GB2109265B - Reaction column and use thereof - Google Patents

Reaction column and use thereof

Info

Publication number
GB2109265B
GB2109265B GB08233066A GB8233066A GB2109265B GB 2109265 B GB2109265 B GB 2109265B GB 08233066 A GB08233066 A GB 08233066A GB 8233066 A GB8233066 A GB 8233066A GB 2109265 B GB2109265 B GB 2109265B
Authority
GB
United Kingdom
Prior art keywords
column
pressure
openings
liquid column
bubble
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB08233066A
Other versions
GB2109265A (en
Inventor
Norbert Bremus
Lutz Jeromin
Eberhard Peukert
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Publication of GB2109265A publication Critical patent/GB2109265A/en
Application granted granted Critical
Publication of GB2109265B publication Critical patent/GB2109265B/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/16—Fractionating columns in which vapour bubbles through liquid
    • B01D3/18—Fractionating columns in which vapour bubbles through liquid with horizontal bubble plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor

Abstract

A low vapour load reaction column comprises one or more bubble plates 1 with immersion caps 2 of which the side edges comprise openings or perforations 3 for the passage of the gas phase, one or more immersed inlets 5, one or more outlets 7 and, optionally, inflow and outflow weirs 6, 8, characterised in that it has an internal diameter of from 500 to 3000 mm and one or more orifices (4) below each bubble cap (2) of which the openings in the plate (1) are designed in such away that the dry pressure loss occurring under the particular conditions under which the column is operated are 15 times to 60 times greater than the pressure difference between the pressure of the liquid column at the outlet and the pressure of the liquid column at the inlet. This column is particularly suitable for the continuous catalytic esterification of aliphatic carboxylic acids of 2 to 24 carbon atoms with alcohols in countercurrent, and for transesterifications. <IMAGE>
GB08233066A 1981-11-21 1982-11-19 Reaction column and use thereof Expired GB2109265B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19813146142 DE3146142A1 (en) 1981-11-21 1981-11-21 REACTION COLUMN AND ITS USE

Publications (2)

Publication Number Publication Date
GB2109265A GB2109265A (en) 1983-06-02
GB2109265B true GB2109265B (en) 1985-09-04

Family

ID=6146862

Family Applications (1)

Application Number Title Priority Date Filing Date
GB08233066A Expired GB2109265B (en) 1981-11-21 1982-11-19 Reaction column and use thereof

Country Status (7)

Country Link
EP (1) EP0082301B1 (en)
JP (1) JPS5895549A (en)
AT (1) ATE14678T1 (en)
DE (2) DE3146142A1 (en)
GB (1) GB2109265B (en)
MY (1) MY8600317A (en)
PH (1) PH18812A (en)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3809417A1 (en) * 1988-03-21 1989-10-12 Henkel Kgaa METHOD FOR CONTINUOUSLY Esterifying Fatty Acids
WO1990008127A1 (en) * 1989-01-17 1990-07-26 Davy Mckee (London) Limited Process and apparatus
GB2299521B (en) * 1995-03-02 1998-09-09 Norton Chem Process Prod High capacity trays
US5844111A (en) * 1995-06-07 1998-12-01 The Procter & Gamble Company Method for purifying an inert gas while preparing lower alkyl esters
US5648483A (en) * 1995-06-07 1997-07-15 The Procter & Gamble Company Continuous transesterification method for preparing polyol polyesters
DE19623508C2 (en) * 1996-06-13 1998-08-20 Henkel Kgaa Process for the preparation of dialkyl carbonates
US5945529A (en) * 1996-07-19 1999-08-31 The Procter & Gamble Company Synthesis of polyol fatty acid polyesters using column with inert gas stripping
DE10257525A1 (en) 2002-12-10 2004-07-01 Cognis Deutschland Gmbh & Co. Kg Process for the production of linear or branched fatty acid esters by heterogeneously catalyzed reactive rectification with a pre-reactor
BRPI0618334B1 (en) * 2005-11-25 2016-01-05 Asahi Kasei Chemicals Corp process for the industrial production of a dialkyl carbonate and a diol, and a multi-stage continuous distillation column
CN101321805B (en) * 2005-11-30 2012-03-28 旭化成化学株式会社 Industrial production process for high-quality aromatic polycarbonate
KR20080067380A (en) * 2005-12-12 2008-07-18 아사히 가세이 케미칼즈 가부시키가이샤 Process for industrially producing high quality aromatic polycarbonate
TWI314549B (en) 2005-12-26 2009-09-11 Asahi Kasei Chemicals Corp Industrial process for separating out dialkyl carbonate
TW200738601A (en) * 2005-12-27 2007-10-16 Asahi Kasei Chemicals Corp Industrial process for production of dialkyl carbonate and diol
KR101554607B1 (en) * 2008-11-07 2015-09-22 에스케이케미칼주식회사 Method and apparatus for preparing fatty acid alkyl ester using fatty acid

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2778621A (en) * 1953-12-08 1957-01-22 Standard Oil Co Entrainment-obviating bubble cap
FR1327227A (en) * 1962-04-05 1963-05-17 Air Liquide Tray guarded for contacting liquids and gases
JPS4631321B1 (en) * 1968-10-08 1971-09-11
US3712595A (en) * 1971-07-12 1973-01-23 A Hirsch Upflow distributive trays for fractionating columns and absorption towers
CA1063777A (en) * 1974-04-24 1979-10-09 Allen W. Hancock (Ii) Distillation column reactor and process
DE2503195C3 (en) * 1975-01-27 1984-10-18 Henkel KGaA, 4000 Düsseldorf Process and device for the continuous catalytic esterification of fatty acids with alcohols

Also Published As

Publication number Publication date
GB2109265A (en) 1983-06-02
DE3146142A1 (en) 1983-06-01
ATE14678T1 (en) 1985-08-15
EP0082301A1 (en) 1983-06-29
DE3265279D1 (en) 1985-09-12
JPS5895549A (en) 1983-06-07
PH18812A (en) 1985-09-27
MY8600317A (en) 1986-12-31
EP0082301B1 (en) 1985-08-07

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Legal Events

Date Code Title Description
PE20 Patent expired after termination of 20 years

Effective date: 20021118