GB1590154A - Process for preparing low dusting granulated dyestuffs - Google Patents
Process for preparing low dusting granulated dyestuffs Download PDFInfo
- Publication number
- GB1590154A GB1590154A GB16166/77A GB1616677A GB1590154A GB 1590154 A GB1590154 A GB 1590154A GB 16166/77 A GB16166/77 A GB 16166/77A GB 1616677 A GB1616677 A GB 1616677A GB 1590154 A GB1590154 A GB 1590154A
- Authority
- GB
- United Kingdom
- Prior art keywords
- water
- granules
- soluble
- weight
- dyestuff
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 11
- 238000010410 dusting Methods 0.000 title description 4
- 239000000975 dye Substances 0.000 claims abstract description 29
- 239000008187 granular material Substances 0.000 claims abstract description 17
- 229920003169 water-soluble polymer Polymers 0.000 claims abstract description 17
- 125000000129 anionic group Chemical group 0.000 claims abstract description 15
- 239000004094 surface-active agent Substances 0.000 claims abstract description 15
- 239000000428 dust Substances 0.000 claims abstract description 14
- 238000001694 spray drying Methods 0.000 claims abstract description 5
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 60
- 238000000034 method Methods 0.000 claims description 38
- -1 alkali-metal salt Chemical class 0.000 claims description 15
- 229910052783 alkali metal Inorganic materials 0.000 claims description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 159000000000 sodium salts Chemical class 0.000 claims description 9
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 8
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical group OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 7
- KVBGVZZKJNLNJU-UHFFFAOYSA-N naphthalene-2-sulfonic acid Chemical compound C1=CC=CC2=CC(S(=O)(=O)O)=CC=C21 KVBGVZZKJNLNJU-UHFFFAOYSA-N 0.000 claims description 7
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 6
- 150000001340 alkali metals Chemical class 0.000 claims description 5
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- IMROMDMJAWUWLK-UHFFFAOYSA-N Ethenol Chemical compound OC=C IMROMDMJAWUWLK-UHFFFAOYSA-N 0.000 claims description 4
- 238000000889 atomisation Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 229920002845 Poly(methacrylic acid) Polymers 0.000 claims description 3
- 229920002125 Sokalan® Polymers 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 3
- 235000010265 sodium sulphite Nutrition 0.000 claims description 3
- 229920001732 Lignosulfonate Polymers 0.000 claims description 2
- 239000004117 Lignosulphonate Substances 0.000 claims description 2
- 235000019357 lignosulphonate Nutrition 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 239000000985 reactive dye Substances 0.000 abstract 1
- 235000019256 formaldehyde Nutrition 0.000 description 14
- 229960004279 formaldehyde Drugs 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 229910052700 potassium Inorganic materials 0.000 description 4
- 239000011591 potassium Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Inorganic materials [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 3
- IHRFTCGTRALYFG-UHFFFAOYSA-N 4-[[4-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]-2-sulfophenyl]diazenyl]-5-oxo-1-(4-sulfophenyl)-4h-pyrazole-3-carboxylic acid Chemical compound OC(=O)C1=NN(C=2C=CC(=CC=2)S(O)(=O)=O)C(=O)C1N=NC(C(=C1)S(O)(=O)=O)=CC=C1NC1=NC(Cl)=NC(Cl)=N1 IHRFTCGTRALYFG-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 2
- 229910052939 potassium sulfate Inorganic materials 0.000 description 2
- 239000001120 potassium sulphate Substances 0.000 description 2
- 235000011151 potassium sulphates Nutrition 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 229920005552 sodium lignosulfonate Polymers 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 229920001448 anionic polyelectrolyte Polymers 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- KWKXNDCHNDYVRT-UHFFFAOYSA-N dodecylbenzene Chemical compound CCCCCCCCCCCCC1=CC=CC=C1 KWKXNDCHNDYVRT-UHFFFAOYSA-N 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 229920000193 polymethacrylate Polymers 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000015424 sodium Nutrition 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L sodium sulphate Substances [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- ARXWHYHTMGGNST-UHFFFAOYSA-K trisodium 2-[[6-[(4,6-dichloro-1,3,5-triazin-2-yl)-methylamino]-1-hydroxy-3-sulfonatonaphthalen-2-yl]diazenyl]naphthalene-1,5-disulfonate Chemical compound [Na+].[Na+].[Na+].CN(c1ccc2c(O)c(N=Nc3ccc4c(cccc4c3S([O-])(=O)=O)S([O-])(=O)=O)c(cc2c1)S([O-])(=O)=O)c1nc(Cl)nc(Cl)n1 ARXWHYHTMGGNST-UHFFFAOYSA-K 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0003—Drying, e.g. sprax drying; Sublimation of the solvent
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0092—Dyes in solid form
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
- Detergent Compositions (AREA)
- Optical Filters (AREA)
- Glanulating (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB16166/77A GB1590154A (en) | 1977-04-19 | 1977-04-19 | Process for preparing low dusting granulated dyestuffs |
| DE19782813982 DE2813982A1 (de) | 1977-04-19 | 1978-03-31 | Verfahren zur herstellung von wasserloeslichen farbstoffen in form von granalien mit einem niedrigen staubgehalt |
| IT22228/78A IT1095557B (it) | 1977-04-19 | 1978-04-12 | Processo di granulazione |
| FR7811327A FR2388028A1 (fr) | 1977-04-19 | 1978-04-18 | Procede de production de colorants hydrosolubles sous une forme granulaire |
| JP4582178A JPS53132031A (en) | 1977-04-19 | 1978-04-18 | Method of making granular waterrsoluble dyestuff with low dust content |
| CH421978A CH632293A5 (en) | 1977-04-19 | 1978-04-19 | Process for preparing water-soluble dyes in the form of granules having a low dust content and the water-soluble dyes prepared thereby |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB16166/77A GB1590154A (en) | 1977-04-19 | 1977-04-19 | Process for preparing low dusting granulated dyestuffs |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1590154A true GB1590154A (en) | 1981-05-28 |
Family
ID=10072360
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB16166/77A Expired GB1590154A (en) | 1977-04-19 | 1977-04-19 | Process for preparing low dusting granulated dyestuffs |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS53132031A (it) |
| CH (1) | CH632293A5 (it) |
| DE (1) | DE2813982A1 (it) |
| FR (1) | FR2388028A1 (it) |
| GB (1) | GB1590154A (it) |
| IT (1) | IT1095557B (it) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4425134A (en) | 1979-10-02 | 1984-01-10 | Ciba-Geigy Corporation | Process for producing agglomerates of water-soluble dyes |
| US4624678A (en) * | 1984-05-04 | 1986-11-25 | Ciba-Geigy Corporation | Process for the preparation of granular dye formulations |
| GB2175612A (en) * | 1985-05-17 | 1986-12-03 | Kao Corp | Dyeing assistant composition |
| US5030244A (en) * | 1988-06-08 | 1991-07-09 | Ciba-Geigy Corporation | Preparation of granules of dyes, optical whiteners or photoactivators from an aqueous suspension of naphthalene sulfonic acid-formaldehyde condensate dispersant |
| US5910623A (en) * | 1996-08-20 | 1999-06-08 | Basf Aktiengesellschaft | Mixtures of sulfo-containing 1:2 metal complexes with vinyl polymers |
| WO2002046313A2 (de) * | 2000-12-07 | 2002-06-13 | Goldschmidt Ag | Verfahren zur herstellung von staubfreien, rieselfähigen pigmentkonzentraten |
| WO2003035769A2 (en) * | 2001-10-24 | 2003-05-01 | Ciba Specialty Chemicals Holding Inc. | A method for producing a granular formulation of plastic-soluble colorants |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0024654A1 (de) * | 1979-08-22 | 1981-03-11 | Ciba-Geigy Ag | Granulate von faserreaktiven Farbstoffen und Verfahren zu ihrer Herstellung |
| US4560747A (en) * | 1979-10-30 | 1985-12-24 | Ciba Geigy Corporation | Process for producing granulates of water-soluble dyes by fluidized bed granulation |
| EP1816171B1 (en) * | 1997-09-08 | 2014-01-15 | Basf Se | Stir-in pigment compositions |
| DE102016009514A1 (de) * | 2016-08-04 | 2018-02-08 | Giesecke+Devrient Currency Technology Gmbh | Verfahren und Vorrichtung zum Erzeugen von Kompositpartikeln |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH500270A (de) * | 1966-06-17 | 1970-12-15 | Ciba Geigy Ag | Handelsfähiges Farbstoffpräparat |
| DE2127669A1 (de) * | 1970-06-04 | 1971-12-16 | Ciba-Geigy Ag, Basel (Schweiz) | Kaltwasserlösliche Farbstoffpräparate |
| DE2341292C3 (de) * | 1973-08-16 | 1978-08-24 | Bayer Ag, 5090 Leverkusen | Farbstoffpräparationen, konzentrierte Lösungen dieser Farbstoffpräparationen und deren Verwendung |
-
1977
- 1977-04-19 GB GB16166/77A patent/GB1590154A/en not_active Expired
-
1978
- 1978-03-31 DE DE19782813982 patent/DE2813982A1/de not_active Withdrawn
- 1978-04-12 IT IT22228/78A patent/IT1095557B/it active
- 1978-04-18 JP JP4582178A patent/JPS53132031A/ja active Pending
- 1978-04-18 FR FR7811327A patent/FR2388028A1/fr active Granted
- 1978-04-19 CH CH421978A patent/CH632293A5/de not_active IP Right Cessation
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4425134A (en) | 1979-10-02 | 1984-01-10 | Ciba-Geigy Corporation | Process for producing agglomerates of water-soluble dyes |
| US4624678A (en) * | 1984-05-04 | 1986-11-25 | Ciba-Geigy Corporation | Process for the preparation of granular dye formulations |
| GB2175612A (en) * | 1985-05-17 | 1986-12-03 | Kao Corp | Dyeing assistant composition |
| GB2175612B (en) * | 1985-05-17 | 1990-01-24 | Kao Corp | Method of dip-dyeing cellulosic fibres. |
| US5030244A (en) * | 1988-06-08 | 1991-07-09 | Ciba-Geigy Corporation | Preparation of granules of dyes, optical whiteners or photoactivators from an aqueous suspension of naphthalene sulfonic acid-formaldehyde condensate dispersant |
| US5910623A (en) * | 1996-08-20 | 1999-06-08 | Basf Aktiengesellschaft | Mixtures of sulfo-containing 1:2 metal complexes with vinyl polymers |
| WO2002046313A2 (de) * | 2000-12-07 | 2002-06-13 | Goldschmidt Ag | Verfahren zur herstellung von staubfreien, rieselfähigen pigmentkonzentraten |
| WO2002046313A3 (de) * | 2000-12-07 | 2002-09-26 | Goldschmidt Ag Th | Verfahren zur herstellung von staubfreien, rieselfähigen pigmentkonzentraten |
| WO2003035769A2 (en) * | 2001-10-24 | 2003-05-01 | Ciba Specialty Chemicals Holding Inc. | A method for producing a granular formulation of plastic-soluble colorants |
| WO2003035769A3 (en) * | 2001-10-24 | 2003-09-18 | Ciba Sc Holding Ag | A method for producing a granular formulation of plastic-soluble colorants |
| US7608117B2 (en) | 2001-10-24 | 2009-10-27 | Ciba Specialty Chemicals Corporation | Method for producing a granular formulation of plastic-soluble colorants |
Also Published As
| Publication number | Publication date |
|---|---|
| IT1095557B (it) | 1985-08-10 |
| IT7822228A0 (it) | 1978-04-12 |
| CH632293A5 (en) | 1982-09-30 |
| FR2388028A1 (fr) | 1978-11-17 |
| JPS53132031A (en) | 1978-11-17 |
| FR2388028B1 (it) | 1983-04-15 |
| DE2813982A1 (de) | 1978-10-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |