GB1379126A - Process for the manufacture of lactams - Google Patents
Process for the manufacture of lactamsInfo
- Publication number
- GB1379126A GB1379126A GB1471072A GB1471072A GB1379126A GB 1379126 A GB1379126 A GB 1379126A GB 1471072 A GB1471072 A GB 1471072A GB 1471072 A GB1471072 A GB 1471072A GB 1379126 A GB1379126 A GB 1379126A
- Authority
- GB
- United Kingdom
- Prior art keywords
- gas
- lactams
- neutralization
- bisulphate
- rearrangement
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003951 lactams Chemical class 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 239000007789 gas Substances 0.000 abstract 4
- NXPHCVPFHOVZBC-UHFFFAOYSA-N hydroxylamine;sulfuric acid Chemical compound ON.OS(O)(=O)=O NXPHCVPFHOVZBC-UHFFFAOYSA-N 0.000 abstract 3
- 238000006386 neutralization reaction Methods 0.000 abstract 3
- 230000008707 rearrangement Effects 0.000 abstract 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 2
- 239000005864 Sulphur Substances 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-M bisulphate group Chemical group S([O-])(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 abstract 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 2
- VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 abstract 2
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 abstract 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 238000002360 preparation method Methods 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 1
- 239000004157 Nitrosyl chloride Substances 0.000 abstract 1
- BIGPRXCJEDHCLP-UHFFFAOYSA-N ammonium bisulfate Chemical compound [NH4+].OS([O-])(=O)=O BIGPRXCJEDHCLP-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000002485 combustion reaction Methods 0.000 abstract 1
- 239000000446 fuel Substances 0.000 abstract 1
- 239000000295 fuel oil Substances 0.000 abstract 1
- 239000003345 natural gas Substances 0.000 abstract 1
- VPCDQGACGWYTMC-UHFFFAOYSA-N nitrosyl chloride Chemical compound ClN=O VPCDQGACGWYTMC-UHFFFAOYSA-N 0.000 abstract 1
- 235000019392 nitrosyl chloride Nutrition 0.000 abstract 1
- 238000006146 oximation reaction Methods 0.000 abstract 1
- 150000002923 oximes Chemical class 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000002243 precursor Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/48—Sulfur dioxide; Sulfurous acid
- C01B17/50—Preparation of sulfur dioxide
- C01B17/501—Preparation of sulfur dioxide by reduction of sulfur compounds
- C01B17/504—Preparation of sulfur dioxide by reduction of sulfur compounds of ammonium sulfates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/24—Sulfates of ammonium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Hydrogenated Pyridines (AREA)
- Cephalosporin Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712130036 DE2130036B2 (de) | 1971-06-18 | 1971-06-18 | Verfahren zur herstellung von lactamen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1379126A true GB1379126A (en) | 1975-01-02 |
Family
ID=5810994
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1471072A Expired GB1379126A (en) | 1971-06-18 | 1972-03-29 | Process for the manufacture of lactams |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4054562A (enExample) |
| JP (1) | JPS4917276B1 (enExample) |
| AT (1) | AT318642B (enExample) |
| BE (1) | BE784559A (enExample) |
| CH (1) | CH591442A5 (enExample) |
| DE (1) | DE2130036B2 (enExample) |
| ES (1) | ES404007A1 (enExample) |
| FR (1) | FR2141794B1 (enExample) |
| GB (1) | GB1379126A (enExample) |
| IT (1) | IT956409B (enExample) |
| NL (1) | NL7207713A (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL7601061A (nl) * | 1976-02-03 | 1977-08-05 | Stamicarbon | Werkwijze voor het winnen van epsilon-caprolac- tam uit een epsilon-caprolactamzwavelzuur-reac- tiemengsel. |
| NL7607047A (nl) * | 1976-06-28 | 1977-12-30 | Stamicarbon | Werkwijze voor het winnen van epsilon-caprolac- tam uit een epsilon-caprolactam-zwavelzuur- -reactiemengsel. |
| NL7700882A (nl) * | 1977-01-28 | 1978-08-01 | Stamicarbon | Werkwijze voor het winnen van epsilon-caprolac- tam uit een epsilon-caprolactamzwavelzuurreac- tiemengsel. |
| DE2845019A1 (de) * | 1978-10-16 | 1980-04-30 | Basf Ag | Verfahren zur kontinuierlichen herstellung von epsilon -caprolactam durch beckmann'sche umlagerung |
| IL64712A (en) * | 1982-01-05 | 1984-07-31 | Fertilizer Dev Sa | Process for recovering sulfuric acid and ammonia from diammonium sulfate |
| GB8610856D0 (en) * | 1986-05-02 | 1986-06-11 | Boc Group Plc | Treatment of waste material |
| US5498790A (en) * | 1993-06-09 | 1996-03-12 | Novus International, Inc. | Regeneration of sulfuric acid from sulfate by-products of 2-hydroxy-4-(methylthio)butyric acid manufacture |
| US6469163B1 (en) * | 1998-12-24 | 2002-10-22 | Praxair Technology Inc. | Method for production of hydroxylamine sulfate in the conventional process for the synthesis of caprolactam |
| US7022844B2 (en) | 2002-09-21 | 2006-04-04 | Honeywell International Inc. | Amide-based compounds, production, recovery, purification and uses thereof |
| ES2757073T3 (es) | 2015-04-02 | 2020-04-28 | Anthea Aromatics Private Ltd | Procedimiento eficaz para la síntesis de amidas cíclicas |
| WO2026017802A1 (en) | 2024-07-18 | 2026-01-22 | Katholieke Universiteit Leuven | Process for the recovery of sulphuric acid and base from inorganic sulphate salts |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3133055A (en) * | 1964-05-12 | Production ofcaprolactam | ||
| US2221369A (en) * | 1940-11-12 | Process foe producing lactams | ||
| BE621900A (enExample) * | 1961-08-30 | 1900-01-01 | ||
| DE1199243B (de) * | 1963-07-10 | 1965-08-26 | Huels Chemische Werke Ag | Verfahren zur Herstellung schwefeldioxydhaltiger Gase aus ammoniumsalzhaltigen Abfallschwefelsaeuren |
| NL136780C (enExample) * | 1963-10-31 | |||
| GB1084096A (enExample) * | 1963-12-03 | 1900-01-01 | ||
| DE1229995B (de) * | 1964-01-17 | 1966-12-08 | Chemiebau Dr A Zieren Ges Mit | Verfahren zur Gewinnung von Ammoniak und Schwefeldioxyd |
| NL135679C (enExample) * | 1968-11-12 | 1900-01-01 | ||
| GB1367241A (en) * | 1971-02-19 | 1974-09-18 | Zieren Chemiebau Gmbh Dr A | Process for the combustion of ammonium sulphate |
| DE2110036C3 (de) * | 1971-03-03 | 1975-10-02 | Davy Powergas Gmbh, 5000 Koeln | Verfahren zur Spaltung von Ammoniumsulfat |
| CA989830A (en) * | 1971-05-07 | 1976-05-25 | Abraham H. De Rooij | Process for preparing and recovering lactams |
| NL164028C (nl) * | 1971-05-07 | 1980-11-17 | Stamicarbon | Werkwijze voor de afscheiding van lactamen. |
-
1971
- 1971-06-18 DE DE19712130036 patent/DE2130036B2/de not_active Withdrawn
-
1972
- 1972-03-29 GB GB1471072A patent/GB1379126A/en not_active Expired
- 1972-05-11 JP JP47046833A patent/JPS4917276B1/ja active Pending
- 1972-06-07 NL NL7207713A patent/NL7207713A/xx unknown
- 1972-06-08 BE BE784559A patent/BE784559A/xx unknown
- 1972-06-08 FR FR7220559A patent/FR2141794B1/fr not_active Expired
- 1972-06-08 AT AT492872A patent/AT318642B/de not_active IP Right Cessation
- 1972-06-09 IT IT25479/72A patent/IT956409B/it active
- 1972-06-09 US US05/261,219 patent/US4054562A/en not_active Expired - Lifetime
- 1972-06-15 CH CH896172A patent/CH591442A5/xx not_active IP Right Cessation
- 1972-06-17 ES ES404007A patent/ES404007A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| IT956409B (it) | 1973-10-10 |
| BE784559A (fr) | 1972-10-02 |
| DE2130036B2 (de) | 1977-02-10 |
| NL7207713A (enExample) | 1972-12-20 |
| US4054562A (en) | 1977-10-18 |
| AT318642B (de) | 1974-11-11 |
| DE2130036A1 (de) | 1973-01-04 |
| JPS4917276B1 (enExample) | 1974-04-27 |
| ES404007A1 (es) | 1975-06-01 |
| FR2141794B1 (enExample) | 1977-12-23 |
| CH591442A5 (enExample) | 1977-09-15 |
| FR2141794A1 (enExample) | 1973-01-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB1379126A (en) | Process for the manufacture of lactams | |
| US3761575A (en) | Process for the cracking of ammonium sulfate | |
| US3991047A (en) | Process for preparing lactams | |
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| GB1370951A (en) | Process for the manufacture of a lactam | |
| GB1506139A (en) | Process for the recovery of epsilon-caprolactam from a reaction mixture of epsilon-caprolactam and sulphuric acid | |
| CA1115929A (en) | Process for the recovery of ammonia and sulphur dioxide from a contaminated ammonium salt of sulphuric acid | |
| US4140685A (en) | Process for recovering ε-caprolactam from an ε-caprolactam/sulfuric acid reaction mixture | |
| GB1221627A (en) | Improved oxime preparation | |
| GB1407161A (en) | Process for the production of a sulphur dioxide-containing gas | |
| US3758564A (en) | Process for preparation of straight chain alkane dicarboxylic acids | |
| US3133055A (en) | Production ofcaprolactam | |
| GB1106740A (en) | Process for the preparation of lactams | |
| GB1491139A (en) | Simultaneous production of cyclohexanone oxime and concentrated ammonium sulphate solution | |
| CA1100961A (en) | PROCESS FOR THE RECOVERY OF .epsilon.-CAPROLACTAM FROM A REACTION MIXTURE OF .epsilon.-CAPROLACTAM AND SULPHURIC ACID | |
| GB1277592A (en) | A process for the production of an amorphous highly dispersed germanium dioxide | |
| GB1374545A (en) | Process and apparatus for the manufacture of phosphorous acid | |
| US3821202A (en) | Process for purifying lactams | |
| GB1379283A (en) | Separation of lactam from a medium containing concentrated sulphuric acid or sulphuric acid and sulphur trioxide | |
| GB758400A (en) | Process for the separation of sulphur from oxime-sulphur mixtures | |
| GB830630A (en) | Improvements in the production of lactams from oxime hydrochlorides | |
| GB1353448A (en) | Process for preparing lactams | |
| KR810000781B1 (ko) | ε-카프로락탐과 황산의 반응혼합물로부터 ε-카프로락탐을 회수하는 방법 | |
| GB1317638A (en) | Process for the selective production of laurolactam | |
| US2733239A (en) | Process for the separation of sulphur |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |