GB1432190A - Separation of acrylic acid from the reaction gases from propylene or acrolein oxidation - Google Patents
Separation of acrylic acid from the reaction gases from propylene or acrolein oxidationInfo
- Publication number
- GB1432190A GB1432190A GB3991673A GB3991673A GB1432190A GB 1432190 A GB1432190 A GB 1432190A GB 3991673 A GB3991673 A GB 3991673A GB 3991673 A GB3991673 A GB 3991673A GB 1432190 A GB1432190 A GB 1432190A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acrylic acid
- propylene
- absorber
- aug
- separation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 title abstract 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title abstract 6
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 title abstract 4
- 230000003647 oxidation Effects 0.000 title abstract 2
- 238000007254 oxidation reaction Methods 0.000 title abstract 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 title abstract 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 title abstract 2
- 238000006243 chemical reaction Methods 0.000 title 1
- 239000007789 gas Substances 0.000 title 1
- 238000000926 separation method Methods 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- 238000010521 absorption reaction Methods 0.000 abstract 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- 239000006096 absorbing agent Substances 0.000 abstract 2
- 150000001733 carboxylic acid esters Chemical class 0.000 abstract 2
- 150000002148 esters Chemical class 0.000 abstract 2
- 239000011261 inert gas Substances 0.000 abstract 2
- 239000012495 reaction gas Substances 0.000 abstract 2
- 239000002250 absorbent Substances 0.000 abstract 1
- 230000002745 absorbent Effects 0.000 abstract 1
- 150000001279 adipic acids Chemical class 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- -1 isooctyl-2-ethylhexyl Chemical group 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 abstract 1
- 150000002889 oleic acids Chemical class 0.000 abstract 1
- 150000003022 phthalic acids Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
- C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1487—Removing organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1493—Selection of liquid materials for use as absorbents
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/22—Accessories
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treating Waste Gases (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2241714A DE2241714A1 (de) | 1972-08-24 | 1972-08-24 | Verfahren zur abtrennung von acrylsaeure aus den reaktionsgasen der propylenoder acroleinoxydation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1432190A true GB1432190A (en) | 1976-04-14 |
Family
ID=5854458
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3991673A Expired GB1432190A (en) | 1972-08-24 | 1973-08-23 | Separation of acrylic acid from the reaction gases from propylene or acrolein oxidation |
Country Status (10)
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5728872A (en) * | 1994-06-27 | 1998-03-17 | Lutz Riemenschneider | Stabilized acrylic acid compositions |
| US6575250B1 (en) | 1999-11-15 | 2003-06-10 | Shell Oil Company | Expanding a tubular element in a wellbore |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AR206439A1 (es) * | 1974-10-07 | 1976-07-23 | Celanese Corp | Un metodo para la recuperacion de un acido acrilico crudo |
| DE2449780C3 (de) * | 1974-10-19 | 1987-01-22 | Basf Ag, 6700 Ludwigshafen | Verfahren zum Abtrennen schwer- oder nichtflüchtiger Nebenprodukte der Propylen- und/oder Acroleinoxidation von den für die Absorbtion der Acrylsäure aus den Reaktionsgasen verwendeten Lösungsmitteln |
| FR2427117A1 (fr) * | 1978-06-01 | 1979-12-28 | Mo I Khim | Procede de formation de courants dans les appareils d'echange de masse et de chaleur |
| US4180681A (en) * | 1978-08-17 | 1979-12-25 | Atlantic Richfield Company | Preparation and recovery of methacrylic acid from an aqueous sodium methacrylate solution |
| US4999452A (en) * | 1989-05-15 | 1991-03-12 | Union Carbide Chemicals And Plastics Company Inc. | Process for producing acrylic ester |
| JP3289303B2 (ja) * | 1992-03-06 | 2002-06-04 | 住友化学工業株式会社 | アクロレインの製造方法 |
| DE4308087C2 (de) * | 1993-03-13 | 1997-02-06 | Basf Ag | Verfahren zur Abtrennung von Acrylsäure aus den Reaktionsgasen der katalytischen Oxidation von Propylen und/oder Acrolein |
| DE4436243A1 (de) * | 1994-10-11 | 1996-04-18 | Basf Ag | Verfahren zur Abtrennung von (Meth)acrylsäure aus dem Reaktionsgasgemisch der katalytischen Gasphasenoxidation C¶3¶-/C¶4¶-Verbindungen |
| FR2735989B1 (fr) * | 1995-06-29 | 1997-08-14 | Rhone Poulenc Nutrition Animal | Procede et installation de purification d'un flux gazeux contenant de l'acroleine |
| FR2736912B1 (fr) * | 1995-07-18 | 1997-08-22 | Atochem Elf Sa | Procede de purification de l'acide acrylique obtenu par oxydation catalytique du propylene |
| FR2756280B1 (fr) * | 1996-11-25 | 1998-12-24 | Atochem Elf Sa | Purification de l'acide acrylique obtenu par oxydation catalytique du propylene |
| US6180827B1 (en) * | 1998-02-03 | 2001-01-30 | Hfm International, Inc. | Recovery of acrylic acid from process or waste water streams |
| JP3948855B2 (ja) * | 1999-06-10 | 2007-07-25 | 株式会社日本触媒 | （メタ）アクリル酸の製造方法 |
| JP4308372B2 (ja) | 1999-07-06 | 2009-08-05 | 株式会社日本触媒 | （メタ）アクリル酸および／または（メタ）アクロレインの吸収方法及びその装置 |
| US6888025B2 (en) * | 2000-02-14 | 2005-05-03 | Nippon Shokubai, Co. Ltd. | Method for absorbing acrylic acid and method for purifying acrylic acid |
| JP2001226320A (ja) * | 2000-02-14 | 2001-08-21 | Nippon Shokubai Co Ltd | アクリル酸の捕集方法およびアクリル酸の精製方法 |
| DE10138150A1 (de) * | 2001-08-03 | 2003-02-13 | Basf Ag | Verfahren zur Herstellung wasserabsorbierender Harze |
| FR2861724B1 (fr) | 2003-11-04 | 2005-12-30 | Arkema | Procede de purification de l'acide (meth)acrylique obtenu par oxydation d'un substrat gazeux |
| US9156769B2 (en) | 2008-10-15 | 2015-10-13 | Arkema Inc. | Method of recovering carboxylic acids from dilute aqueous streams |
| WO2010044990A1 (en) * | 2008-10-15 | 2010-04-22 | Arkema Inc. | Method of recovering carboxylic acids from dilute aqueous streams |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1359885A (fr) * | 1963-03-21 | 1964-04-30 | Electrochimie Soc | Procédé de fabrication d'acide acrylique glacial |
| GB995472A (en) * | 1963-05-16 | 1965-06-16 | Distillers Co Yeast Ltd | Improvements in or relating to acrylic acid production |
| GB997325A (en) * | 1963-06-20 | 1965-07-07 | Distillers Co Yeast Ltd | Recovery of acrylic acid |
| US3555082A (en) * | 1966-12-15 | 1971-01-12 | Knapsack Ag | Process for isolating acrylic acid from the reaction gases obtained by oxidation of propylene or acrolein |
| DE1618612B2 (de) * | 1967-06-29 | 1973-03-15 | Knapsack AG, 5033 Hurth Knapsack | Verfahren zur gewinnung reiner acrylsaeure aus waessriger rohsaeure |
| US3666632A (en) * | 1968-10-08 | 1972-05-30 | Asahi Chemical Ind | Method for the separation of acrylic acid from aqueous solution containing acrylic acid and acetic acid |
| US3527677A (en) * | 1969-03-06 | 1970-09-08 | Goodrich Co B F | Process for dehydration of aqueous acrylic acid solutions by extractive - azeotropic distillation with 2-ethylhexanol or 2-ethylhexylacrylate |
| JPS4924898B1 (US06653308-20031125-C00199.png) * | 1970-12-26 | 1974-06-26 | ||
| BE786398A (fr) * | 1971-07-21 | 1973-01-18 | Basf Ag | Procede de preparation de l'acide acrylique anhydre |
-
1972
- 1972-08-24 DE DE2241714A patent/DE2241714A1/de active Pending
-
1973
- 1973-07-30 CH CH1106073A patent/CH581598A5/xx not_active IP Right Cessation
- 1973-08-21 NL NL7311516A patent/NL7311516A/xx unknown
- 1973-08-21 CA CA179,316A patent/CA1001655A/en not_active Expired
- 1973-08-21 FR FR7330273A patent/FR2196986B1/fr not_active Expired
- 1973-08-23 IT IT52149/73A patent/IT990407B/it active
- 1973-08-23 US US391012A patent/US3868417A/en not_active Expired - Lifetime
- 1973-08-23 GB GB3991673A patent/GB1432190A/en not_active Expired
- 1973-08-24 BE BE134898A patent/BE803985A/xx unknown
- 1973-08-24 JP JP9452673A patent/JPS5621010B2/ja not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5728872A (en) * | 1994-06-27 | 1998-03-17 | Lutz Riemenschneider | Stabilized acrylic acid compositions |
| US6575250B1 (en) | 1999-11-15 | 2003-06-10 | Shell Oil Company | Expanding a tubular element in a wellbore |
Also Published As
| Publication number | Publication date |
|---|---|
| BE803985A (fr) | 1974-02-25 |
| CH581598A5 (US06653308-20031125-C00199.png) | 1976-11-15 |
| FR2196986A1 (US06653308-20031125-C00199.png) | 1974-03-22 |
| CA1001655A (en) | 1976-12-14 |
| FR2196986B1 (US06653308-20031125-C00199.png) | 1977-02-25 |
| US3868417A (en) | 1975-02-25 |
| JPS4956915A (US06653308-20031125-C00199.png) | 1974-06-03 |
| IT990407B (it) | 1975-06-20 |
| JPS5621010B2 (US06653308-20031125-C00199.png) | 1981-05-16 |
| DE2241714A1 (de) | 1974-03-28 |
| DE2241714B2 (US06653308-20031125-C00199.png) | 1974-09-19 |
| NL7311516A (US06653308-20031125-C00199.png) | 1974-02-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |