GB1456260A - Method for crystallization of fructose from water solution - Google Patents
Method for crystallization of fructose from water solutionInfo
- Publication number
- GB1456260A GB1456260A GB5305674A GB5305674A GB1456260A GB 1456260 A GB1456260 A GB 1456260A GB 5305674 A GB5305674 A GB 5305674A GB 5305674 A GB5305674 A GB 5305674A GB 1456260 A GB1456260 A GB 1456260A
- Authority
- GB
- United Kingdom
- Prior art keywords
- fructose
- solution
- crystals
- mass
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Saccharide Compounds (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
1456260 Crystallizing fructose SUOMEN SOKERI OSAKEYHTIO 9 Dec 1974 [28 Jan 1974] 53056/74 Heading B1G [Also in Division C2] Fructose crystals having a crystal size of 200 to 600 Ám are obtained by crystallizing fructose from an aqueous solution thereof, containing at least 90% by weight of dry substance of which dry substance at least 90 percent by weight is fructose, in a process which comprises (a) providing such a fructose solution (b) adjusting the pH of said solution to 4.0-6.0, preferably 4.5-5.5, (c) bringing the aqueous fructose solution to a temperature at which it is saturated with respect to fructose, (a) adding fructose seed crystals to the solution, (e) lowering the temperature of the resulting mass at a controlled rate to cause the mass to be supersaturated with respect to fructose and to bring about an increase in the crystal size of the seed crystals without substantial formation of new fructose crystals and (f) separating the fructose crystals from the mass when the crystal size is 200-600 Ám. The process may be carried out continuously using as seed crystals, crystals taken from a previous crystallization and recrystallization may be accelerated by blowing warm dry air on to the surface of the mass to evaporate water therefrom during crystallisation. The rate of crystallisation of fructose may be increased by the addition to the solution of 2-4% by weight, based on the sugar solids, of methanol, ethanol, and/or isopropanol.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US437224A US3883365A (en) | 1972-01-04 | 1974-01-28 | PH adjustment in fructose crystallization for increased yield |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1456260A true GB1456260A (en) | 1976-11-24 |
Family
ID=23735578
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB5305674A Expired GB1456260A (en) | 1974-01-28 | 1974-12-09 | Method for crystallization of fructose from water solution |
Country Status (22)
| Country | Link |
|---|---|
| JP (1) | JPS5838160B2 (en) |
| AT (1) | AT346785B (en) |
| BE (1) | BE824362A (en) |
| BG (1) | BG24961A3 (en) |
| CA (1) | CA1030533A (en) |
| CH (1) | CH596318A5 (en) |
| CS (1) | CS207335B2 (en) |
| DE (1) | DE2502558C2 (en) |
| DK (1) | DK24875A (en) |
| ES (1) | ES433589A1 (en) |
| FI (1) | FI58654C (en) |
| FR (1) | FR2259151B1 (en) |
| GB (1) | GB1456260A (en) |
| HU (1) | HU174513B (en) |
| IE (1) | IE41769B1 (en) |
| IT (1) | IT1026412B (en) |
| NL (1) | NL186183C (en) |
| PL (1) | PL102673B1 (en) |
| RO (1) | RO76829A (en) |
| SE (1) | SE434407B (en) |
| YU (1) | YU36540B (en) |
| ZA (1) | ZA7590B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4041317B4 (en) * | 1990-01-18 | 2005-09-08 | Xyrofin Oy | Process for crystallizing crystal water-free fructose from its aqueous solutions |
| KR101749527B1 (en) | 2014-10-20 | 2017-06-21 | 씨제이제일제당(주) | A method of manufacturing a d-psicose crystal |
| US10808002B2 (en) | 2014-10-20 | 2020-10-20 | Cj Cheiljedang Corporation | Method for preparing D-psicose crystal |
| KR101981388B1 (en) * | 2017-06-14 | 2019-05-22 | 씨제이제일제당 (주) | A method of manufacturing a d-psicose crystal |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2949389A (en) * | 1958-03-17 | 1960-08-16 | Dawe S Lab Inc | Production of levulose |
| DE2017500A1 (en) * | 1970-04-11 | 1971-10-28 | Engel, Herbert, 8000 München | Rotating recording and playback systems |
| FI46631C (en) * | 1971-03-11 | 1973-05-08 | Suomen Sokeri Oy | Process for crystallizing fructose from concentrated aqueous solution |
| JPS5239901B2 (en) * | 1973-02-12 | 1977-10-07 |
-
1974
- 1974-12-09 GB GB5305674A patent/GB1456260A/en not_active Expired
- 1974-12-18 CA CA216,625A patent/CA1030533A/en not_active Expired
- 1974-12-30 NL NLAANVRAGE7417006,A patent/NL186183C/en not_active IP Right Cessation
-
1975
- 1975-01-04 ES ES433589A patent/ES433589A1/en not_active Expired
- 1975-01-06 ZA ZA00750090A patent/ZA7590B/en unknown
- 1975-01-06 IE IE27/75A patent/IE41769B1/en unknown
- 1975-01-07 HU HU75SU885A patent/HU174513B/en unknown
- 1975-01-09 YU YU00042/75A patent/YU36540B/en unknown
- 1975-01-14 BE BE152358A patent/BE824362A/en not_active IP Right Cessation
- 1975-01-21 IT IT7547778A patent/IT1026412B/en active
- 1975-01-22 FI FI750158A patent/FI58654C/en not_active IP Right Cessation
- 1975-01-23 DE DE2502558A patent/DE2502558C2/en not_active Expired
- 1975-01-23 RO RO7581207A patent/RO76829A/en unknown
- 1975-01-23 SE SE7500717A patent/SE434407B/en not_active IP Right Cessation
- 1975-01-24 FR FR7502243A patent/FR2259151B1/fr not_active Expired
- 1975-01-24 CH CH88075A patent/CH596318A5/xx not_active IP Right Cessation
- 1975-01-24 CS CS75492A patent/CS207335B2/en unknown
- 1975-01-25 PL PL1975177575A patent/PL102673B1/en unknown
- 1975-01-27 DK DK24875*#A patent/DK24875A/da not_active Application Discontinuation
- 1975-01-27 BG BG028821A patent/BG24961A3/en unknown
- 1975-01-27 AT AT57075A patent/AT346785B/en not_active IP Right Cessation
- 1975-01-28 JP JP50011818A patent/JPS5838160B2/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2259151B1 (en) | 1979-04-13 |
| NL186183C (en) | 1990-10-01 |
| FI58654C (en) | 1981-03-10 |
| YU4275A (en) | 1982-02-25 |
| BG24961A3 (en) | 1978-06-15 |
| CH596318A5 (en) | 1978-03-15 |
| AT346785B (en) | 1978-11-27 |
| YU36540B (en) | 1984-02-29 |
| AU7649374A (en) | 1976-07-01 |
| IT1026412B (en) | 1978-09-20 |
| DE2502558A1 (en) | 1975-07-31 |
| DE2502558C2 (en) | 1981-10-08 |
| NL7417006A (en) | 1975-07-30 |
| FI750158A (en) | 1975-07-29 |
| SE7500717L (en) | 1975-07-29 |
| HU174513B (en) | 1980-01-28 |
| ATA57075A (en) | 1978-03-15 |
| ES433589A1 (en) | 1977-02-16 |
| CS207335B2 (en) | 1981-07-31 |
| JPS5838160B2 (en) | 1983-08-20 |
| DK24875A (en) | 1975-09-29 |
| JPS50105842A (en) | 1975-08-20 |
| NL186183B (en) | 1990-05-01 |
| ZA7590B (en) | 1976-01-28 |
| FR2259151A1 (en) | 1975-08-22 |
| PL102673B1 (en) | 1979-04-30 |
| BE824362A (en) | 1975-05-02 |
| IE41769L (en) | 1975-07-28 |
| CA1030533A (en) | 1978-05-02 |
| RO76829A (en) | 1981-11-04 |
| IE41769B1 (en) | 1980-03-26 |
| SE434407B (en) | 1984-07-23 |
| FI58654B (en) | 1980-11-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US3928062A (en) | Method for obtaining anhydrous fructose crystals | |
| KR860000386A (en) | Method for preparing crystalline alpha-maltose | |
| DK90481A (en) | Crystalline GLUCOSE AND PROCEDURE FOR PREPARING THEREOF | |
| FI831105L (en) | FOERFARANDE FOER FRAMSTAELLNING AV ISOMALTULOS (6-0- -D-GLUCOPYRANOSIDO-D-FRUKTOS) MED TILLHJAELP AV IMMOBILISERADE BAKTERIECELLER. | |
| FI872487A0 (en) | FOERFARANDE FOER KRISTALLISERING AV FRUKTOS. | |
| US2588449A (en) | Levulose dihydrate | |
| GB1456260A (en) | Method for crystallization of fructose from water solution | |
| KR890009961A (en) | High purity crystalline lactulose and preparation method thereof | |
| ES468165A1 (en) | Method for the manufacture of crystals of sodium carbonate monohydrate | |
| IE37304B1 (en) | Improvements in or relating to the crystallisation of fructose | |
| ES462861A1 (en) | Method for the production of powdered dextrose | |
| IE37955B1 (en) | Crystallization apparatus | |
| US1942660A (en) | Process for the preparation of gluconic acid and its lactones | |
| AU2001279834A1 (en) | A method of crystallizing maltitol | |
| SU421355A1 (en) | METHOD OF CULTIVATION OF KALIA BIFTALATE MONOCRYSTALS | |
| FR2114772A5 (en) | ||
| KR870005007A (en) | Glucose isomerase concentrate and preparation method thereof | |
| IE38959B1 (en) | Aqueous crystallization of xylitol | |
| SU528935A1 (en) | The method of producing crystalline hydrates | |
| CA2034475A1 (en) | Method for crystallizing anhydrous fructose from its aqueous solutions | |
| GB1446929A (en) | Process for preparing flavoured materials | |
| GB1135954A (en) | A process for producing monoammonium glutamate and monosodium glutamate therefrom | |
| GB1364982A (en) | Phenylalanine derivatives | |
| KR860008204A (en) | Method for preparing crystalline anhydride 19-deoxyaglycone dianemycin | |
| JPS56122329A (en) | Resolving method of dl-mandelic acid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PE20 | Patent expired after termination of 20 years |
Effective date: 19941208 |