GB1447500A - Thermosetting resin and a process for producing same - Google Patents

Thermosetting resin and a process for producing same

Info

Publication number
GB1447500A
GB1447500A GB5457373A GB5457373A GB1447500A GB 1447500 A GB1447500 A GB 1447500A GB 5457373 A GB5457373 A GB 5457373A GB 5457373 A GB5457373 A GB 5457373A GB 1447500 A GB1447500 A GB 1447500A
Authority
GB
United Kingdom
Prior art keywords
isocyanurate
rings
thermosetting resin
diisocyanate
phenylimidazole
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5457373A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Ltd
Original Assignee
Hitachi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Ltd filed Critical Hitachi Ltd
Publication of GB1447500A publication Critical patent/GB1447500A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C08G59/4007Curing agents not provided for by the groups C08G59/42 - C08G59/66
    • C08G59/4014Nitrogen containing compounds
    • C08G59/4028Isocyanates; Thioisocyanates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/003Polymeric products of isocyanates or isothiocyanates with epoxy compounds having no active hydrogen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04Preparatory processes
    • C08G69/06Solid state polycondensation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2115/00Oligomerisation
    • C08G2115/02Oligomerisation to isocyanurate groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Paints Or Removers (AREA)
  • Manufacture Of Motors, Generators (AREA)
  • Epoxy Resins (AREA)

Abstract

1447500 Polymers containing oxazolidone and isocyanurate rings HITACHI Ltd 23 Nov 1973 [29 Nov 1972] 54573/73 Heading C3B A resin composition comprising one equivalent of an at least di-epoxide (I) and at least 1À5 equivalents of a polyisocyanate (II) is heated at 80‹ C. or above in the presence of 0À1-10% by wt. (of I+II) of a catalyst (III) for the formation of isocyanurate and oxazolidene rings. The product is a thermosetting resin containing as a recurring unit 2 or more isocyanurate rings each connected through an isocyanate residue and an oxazolidone ring connected at one side through an isocyanate residue to an isocyanurate having at the other side an epoxy residue. I may be a diglycidyl ether of bisphenol A or an epoxy novolac resin. II may be 4,4<SP>1</SP>-diphenylmethane diisocyanate, 2,4-tolylene diisocyanate or naphthalene-1,5- diisocyanate. III may be N-methylmorpholine, 2 - phenylimidazole, 1 - cyanoethyl - 2 - phenylimidazole or 2,4 - diamino - 6 - (2<SP>1</SP> - undecylimidazolyl-1<SP>1</SP>-)ethyl-5-triazine. Uses.-Electrical insulation at high temperatures.
GB5457373A 1972-11-29 1973-11-23 Thermosetting resin and a process for producing same Expired GB1447500A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP47118986A JPS5231000B2 (en) 1972-11-29 1972-11-29

Publications (1)

Publication Number Publication Date
GB1447500A true GB1447500A (en) 1976-08-25

Family

ID=14750165

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5457373A Expired GB1447500A (en) 1972-11-29 1973-11-23 Thermosetting resin and a process for producing same

Country Status (11)

Country Link
JP (1) JPS5231000B2 (en)
AU (1) AU470978B2 (en)
CA (1) CA1006293A (en)
CH (1) CH606170A5 (en)
DE (1) DE2359386C3 (en)
FR (1) FR2207952B1 (en)
GB (1) GB1447500A (en)
IN (1) IN140854B (en)
NL (1) NL163539C (en)
SE (1) SE417977B (en)
SU (1) SU525433A3 (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2811858A1 (en) * 1977-03-19 1978-10-05 Hitachi Ltd ELECTRICAL INSULATION ARRANGEMENT
EP1426392A1 (en) * 2001-08-30 2004-06-09 Mitsubishi Gas Chemical Company, Inc. Composition for optical material
WO2012010732A1 (en) * 2010-07-20 2012-01-26 Universitat Politècnica De Catalunya Composition and method for cross-linking an epoxy resin with an isocyanate, and cross-linked material thus obtained
WO2018033562A1 (en) * 2016-08-19 2018-02-22 Covestro Deutschland Ag Process for the synthesis of polyoxazolidinone compounds
US10689476B2 (en) 2014-12-22 2020-06-23 Henkel Ag & Co. Kgaa Oxazolidinone- and isocyanurate-crosslinked matrix for fiber-reinforced material
US10787536B2 (en) 2014-12-22 2020-09-29 Henkel Ag & Co. Kgaa Catalyst composition for curing resins containing epoxy groups
CN117542641A (en) * 2023-11-08 2024-02-09 江苏普隆磁电有限公司 Preparation method of heat-resistant NdFeB magnet

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5727894B2 (en) * 1974-10-11 1982-06-14
JPS5174095A (en) * 1974-12-25 1976-06-26 Mitsubishi Chem Ind Okisazoridon isoshianureetofuoomuno seizoho
JPS51106002A (en) * 1975-03-14 1976-09-20 Hitachi Ltd Denkimakisen no zetsuenshorihoho
JPS51115602A (en) * 1975-04-04 1976-10-12 Hitachi Ltd Winding of electric machines and apparatuses
JPS51121705A (en) * 1975-04-18 1976-10-25 Hitachi Ltd Insulated winding of electric machine
JPS52112799A (en) * 1976-03-19 1977-09-21 Hitachi Ltd Manufacturing method of electrical insulation body
JPS52151396A (en) * 1976-06-11 1977-12-15 Hitachi Chem Co Ltd Composition for anticorrosive frp
JPS53115001A (en) * 1977-03-17 1978-10-07 Matsushita Electric Ind Co Ltd Preparing coreless armature
DE2722400C2 (en) * 1977-05-17 1985-05-30 Bayer Ag, 5090 Leverkusen Process for the production of heat-resistant, bubble-free plastics containing isocyanurate groups
CH624968A5 (en) * 1977-06-14 1981-08-31 Ciba Geigy Ag
DE3068153D1 (en) * 1980-03-03 1984-07-19 Bbc Brown Boveri & Cie Duroplastically hardenable resin mixture free of solvents, and its use
DE3323122A1 (en) * 1983-06-27 1985-05-23 Siemens AG, 1000 Berlin und 8000 München METHOD FOR PRODUCING REACTION RESIN MOLDINGS
DE3323084A1 (en) * 1983-06-27 1985-01-10 Siemens AG, 1000 Berlin und 8000 München METHOD FOR PRODUCING SHAPED MATERIALS
GB8412900D0 (en) * 1984-05-21 1984-06-27 Secr Defence Thermosetting resin compositions
GB8912952D0 (en) * 1989-06-06 1989-07-26 Dow Rheinmuenster Epoxy-terminated polyoxazolidones,process for the preparation thereof and electrical laminates made from the epoxy-terminated polyoxazolidones
JP3133090B2 (en) * 1991-04-03 2001-02-05 富士電機株式会社 Insulation method for salient field winding
DE4223630A1 (en) * 1992-07-17 1994-01-20 Siemens Ag Prepolymer epoxy resin mixture containing oxazolidinone structures
JPH0686384U (en) * 1993-05-17 1994-12-13 ホシデン株式会社 Electric cord drawer
US20150210846A1 (en) * 2012-04-27 2015-07-30 Dow Global Technologies Llc Curable epoxy resin compositions and composites made therefrom
KR102021318B1 (en) * 2012-06-26 2019-09-16 다우 글로벌 테크놀로지스 엘엘씨 Insulating composites for power transmission and distribution
US9834671B2 (en) * 2012-11-07 2017-12-05 Dow Global Technologies Llc Curable epoxy composition and a composite made therefrom
JP6903899B2 (en) * 2016-11-25 2021-07-14 東ソー株式会社 Hard Isocyanurate Foam Composition and Method for Producing Hard Isocyanurate Foam
MX2020011821A (en) * 2018-05-18 2021-02-09 Dow Global Technologies Llc A polyisocyanate component, a polyurethane foaming system and an article made therefrom.

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA833619A (en) * 1970-02-03 Edward F. Hayash, Jr. High temperature resistant, low flame spread cellular polymers
DE951168C (en) * 1953-02-01 1956-10-25 Bayer Ag Process for the production of higher molecular weight polyisocyanates
US3020262A (en) * 1957-12-19 1962-02-06 Jefferson Chem Co Inc Method for producing 2-oxazolidones from epoxides and isocyanates
BE593093A (en) * 1959-09-12
US3198551A (en) * 1961-03-27 1965-08-03 Garner Fay Troy Pusher vehicle
US3206352A (en) * 1962-03-23 1965-09-14 Monsanto Res Corp Polymeric polyisocyanurate laminating resin prepared from a diaryl dhsocyanate and acocatalyst system
US3211703A (en) * 1962-03-23 1965-10-12 Monsanto Res Corp Polyaliphatic polyisocyanurate laminating resin prepared in the presence of a cocatalyst system
US3494888A (en) * 1966-08-30 1970-02-10 Wilbur R Mcelroy Resin compositions from polyepoxides and isocyanate polymers
US3745133A (en) * 1968-02-05 1973-07-10 Upjohn Co Cellular isocyanurate containing polymers
US3793236A (en) * 1971-02-12 1974-02-19 Mitsubishi Chem Ind Oxazolidone-modified isocyanurate resins

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2811858A1 (en) * 1977-03-19 1978-10-05 Hitachi Ltd ELECTRICAL INSULATION ARRANGEMENT
US4239998A (en) 1977-03-19 1980-12-16 Hitachi, Ltd. Method for electrically insulating an electrically conducting article and product produced thereby
EP1426392A1 (en) * 2001-08-30 2004-06-09 Mitsubishi Gas Chemical Company, Inc. Composition for optical material
EP1426392A4 (en) * 2001-08-30 2004-11-10 Mitsubishi Gas Chemical Co Composition for optical material
US6960640B2 (en) 2001-08-30 2005-11-01 Mitsubishi Gas Chemical Co., Ltd. Composition for optical material
ES2373276A1 (en) * 2010-07-20 2012-02-02 Universitat Rovira I Virgili Composition and method for cross-linking an epoxy resin with an isocyanate, and cross-linked material thus obtained
WO2012010732A1 (en) * 2010-07-20 2012-01-26 Universitat Politècnica De Catalunya Composition and method for cross-linking an epoxy resin with an isocyanate, and cross-linked material thus obtained
US10689476B2 (en) 2014-12-22 2020-06-23 Henkel Ag & Co. Kgaa Oxazolidinone- and isocyanurate-crosslinked matrix for fiber-reinforced material
US10787536B2 (en) 2014-12-22 2020-09-29 Henkel Ag & Co. Kgaa Catalyst composition for curing resins containing epoxy groups
WO2018033562A1 (en) * 2016-08-19 2018-02-22 Covestro Deutschland Ag Process for the synthesis of polyoxazolidinone compounds
CN109642010A (en) * 2016-08-19 2019-04-16 科思创德国股份有限公司 The synthetic method of poly- Oxazolidinone compound
CN109642010B (en) * 2016-08-19 2021-06-04 科思创德国股份有限公司 Synthesis method of polyoxazolidone compound
US11326018B2 (en) 2016-08-19 2022-05-10 Covestro Deutschland Ag Process for the synthesis of polyoxazolidinone compounds
CN117542641A (en) * 2023-11-08 2024-02-09 江苏普隆磁电有限公司 Preparation method of heat-resistant NdFeB magnet

Also Published As

Publication number Publication date
AU470978B2 (en) 1976-04-08
AU6294773A (en) 1975-05-29
FR2207952B1 (en) 1978-11-10
CA1006293A (en) 1977-03-01
CH606170A5 (en) 1978-10-31
SE417977B (en) 1981-04-27
FR2207952A1 (en) 1974-06-21
NL7316281A (en) 1974-05-31
SU525433A3 (en) 1976-08-15
NL163539B (en) 1980-04-15
DE2359386C3 (en) 1985-12-05
DE2359386A1 (en) 1974-06-20
JPS4994798A (en) 1974-09-09
NL163539C (en) 1980-09-15
DE2359386B2 (en) 1980-08-07
IN140854B (en) 1977-01-01
JPS5231000B2 (en) 1977-08-11

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PE20 Patent expired after termination of 20 years

Effective date: 19931122