal generator for selectively generating and applying a voltage or signal to the calibration coil 451. A reference impedance 453 or resistance may be provided in circuit with the calibration coil 451 for limiting a current flow through the calibration coil 451. Alternatively, a current limited output from a power supply or signal generator may be used. Although not shown in Figure 4, a power source may be included in the calibration unit 450 for providing an electrical current or signal for the calibration coil 451, which is selectively applied via the switch 452.
Each calibration coil 451 may be positioned around a pole of the magnetic core 410 50 as to interact with a portion of the magnetic flux 440 generated by the excitation source 420 which would be applied to the metal target.
When the switch 452 is closed, an electrical current is able to flow around the calibration circuit containing the calibration coil 451 and reference impedance 453. The calibration unit 450 has an effect on the magnetic sensor similar to that of the flow of the eddy currents that would be induced in the metal target by the excitation source 420. Consequently the calibration unit 450 can provide a known input to the sensor unit 400 which may be used to calibrate the sensor unit 400. The calibration unit 450 may be activated manually, such as by user activation of the switch 452, or automatically i.e. by the switch 452, power source or signal generator being activated by a control unit, such as a microprocessor or the like.
Figure 5 illustrates an apparatus 500 according to a further embodiment of the invention.
The apparatus 500 comprises an electromagnetic sensor 410, 420, 430, 440, 445 as previously described with reference to Figure 4 and a repeated discussion of like numbered parts will be omitted for clarity. The apparatus 500 further includes a calibration unit 550 having a plurality of calibration circuits 551, 552, 553, 554. Each calibration circuit 551, 552, 553, 554 may each be considered to be a calibration unit 450 as previously described with reference to Figure 4, and repeat discussion will again be omitted for clarity. As discussed previously, each calibration circuit 551, 552, 553, 554 may include one or more calibration coils.
Each of the calibration circuits 551, 552, 553, 554 may be individually controlled to generate a corresponding magnetic field. Each calibration coil may be configured to operate within a different respective calibration frequency range to calibrate the response of the sensor unit 500 at each frequency range. A first calibration coil 551 may be configured to operate within a first calibration frequency range, which is a relatively low frequency range. The configuration may include providing the first calibration coil 551 with one or relatively few turns. Similarly, the reference impedance associated with the first calibration coil 551 may be relatively low. A fourth calibration coil 554 may be configured to operate within a fourth frequency range, which is a relatively high calibration frequency range. The configuration may include providing the fourth calibration coil 554 with a relatively large number of' turns. Second and third calibration coils 552, 553 may be configured to operate within second and third respective calibration frequency ranges, which may be equally or unequally spaced between the first and fourth calibration frequency ranges. Whilst the second embodiment is shown having four calibration circuits 551, 552, 553, 554, it will be realised that more or less calibration circuits may be provided.
Figure 6 illustrates a system 600 according to some embodiments of the invention. The system 600 is arranged for sensing the microstructurc of a metal target, such as steel being formed in a production process, such as a hot mill.
The system 600 comprises an electromagnetic sensor unit 400 as shown in Figure 4 and a control unit 600. Embodiments of the system 600 may also be envisaged which include the sensor unit 500 of Figure 5. In which case, the control unit 600 may have a plurality, such as four, calibration control signals of different frequency provided to the four calibration coils.
The control unit 600 comprises a signal unit 610 for generating excitation and control signals and receiving detection signals for/from the sensor unit 400, respectively. In particular, the signal unit 610 may output one or more excitation signals to the excitation coil 420 of the sensor unit 400, and may receive detection signals from one or more detection coils 430 of the sensor unit 400 (the embodiment shown in Figure 6 comprises an excitation signal provided to an excitation coil 420 and two detection coils 430, although other numbers of excitation coils and detection coils may be envisaged). The signal unit 610 is further arranged to output a calibration control signal to the calibration unit 450 to be received by the control means 452 for controlling the operation of the calibration circuit.
The control unit 600 may further comprise a signal processing unit 620 for processing detection signals received from the sensor unit 400, as will be explained.
In order to calibrate the sensor unit 400, the control unit 600 generates an excitation signal for the excitation coil 420 of the sensor unit 400. The excitation signal may be a time-variant waveform, such as a sine or cosine waveform. The excitation signal may comprise waveforms summed together to form a multi-frequency waveform. Such waveforms are described in Dickinson et a!, IEEE Transactions on Instrumentation and Measurement (2007), Vol. 56(3), pp. 879-886, which is herein incoiporated by reference, although other waveforms may be used. A driver circuit, although not shown in Figure 6, may be arranged between the output of the signal unit 610 and the one or more excitation coils 420. The control unit 600 also generates a calibration control signal for the calibration unit 450. The calibration control signal may control the switch 452, such that a circuit is selectively formed which includes the calibration coil 451, or may directly generate a calibration signal applied to the calibration coil, such as a signal having a frequency f As a result, a calibration magnetic field is generated. The calibration field effectively modifies the magnetic flux generated by the excitation coil 420 to produce a known effect on the sensor 400, which is similar to that of' the metal target. The calibration field imitates a flow of eddy currents that would be induced in the metal target by the excitation signal. The control unit 600 is further arranged to receive one or more detector signals from the detection coils 430. The signal unit 610 may digitise each of the received signals and communicate information indicative of the received signals and of the generated excitation signal to the signal processing unit 620.
Based on the information received from the signal unit 610, the signal processing unit 620 converts the digitised signals into phasor equivalents using down conversion techniques as will be appreciated, such as from the cited references. The signal processing unit 620 is arranged to determine impedance change in the electromagnetic sensor 500 resulting from the metal target or the calibration field, as will be appreciated by those skilled in the art.
The impedance change is determined having real and imaginary components i.e. as quadrate and in-phase components, as shown in Figure 7. These may be determined by the signal processing unit 620 comparing the excitation coil 420 current and detection coil 430 output voltage waveforms. This may be performed at each of a plurality of frequencies of interest, particularly to obtain a depth-dependent profile since higher frequency signals penetrate more deeply into the metal target. The complex impedance at each frequency may be calculated by the signal processing unit applying Fast Fourier Transforms (FFTs) to the voltage and current waveforms to obtain the phase and magnitude of the respective signals at each separate frequency. An example of multi-frequency measurements is shown in Figure 7 for a non-magnetic metal target and similar multi-frequency measurements may be obtained with the application of the calibration coil arrangement 450, shown in Figure 4.
To calibrate the electromagnetic sensor 400, the signal processing unit 620 is arranged to determine a gradient or sensitivity of the electromagnetic sensor 620 to the output of the calibration unit 450, 550 at one or more frequencies of interest by subtracting a response of the one or more detector coils 430 in the absence of a metal target or output of the calibration unit 450 (a background level) from a response of the detector coils 430 in the absence of a metal target but with the calibration unit 450, 550 generating a known calibration signal.
The operation of the calibration unit may be described as follows. Here complex phasor notation is used to describe the response the sensor. Let, ZQf be the complex impedance output of the sensor when no metal target is present and the calibration circuit is not activated at frequency f, and ZcM be the complex impedance output of the sensor when no metal target is present and the calibration coil is activated, at frequency f, and Z111 be the complex impedance output of the sensor when the metal target is present and the calibration coil is not activated, at frequency f11. The normalised and calibrated sensor output, NNIu can be calculated as follows:
N -______
671i -Oft Finally, the calibrated sensor output ZMn at frequency f11 can further be calculated as ZM=k.NNf where k is a complex scaling factor relating the response of the calibration circuit at frequency f to the ideal response at this frequency.
Some embodiments of the invention exploit a time interval between metal targets i.e. when no metal target is proximal to the electromagnetic sensor, to calibrate the electromagnetic sensor. The time interval, typically a few seconds or more, that occurs on metal production processes, such as hot mills, between rolling operations on each metal slab, bloom or billet to the final product such as strip, plate, medium sections, rail, rod etc, as shown in Fig. 8.
Figure 8 illustrates an example output from an electromagnetic sensor 400, 500 arranged to monitor metal targets produced from a hot mill. Reference numeral 810 denotes an output level when a metal target is present proximal to the sensor 400, 500, whereas 820 denotes an output level when a metal target is not proximal to the sensor i.e. the sensor unit is located between successive metal targets and its output is relatively low. It has been realised that a time interval 820 between metal targets may, in some embodiments, present an opportunity to apply one or more known input conditions to a sensor unit to calibrate that sensor unit. A predetermined threshold level 830 may be utilised to by the control unit 600 to determine when the metal target is not proximal to the sensor.
In order to calibrate the sensor 400, 500 both zero (background) and a predetermined reference level may be applied to the sensor unit 400, 500. The zero reference level may be obtained directly during the time interval between rolling operations when no material is present i.e. with no output from the calibration coil. The predetermined reference level corresponds to an output from the one or more calibration coils. In the prior art, this has been achieved by positioning a reference sample of material with known electromagnetic properties proximal to the sensor unit. However, this is difficult or inconvenient to achieve in a short period of time and/or on a regular basis, such as between metal targets being produced by a hot mill.
Figure 9 illustrates an apparatus 900 according to an embodiment of the invention. The apparatus 900 is arranged to determine a time-dependent profile of the electromagnetic properties of a metal target 950. In particular, the apparatus 900 may be utilised to determine or to monitor the evolution of the electromagnetic properties of the metal target 950 as it cools following a hot production process, such as hot rolling.
The apparatus 900 includes a plurality of electromagnetic sensors 911, 912, 913.. . 91n.
Each electromagnetic sensor 911, 912, 913.. .91n may be as described previously with reference to Figure 4 or 5. However, it will be appreciated that each electromagnetic sensor 911, 912, 913...91n may not comprise a calibration unit 450, 550. That is, some embodiments of the invention include electromagnetic sensors which do not comprise a calibration unit or circuit, although it will be realised that embodiments may be envisaged which do.
The system 900 further comprises a plurality of control units 921, 922, 923, 92n, each associated with a respective electromagnetic sensor 911, 912, 913.. . 91n for determining a phase response of the respective electromagnetic sensor 913.. .9 in to the metal target. The control units may be individually formed i.e. separately arranged to each provide an output to a monitoring system, or may be arranged as shown in Figure 9 where each control unit is a component part of a control system 920. When combinedly formed, as shown in Figure 9, it may be possible to reduce an overall number of components via re-use of some sub-systems. The control units 921, 922, 923, 92n may be as shown in and described with reference to Figure 6. However, each control units 921, 922, 923, 92n may not comprise an output for controlling a calibration unit 450, 550. Each control unit 921, 922, 923, 92n may comprise one or more excitation signal outputs and one or more detector signal inputs for determining the phase response of the electromagnetic sensor when proximal to the metal target. Each control unit 921, 922, 923, 92n is arranged to determine a change in structure of the metal target utilising the respective electromagnetic sensor 911, 912, 913.. .91 n.
The electromagnetic sensors 911, 912, 913.. .91n may be arranged proximal to a path of the metal target through one or more cooling zones, as explained above. The cooling zones may include means for controllably cooling the metal target. The means for controllably cooling the metal target may include one or more means for applying a fluid to the metal target, such as air or other gasses or liquids, such as water or oil. As the metal target is moved in a rolling direction (shown in Figure 10) it moved past a first electromagnetic sensor 911. Responsive to an excitation signal generated by the respective control unit 921, one or more detection signals are received. The excitation signal includes a plurality of frequency components, as indicated in Figure 10, although the number of these multi-frequency components is not limiting. The first control unit 921 is arranged to determine a phase response of the electromagnetic sensor at each frequency of the excitation signal.
Similarly, as the metal target progresses past each of the second, third and fourth electromagnetic sensors 912, 913, 914, the respective control unit is arranged to determine the sensor response at each frequency of excitation signal and the associated phase response, as shown in Figure 10.
it can be observed in Figure 10, although the phase diagrams for each sensor are merely for illustration and are not to scale, that the four illustrated phasors are gradually rotated clockwise indicating the development or evolution of the structure of the metal target as it cools. The control system 920 may therefore determine the structural development of the metal target in real time. Based on the determined developmental rate, the control system 920 may be arranged to output a signal 930 indicative of the structural development to a processor controller 940 arranged to control the metal production process. The signal may indicate a deviation of the structural development of the metal target from a predetermined structural development rate, such that the process controller 940 may vary one or more parameters of the production process to optimise the structural development of the metal target. For example, if the signal 930 indicates that the structure of the metal target is forming as a result of cooling more quickly than desired, the process controller may reduce a rate of fluid flow toward the metal target, such as by reducing a water flow rate from outlets 125 described above. In this way, the cooling of the metal target may be slowed to a desired rate. in this way, the resulting qualities of the metal target may be controlled by real time monitoring of the structural changes of the metal target.
It will be appreciated from the discussion above that some embodiments of the invention allow convenient calibration of electromagnetic sensors. In particular, in some embodiments, the calibration may be performed in an automatically determined period between metal targets. In some embodiments, an array of electromagnetic sensors is utilised to determine an evolution of a microstructure of a metal target. By such monitoring, properties of the metal target may be controlled.
It will be appreciated that embodiments of the present invention can be realised in the form of hardware, software or a combination of hardware and software. Any such software may be stored in the form of volatile or non-volatile storage such as, for example, a storage device like a ROM, whether erasable or rewritable or not, or in the form of memory such as, for example, RAM, memory chips, device or integrated circuits or on an optically or magnetically readable medium such as, for example, a CD, DVD, magnetic disk or magnetic tape. It will be appreciated that the storage devices and storage media are embodiments of machine-readable storage that arc suitable for storing a program or programs that, when executed, implement embodiments of the present invention.
Accordingly, embodiments provide a program comprising code for implementing a system or method as claimed in any preceding claim and a machine readable storage storing such a program. Still further, embodiments of the present invention may be conveyed electronically via any medium such as a communication signal carried over a wired or wireless connection and embodiments suitably encompass the same.
All of the features disclosed in this specification (including any accompanying claims, abstract and drawings), and/or all of the steps of any method or process so disclosed, may be combined in any combination, except combinations where at least some of such features and/or steps are mutually exclusive.
Each feature disclosed in this specification (including any accompanying claims, abstract and drawings), may be replaced by alternative features serving the same, equivalent or similar purpose, unless expressly stated otherwise. Thus, unless expressly stated otherwise, each feature disclosed is one example only of a generic series of equivalent or similar features.
The invention is not restricted to the details of any foregoing embodiments. The claims should not be construed to cover merely the foregoing embodiments, but also any embodiments which fall within the scope of the claims.

Claims (13)

  1. CLAiMS 1. A system for monitoring a microstructure of a metal target, comprising: a plurality of electromagnetic sensors for outputting a magnetic field, wherein an excitation signal output by each of the electromagnetic sensors is a multi-frequency waveform, detecting a resultant magnetic field and outputting a detection signal in response thereto; and a control unit arranged to receive the detection signals from the plurality of electromagnetic sensors, to determine a phase change between the output magnetic field and the resultant magnetic field at each of a plurality of frequencies forming the multi-frequency waveform for each of the plurality of electromagnetic sensors, and to determine a microstructure of a metal target at the plurality of electromagnetic sensors based on the phase changes.
  2. 2. The system of claim 1, wherein the plurality of electromagnetic sensors are arranged in a movement direction of the metal target.
  3. 3. The system of claim 1 or 2, wherein the plurality of electromagnetic sensors are spaced apart in a cooling area of a production process of the metal target.
  4. 4. The system of any of claims I to 3, wherein the control unit is arranged to determine a microstructure evolution of the metal target.
  5. 5. A production process comprising the system of any of claims I to 4, wherein the control unit is arranged to output a signal indicative of the phase transformation of the metal target and one or more parameters of the production process are controlled in response thereto.
  6. 6. The production process of claim 5, wherein the one or more parameters are parameters of a process for cooling the metal target.
  7. 7. A method of monitoring a microstructure of a metal target, comprising: outputting a magnetic field generated in response to a multi-frequency waveform at a plurality of electromagnetic sensors; detecting a resultant magnetic field at the plurality of electromagnetic sensors; determining a phase response of the resultant magnetic field with respect to the output magnetic field at each of a plurality of frequencies forming the multi-frequency waveform; and determining a microstructure of a metal target at each of the plurality of electromagnetic sensors based upon the phase response.
  8. 8. The method of claim 7, wherein the microstructure is determined based further upon a magnitude of the resultant magnetic field with respect to the output magnetic field.
  9. 9. The method of claims 7 or 8, comprising determining a microstructural rate of change of the metal target.
  10. 10. The method of any of claims 7 to 9, comprising varying one or more parameters of a production process in response to the determined microstructure.
  11. 11. The method of claim 10, wherein the one or more parameters comprise cooling parameters of the metal target.
  12. 12. An apparatus substantially as described hereinbefore with reference to Figures 3-10.
  13. 13. A method substantially as described hereinbefore with reference to Figures 3-10.Amendments to the claims have been filed as follows:CLAIMS1. A system for monitoring a microstrueture of a metal target, comprising: a plurality of electromagnetic sensors for outputting a magnetic field, wherein an excitation signal output by each of the electromagnetic sensors is a multi-frequency waveform, detecting a resultant magnetic field and outputting a detection signal in response thereto; and a control system arranged to receive the detection signals from the plurality of electromagnetic sensors, to determine a phase change between the output magnetic field and the resultant magnetic field at each of a plurality of frequencies forming the multi-frequency waveform for each of the plurality of electromagnetic sensors, to determine a microstructure of a metal target at the plurality of electromagnetic sensors based on the (\J 15 phase changes, to determine a microstructural development rate of the metal target and to output a signal indicative of a deviation of the microstructural development rate from a predetermined microstructural development rate; 1 a process controller arranged to receive the signal output from the control system and to control one or more parameters of a production process of the metal target in response thereto.2. The system of claim 1, wherein the plurality of electromagnetic sensors are arranged in a movement direction of the metal target.3. The system of claim 1 or 2, wherein the plurality of electromagnetic sensors are spaced apart in a cooling area of a production process of the metal target.4. The system of any of claims 1 to 3, wherein the control system is arranged to determine a microstructure evolution of the metal target.5. A production process comprising the system of any of claims 1 to 4, the one or more parameters of the production process are controlled in response the signal output by the control system.6. The production process of claim 5, wherein the one or more parameters are parameters of a process for cooling the metal target.7. A method of monitoring a microstructure of a metal target, comprising: outputting a magnetic field generated in response to a multi-frequency waveform at a plurality of electromagnetic sensors; detecting a resultant magnetic field at the plurality of electromagnetic sensors; determining a phase response of the resultant magnetic field with respect to the output magnetic field at each of a plurality of frequencies forming the multi-frequency waveform; and determining a microstructure of a metal target at each of the plurality of electromagnetic sensors based upon the phase response.determining a deviation of a microstructural development rate of the metal target from a predetermined microstructural development rate; controlling one or more parameters of a production process of the metal target in response to the deviation.8. The method of claim 7, wherein the microstructure is determined based further upon a magnitude of the resultant magnetic field with respect to the output magnetic field.9. The method of claim 7 or 8, wherein the one or more parameters comprise cooling parameters of the metal target.10. An apparatus substantially as described hereinbefore with reference to Figures 9-10.11. A method substantially as described hereinbefore with reference to Figures 9-10.
GB1205896.2A 2011-04-27 2011-04-27 Improvements in sensors Active GB2490393B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB1205896.2A GB2490393B (en) 2011-04-27 2011-04-27 Improvements in sensors

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1205896.2A GB2490393B (en) 2011-04-27 2011-04-27 Improvements in sensors

Publications (3)

Publication Number Publication Date
GB201205896D0 GB201205896D0 (en) 2012-05-16
GB2490393A true GB2490393A (en) 2012-10-31
GB2490393B GB2490393B (en) 2013-03-13

Family

ID=46160211

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1205896.2A Active GB2490393B (en) 2011-04-27 2011-04-27 Improvements in sensors

Country Status (1)

Country Link
GB (1) GB2490393B (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2629920C1 (en) * 2016-05-12 2017-09-04 Федеральное государственное унитарное предприятие "Всероссийский научно-исследовательский институт авиационных материалов" (ФГУП "ВИАМ") Steel phase composition control member
WO2019245603A1 (en) * 2018-06-21 2019-12-26 Primetals Technologies USA LLC Method and system for control of steel strip microstructure in thermal processing equipment using electro magnetic sensors
DE102021205429A1 (en) 2021-05-28 2022-12-01 Sms Group Gmbh Plant and process for the production of wire and/or bar-shaped steels
EP4109087A1 (en) 2021-06-21 2022-12-28 NV Bekaert SA Device for in-line monitoring the room temperature microstructure variations
EP4160200A4 (en) * 2020-07-03 2023-12-06 JFE Steel Corporation Sensitivity calibration method, inspection device, and magnetic sensor group

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3433154B1 (en) 2016-03-21 2020-06-17 Railpod Inc. Combined passive and active method and systems to detect and measure internal flaws within metal rails

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1501751A (en) * 1974-01-25 1978-02-22 Siderurgie Fse Inst Rech Controlled cooling of hot-rolling mill products
FR2417102A1 (en) * 1978-02-14 1979-09-07 Siderurgie Fse Inst Rech Sensor for magnetic state of cooling metallic prod. - subjects sample to continuous magnetic field, measures flux variations along length and forms applied signal
EP0178378A2 (en) * 1984-10-19 1986-04-23 Kawasaki Steel Corporation Method of controlling cooling of hot-rolled steel sheet and system therefor
JPS63253253A (en) * 1987-04-10 1988-10-20 Kawasaki Steel Corp Method for measuring transformation rate of hot rolled steel plate
EP1308721A1 (en) * 2001-11-02 2003-05-07 Corus Technology BV Device and method for detecting magnetic properties of a metal object

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1501751A (en) * 1974-01-25 1978-02-22 Siderurgie Fse Inst Rech Controlled cooling of hot-rolling mill products
FR2417102A1 (en) * 1978-02-14 1979-09-07 Siderurgie Fse Inst Rech Sensor for magnetic state of cooling metallic prod. - subjects sample to continuous magnetic field, measures flux variations along length and forms applied signal
EP0178378A2 (en) * 1984-10-19 1986-04-23 Kawasaki Steel Corporation Method of controlling cooling of hot-rolled steel sheet and system therefor
JPS63253253A (en) * 1987-04-10 1988-10-20 Kawasaki Steel Corp Method for measuring transformation rate of hot rolled steel plate
EP1308721A1 (en) * 2001-11-02 2003-05-07 Corus Technology BV Device and method for detecting magnetic properties of a metal object

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Dickinson et al; IEEE Transactions on Instrumentation and Measurement, (2007), Vol 56(3), pp879-886, "The development of a multifrequency electromagnetic instrument for monitoring the phase transformation of hot strip steel". *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2629920C1 (en) * 2016-05-12 2017-09-04 Федеральное государственное унитарное предприятие "Всероссийский научно-исследовательский институт авиационных материалов" (ФГУП "ВИАМ") Steel phase composition control member
WO2019245603A1 (en) * 2018-06-21 2019-12-26 Primetals Technologies USA LLC Method and system for control of steel strip microstructure in thermal processing equipment using electro magnetic sensors
EP4160200A4 (en) * 2020-07-03 2023-12-06 JFE Steel Corporation Sensitivity calibration method, inspection device, and magnetic sensor group
DE102021205429A1 (en) 2021-05-28 2022-12-01 Sms Group Gmbh Plant and process for the production of wire and/or bar-shaped steels
EP4109087A1 (en) 2021-06-21 2022-12-28 NV Bekaert SA Device for in-line monitoring the room temperature microstructure variations
WO2022268507A1 (en) 2021-06-21 2022-12-29 Nv Bekaert Sa Device for in-line monitoring the room temperature microstructure variations

Also Published As

Publication number Publication date
GB2490393B (en) 2013-03-13
GB201205896D0 (en) 2012-05-16

Similar Documents

Publication Publication Date Title
US10144987B2 (en) Sensors
Lu et al. Conductivity Lift-off Invariance and measurement of permeability for ferrite metallic plates
GB2490393A (en) Monitoring microstructure of a metal target
Hao et al. Off-line measurement of decarburization of steels using a multifrequency electromagnetic sensor
Dickinson et al. The development of a multifrequency electromagnetic instrument for monitoring the phase transformation of hot strip steel
Shen et al. Real-time in-line steel microstructure control through magnetic properties using an EM sensor
Hao et al. Modelling the electromagnetic response of two-phase steel microstructures
Zhu et al. Modeling and experimental study of a multi-frequency electromagnetic sensor system for rail decarburisation measurement
JP7343575B2 (en) Device for in-line measurement of the proportion of austenite in steel
KR100711471B1 (en) On-line transformation ratio determination device of hot rolled steel sheet
Zhu et al. Evaluation of rail decarburisation depth using a H-shaped electromagnetic sensor
Yang et al. In-line quantitative measurement of transformed phase fraction by EM sensors during controlled cooling on the run-out table of a hot strip mill
Johnstone et al. Using electromagnetic methods to monitor the transformation of steel samples
DE50013642D1 (en) METHOD AND DEVICE FOR INITIATING DETERMINATION OF THE CONVERSION RATE OF A NONMAGNETIC PHASE TO A FERROMAGNETIC PHASE OF A METALLIC WORKPIECE
Shu et al. The effect of stress and incentive magnetic field on the average volume of magnetic Barkhausen jump in iron
Davis et al. Impedance spectroscopy for remote analysis of steel microstructures
JP2011252787A (en) Hardening quality inspection device
Hao et al. Monitoring of Steel Microstructures using Electromagnetic Sensors
Pal’a et al. Optimisation of amplitude distribution of magnetic Barkhausen noise
Papaelias et al. Measurement of the Ferrite-Austenite Phase Balance during Transformation in steel using Electromagnetic Sensors

Legal Events

Date Code Title Description
732E Amendments to the register in respect of changes of name or changes affecting rights (sect. 32/1977)

Free format text: REGISTERED BETWEEN 20150625 AND 20150701