GB1421577A - Continuously operating evaporation drystallisation apparatus - Google Patents
Continuously operating evaporation drystallisation apparatusInfo
- Publication number
- GB1421577A GB1421577A GB1393973A GB1393973A GB1421577A GB 1421577 A GB1421577 A GB 1421577A GB 1393973 A GB1393973 A GB 1393973A GB 1393973 A GB1393973 A GB 1393973A GB 1421577 A GB1421577 A GB 1421577A
- Authority
- GB
- United Kingdom
- Prior art keywords
- partitions
- solution
- compartment
- compartments
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
- B01D9/0031—Evaporation of components of the mixture to be separated by heating
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Seasonings (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
1421577 Evaporative crystallisation SOC FIVES LILLE-CAIL 22 March 1973 [29 March 1972] 13939/73 Heading BIG Apparatus for crystallizing by evaporation and which includes regulating the supply of sub-saturated solution and also washing the inner walls of the apparatus with this solution comprises a vertically disposed cylindrical tank in which the lower portion of the tank is divided into a plurality of compartments by radial partitions and wherein successive compartments communicate with each other by apertures formed in the partitions except for the outlet compartment and that one situated immediately after it and a device for supplying sub-saturated solution comprising a pipe with a plurality of holes spaced along the pipe from which is projected the solution, means for rotating the pipe about a vertical axis above the partitions and shutter means associated with the partitions to regulate the cross-sectional opening at the top of each compartment whereby the rate of flow of subsaturated solution into each compartment is regulated. Preferably the shutters are mounted so as to be capable of pivoting on the upper edge of the partitions. Figures 1 and 3 show respectively a vertical section of a crystallisation apparatus and a digrammatic view of the radial partitions and shutters wherein tank 10 is divided into eight compartments by partitions 15 which contain apertures 28 except in compartments 0 and 7. In compartment 0 the solution is concentrated by heater 30, until saturated, whilst from 7 the desired crystalline material is recovered from a conduit (not shown). The jet pipe 32 is rotated by a geared motor (not shown) and distributes the unsaturated solution successively into all the compartments, the distribution into each compartment being regulated by movable shutters 18 pivoting on axis 20.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7210951A FR2177535A1 (en) | 1972-03-29 | 1972-03-29 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1421577A true GB1421577A (en) | 1976-01-21 |
Family
ID=9095970
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1393973A Expired GB1421577A (en) | 1972-03-29 | 1973-03-22 | Continuously operating evaporation drystallisation apparatus |
Country Status (17)
Country | Link |
---|---|
US (1) | US3880593A (en) |
JP (1) | JPS498461A (en) |
AR (1) | AR197595A1 (en) |
BE (1) | BE797530A (en) |
BR (1) | BR7302238D0 (en) |
CA (1) | CA990638A (en) |
CS (1) | CS170469B2 (en) |
DE (1) | DE2315835C3 (en) |
ES (1) | ES413034A1 (en) |
FR (1) | FR2177535A1 (en) |
GB (1) | GB1421577A (en) |
IT (1) | IT981717B (en) |
NL (1) | NL7304424A (en) |
PL (1) | PL85222B1 (en) |
SE (1) | SE375914B (en) |
SU (1) | SU480210A3 (en) |
ZA (1) | ZA732072B (en) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2695837B1 (en) * | 1992-09-24 | 1994-11-25 | Fcb | Continuous evaporative crystallization apparatus. |
DE19747218B4 (en) * | 1997-10-25 | 2004-07-08 | Gebrüder Lödige Maschinenbau-Gesellschaft mit beschränkter Haftung | Process for the recovery and drying of a solid contained in a pumpable liquid |
BR0111644B1 (en) * | 2000-06-01 | 2010-12-28 | continuous vacuum tank and method of crystallization of the solute of a solution. | |
CN102215928B (en) * | 2008-09-18 | 2013-11-27 | 唐加特胡雷特有限公司 | Continuous vacuum pand internal insulation arrangement thereof |
CN103463824A (en) * | 2013-09-29 | 2013-12-25 | 王金林 | Efficient rotating spray evaporator |
CN105126381B (en) * | 2015-09-15 | 2017-02-01 | 山东东源新材料科技有限公司 | Evaporation crystallization system for producing vanadium-free rare-earth base titanium tungsten powder |
RU2686656C1 (en) * | 2018-08-10 | 2019-04-29 | Ануар Райханович Кулмагамбетов | Evaporator for producing steam using volcanic magma and method of operation thereof |
WO2021239813A1 (en) * | 2020-05-27 | 2021-12-02 | Pfeifer & Langen GmbH & Co. KG | Crystallization of allulose under reduced pressure |
EP4000419A1 (en) | 2020-11-23 | 2022-05-25 | Savanna Ingredients GmbH | Drying of allulose crystals |
CN113856235A (en) * | 2021-09-29 | 2021-12-31 | 浙江大华技术股份有限公司 | Cooling crystallization control method, device, electronic equipment and system |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1340653A (en) * | 1918-07-30 | 1920-05-18 | Freeman I Gibson | Apparatus and process for the continuous distillation of liquids |
US1799478A (en) * | 1925-02-05 | 1931-04-07 | David D Peebles | Method of evaporating liquids and apparatus therefor |
US2658029A (en) * | 1951-10-27 | 1953-11-03 | Metallgesellschaft Ag | Distillation method and apparatus |
US2993844A (en) * | 1958-05-13 | 1961-07-25 | Chicago Bridge & Iron Co | Multi-stage flash evaporator |
DE1418567A1 (en) * | 1960-05-25 | 1968-10-10 | Ajinomoto Kk | Process for the continuous, optical separation of racemic mixtures of gultamic acid, glutamic acid hydrohalides and glutamates |
US3424221A (en) * | 1966-06-06 | 1969-01-28 | Gene W Luce | Apparatus and method for continuous crystallization by evaporation |
FR1494289A (en) * | 1966-07-28 | 1967-09-08 | Fives Lille Cail | Method and device for preventing fouling of walls in continuously operating evaporative crystallization apparatus |
FR1581088A (en) * | 1968-07-17 | 1969-09-12 | ||
FR2101257A5 (en) * | 1970-03-19 | 1972-03-31 | Fives Lille Cail | |
US3715191A (en) * | 1970-07-13 | 1973-02-06 | Whiting Corp | Apparatus for making wet process phosphoric acid |
-
1972
- 1972-03-29 FR FR7210951A patent/FR2177535A1/fr not_active Withdrawn
-
1973
- 1973-03-22 GB GB1393973A patent/GB1421577A/en not_active Expired
- 1973-03-26 ZA ZA732072A patent/ZA732072B/en unknown
- 1973-03-27 SE SE7304309A patent/SE375914B/xx unknown
- 1973-03-27 ES ES413034A patent/ES413034A1/en not_active Expired
- 1973-03-28 SU SU1899941A patent/SU480210A3/en active
- 1973-03-28 CA CA167,388A patent/CA990638A/en not_active Expired
- 1973-03-28 IT IT22290/73A patent/IT981717B/en active
- 1973-03-28 BR BR732238A patent/BR7302238D0/en unknown
- 1973-03-29 BE BE129440A patent/BE797530A/en unknown
- 1973-03-29 JP JP48035127A patent/JPS498461A/ja active Pending
- 1973-03-29 AR AR247307A patent/AR197595A1/en active
- 1973-03-29 PL PL1973161584A patent/PL85222B1/pl unknown
- 1973-03-29 US US345993A patent/US3880593A/en not_active Expired - Lifetime
- 1973-03-29 CS CS2296A patent/CS170469B2/cs unknown
- 1973-03-29 DE DE2315835A patent/DE2315835C3/en not_active Expired
- 1973-03-29 NL NL7304424A patent/NL7304424A/xx not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
DE2315835B2 (en) | 1977-11-17 |
FR2177535A1 (en) | 1973-11-09 |
SE375914B (en) | 1975-05-05 |
CS170469B2 (en) | 1976-08-27 |
NL7304424A (en) | 1973-10-02 |
CA990638A (en) | 1976-06-08 |
SU480210A3 (en) | 1975-08-05 |
ES413034A1 (en) | 1976-01-16 |
IT981717B (en) | 1974-10-10 |
US3880593A (en) | 1975-04-29 |
DE2315835C3 (en) | 1978-07-13 |
BR7302238D0 (en) | 1974-07-25 |
PL85222B1 (en) | 1976-04-30 |
DE2315835A1 (en) | 1973-10-11 |
AR197595A1 (en) | 1974-04-23 |
BE797530A (en) | 1973-07-16 |
ZA732072B (en) | 1973-12-19 |
JPS498461A (en) | 1974-01-25 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed [section 19, patents act 1949] | ||
PCNP | Patent ceased through non-payment of renewal fee |